Metrology and instrumentation: practical applications for engineering and manufacturing (wiley-asme

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MetrologyandInstrumentation

PracticalApplicationsforEngineeringandManufacturing

SamirMekid

KingFahdUniversityofPetroleum&Minerals

Dhahran,SaudiArabia

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Names:Mekid,Samir,author.

Title:Metrologyandinstrumentation:practicalapplicationsfor engineeringandmanufacturing/SamirMekid.

Description:Hoboken,NJ:Wiley,2021.|Series:Wiley-ASMEPressseries| Includesindex.

Identifiers:LCCN2021034345(print)|LCCN2021034346(ebook)|ISBN 9781119721734(hardback)|ISBN9781119721727(adobepdf)|ISBN 9781119721710(epub)

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Contents

Preface xiii Acknowledgments xv AbouttheAuthor xvii

1FundamentalUnitsandConstantsinMetrology 1

1.1Introduction 1

1.2CurrentDefinitionsoftheMainSIUnits 6

1.3NewDefinitionofSevenBaseUnitsoftheSI 6

1.4DerivedInternationalSystem(SI)Units 7

1.5SIConversion 7

1.6FundamentalConstants 8

1.7CommonMeasurements 9

1.8PrinciplesandPracticesofTraceability 10

1.8.1DefinitionofTraceability 10

1.8.2AccreditationandConformityAssessment 11 MultipleChoiceQuestionsofthisChapter 12 References 12

2ScalesofMetrology 13

2.1IntroductiontoPracticalMetrologyacrossAllScales 13 2.2Nanometrology 14

2.2.1IntroductionandNeedinIndustry 14

2.2.2DefinitionofNanometrology 15

2.2.3ImportanceofNanometrologyinScienceandTechnology 15

2.3Standards 18

2.4Micrometrology 22

2.4.1IntroductionandNeedinIndustry 22

2.4.2DefinitionofMicrometrology 22

2.4.3ExamplesofMicrometrologyofMicroparts 22

2.5MacroscaleMetrology 23

2.5.1Standards 25

2.6Large-ScaleMetrologyandLarge-VolumeMetrology 29

2.6.1IntroductionandNeedinIndustry 29

2.6.2Definition 30

2.6.3VerificationStandards 32

2.7InstrumentsTechniques 34

2.7.1LargeCoordinateMeasuringMachines 35

2.7.2LaserTrackers 35

2.7.3Theodolite 35 MultipleChoiceQuestionsofthisChapter 37 References 37

3AppliedMathandStatistics 39

3.1Introduction 39

3.2ScientificandEngineeringNotation 39

3.3Imperial/MetricConversions 40

3.4Ratio 41

3.5LinearInterpolation 42

3.6NumberBases 42

3.7SignificantFigures,Rounding,andTruncation 43

3.8GeometryandVolumes 44

3.8.1Perimeter 44

3.8.2VolumeandArea 44

3.9AngularConversions 44

3.10GraphsandPlots 45

3.11StatisticalAnalysisandCommonDistributions 47

3.11.1DefinitionofMeasurementData 47

3.11.2StatisticalMeasurements 47

3.11.3StatisticalAnalysisofMeasurements 47

3.11.4Probability 48

3.11.5SampleandPopulation 49

3.11.6FormulationofMeanandVarianceforDirectMeasurements 49

3.11.7MeanandVarianceBasedonSamples 50

3.11.8TheStandardDeviationoftheMean 51

3.12FormulationoftheStandardUncertaintyandAverageofIndirectMeasurements 52

3.12.1HowtoDeterminetheMeasuredValueandRandomError? 52

3.12.2RepeatedMeasurementsofOneSingleQuantity 52

3.12.3NormalDistribution 53

3.12.4Student’s t-distribution 55 MultipleChoiceQuestionsofthisChapter 60

4ErrorsandtheirSources 61 Introduction 61

4.1DefinitionoftheErrorandTheirTypes 61

4.1.1SystematicErrors 62

4.1.2RandomErrors 63

4.1.3ComponentsofMotionErrorAssessment 63

4.2MeasurementCharacteristics 63

4.2.1CharacterizationoftheMeasurement 63

4.2.2Resolution,ErrorUncertainty,andRepeatability 64

4.2.3ModelofMeasurement 67

4.3PropagationofErrors 69

4.4SourcesofErrors 73

4.4.1StaticErrorsandDynamicErrors 73

4.5ErrorBudget 77

4.5.1ComponentsoftheErrorBudget 77

4.5.2ExampleofError-BudgetTable 78

4.6ErrorEliminationTechniques 79

4.6.1Methods 79

4.7ModelofErrorsinCNCUsingHTM 81

4.8CaseStudyofErrorsBudget 87

4.8.1DescriptionoftheDesignedSystem 87

4.8.2ErrorModelingandExperimentalTesting 88

4.9SolvedProblems 96

MultipleChoiceQuestionsofthisChapter 97 References 97

5MeasurementandMeasurementSystems 99

5.1Introduction 99

5.2WhatCanBeStandardinaMeasurement? 101

5.3DefinitionsofKeyMeasurementComponents 102

5.3.1MeasurementSystem 102

5.3.2MeasurementSystemAnalysis 103

5.3.3MeasurementProcess 103

5.4PhysicalMeasurementProcess(PMP) 103

5.5DifferencebetweenNumberandanAnalysisModel 104

5.6MeasurementMethods 105

5.6.1MetrologyandMeasurement 105

5.6.2MetrologicalCharacteristicsofMeasuringInstruments 108

5.7InstrumentationforMeasurement 109

5.7.1Background 109

5.7.2MeasurementInstrumentations 109

5.7.3DigitalMeasuringDeviceFundamentals 109

5.8Non-PortableDimensionalMeasuringDevices 110

5.8.1LaserInterferometry,ApplicationtoCNCMachines 110

5.8.2CoordinateMeasuringMachine(CMM) 118

5.9MetrologyLaboratoryTestforStudents 140

MultipleChoiceQuestionsofthisChapter 146 References 146

6ToleranceStack-UpAnalysis 149

6.1Introduction 149

6.1.1ImportanceofToleranceStack-UpAnalysis 149

6.1.2NeedforToleranceStack-UpAnalysisinAssemblies 151

6.1.3ManufacturingConsiderationsinEngineeringDesign 151

6.1.4TechnicalDrawing 152

6.1.5Definitions,Format,andWorkflowofToleranceStack-Up 153

6.2BriefIntroductiontoGeometricDimensioningandTolerancing(GD&T) 156

6.2.1NotationandProblemFormulation 156

6.2.2DimensionTypes 157

6.2.3CoordinateDimensioning 158

6.2.4ToleranceTypes 160

6.2.5CharacteristicsofFeaturesandTheirTolerances 162

6.3ToleranceFormatandDecimalPlaces 164

6.4ConvertingPlus/MinusDimensionsandTolerancesintoEqual-BilaterallyToleranced Dimensions 165

6.5ToleranceStackAnalysis 167

6.5.1Worst-CaseToleranceAnalysis 169

6.5.2RulesforAssemblyShift 169

6.5.3Worst-CaseToleranceStack-UpinSymmetricDimensionalTolerance 171

6.5.4Worst-CaseToleranceStack-UpinAsymmetricDimensionalTolerance 173

6.6StatisticalToleranceAnalysis 173

6.6.1DefinitionofStatisticalToleranceAnalysis 173

6.6.2Worst-CaseAnalysisvsRSS(Root-SumSquared)StatisticalAnalysis 175

6.6.3Second-OrderToleranceAnalysis 176

6.6.4CasesDiscussions 176

6.6.5UnderstandingMaterialConditionModifiers 178 AppendixAfromISOandASMEY14Symbols 188 MultipleChoiceQuestionsofthisChapter 189 References 189

7InstrumentCalibrationMethods 191

7.1Introduction 191

7.2DefinitionofCalibration 191

7.3NeedforCalibration 192

7.4CharacteristicsofCalibration 193

7.5CalibrationOverallRequirementsandProcedures 195

7.5.1CalibrationMethods/Procedures 195

7.6CalibrationLaboratoryRequirements 197

7.7IndustryPracticesandRegulations 198

7.8CalibrationandLimitationsofaDigitalSystem 199

7.9VerificationandCalibrationofCNCMachineTool 201

7.10InspectionofthePositioningAccuracyofCNCMachineTools 202

7.11CNCMachineErrorAssessmentandCalibration 207

7.12AssessmentoftheContouringintheCNCMachineUsingaKinematicBallbar System 219

7.13Calibrationof3-axisCNCMachineTool 221

7.14CalibrationofaCoordinateMeasuringMachine(CMM) 225

7.14.1CMMPerformanceVerification 225

7.14.2AccreditationofCalibrationLaboratories 226

Section1:ScopeandDescription 231

Section2:CalibrationRequirements 232

Section3:PreliminaryOperations 232

Section4:CalibrationProcess 233

Section5:DataAnalysis 234

Section6:CalibrationReport 234

MultipleChoiceQuestionsofthisChapter 235 References 235

8UncertaintyinMeasurements 237

8.1IntroductionandBackground 237

8.2UncertaintyofMeasurement 238

8.3MeasurementError 238

8.4WhyIsUncertaintyofMeasurementImportant? 239

8.5ComponentsandSourcesofUncertainty 239

8.5.1WhatCausesUncertainty? 239

8.5.2UncertaintyBudgetComponents 240

8.5.3TheErrorsAffectingAccuracy 240

8.6StaticErrorsandDynamicErrors 241

8.7TypesofUncertainty 241

8.8UncertaintyEvaluationsandAnalysis 242

8.9UncertaintyReporting 243

8.10HowtoReportUncertainty 245

8.11FractionalUncertaintyRevisited 247

8.12PropagationofUncertainty 247

MultipleChoiceQuestionsofthisChapter 252 References 252

9DimensionalMeasurementsandCalibration 255

9.1LengthMeasurement 255

9.2DisplacementMeasurement 255

9.3ManualInstruments 260

9.3.1Caliper 260

9.3.2VernierCaliper 261

9.3.3Micrometer 262

9.3.4FeelerGauge 262

9.3.5LinerMeasurementTool 263

9.3.6AmericanWireGauge 263

9.3.7BoreGauge 263

9.3.8TelescopicFeelerGauge 264

9.3.9DepthGauge 265

9.3.10AnglePlateorTool 265

9.3.11FlatPlate 266

9.3.12DialGauge 266

9.3.13OilGaugingTapes 267

9.3.14ThreadMeasurement 267

9.3.15Planimeter 267

9.4DiameterandRoundness 269

9.4.1HowtoMeasureaDiameter? 269

9.4.2Roundness 270

9.5AngularMeasurements 276

x Contents

9.5.1LineStandardAngularMeasuringDevices 277

9.5.2FaceStandardAngularMeasuringDevices 277

9.5.3MeasurementofInclines 279

9.5.4OpticalInstrumentsforAngularMeasurement 280

9.6MetrologyforComplexGeometricFeatures 282

9.6.1EdgeDetectionTechniquesUsingaCCDCamera 282

9.6.2FullLaserScanningforReverseEngineering 283

9.7MeasurementSurfaceTexture 285

9.7.1GeometryofSurface 285

9.7.2SurfaceIntegrity 286

9.7.3SpecificationofSurfaces 286

9.7.4SamplingLength 287

9.7.5InstrumentsandMeasurementofRoughness 290 MultipleChoiceQuestionsofthisChapter 291 References 291

10MechanicalMeasurementsandCalibration 293

10.1ImportanceofMechanicalMeasurements 293

10.2MechanicalMeasurementsandCalibration 293

10.3DescriptionofMechanicalInstruments 294

10.3.1MassMeasurements 294

10.3.2ForceMeasurements 295

10.3.3VibrationMeasurements 295

10.3.4VolumeandDensity 296

10.3.5Hydrometers 298

10.3.6AcousticMeasurements 298

10.4CalibrationofMechanicalInstruments 300

10.4.1WhenIsEquipmentCalibrationNeeded? 300

10.4.2WhenIsThereNoNeedforCalibration? 301

10.4.3ProcessofEquipmentCalibration 301

10.5EquipmentValidationforMeasurement 301

10.5.1IsThereaNeedofEquipmentValidation? 302

10.5.2FeaturesandBenefitsofValidation 302

10.5.3ProcessofValidationofEquipment 302

10.6DifferencebetweenCalibrationandValidationofEquipment 303

10.7DifferencebetweenCalibrationandVerification 303

10.8CalibrationofEachInstrument 304

10.8.1MassCalibration 304

10.8.2ForceCalibration 304

10.8.3PressureCalibration 304

10.8.4VibrationMeasurements 306

10.8.5VolumeandDensity 307

10.8.6Hydrometers 308

10.8.7AcousticMeasurements 308

MultipleChoiceQuestionsofthisChapter 308 References 308

11ThermodynamicMeasurements 309

11.1Background 309

11.2ScaleofTemperature 309

11.2.1IdealGasLaw 310

11.2.2Vacuum 310

11.2.3GasConstants 310

11.3Power 312

11.4Enthalpy 312

11.5HumidityMeasurements 312

11.6MethodsofMeasuringTemperature 313

11.7TemperatureMeasuredthroughThermalExpansionMaterials 314

11.7.1Liquid-in-GlassThermometer 314

11.7.2BimetallicThermometer 314

11.7.3ElectricalResistanceThermometry 315

11.7.4ResistanceTemperatureDetectors 316

11.7.5ExamplesforDiscussion 318

11.7.6Thermistors 320

11.8ThermoelectricTemperatureMeasurementorThermocouples 321

11.8.1BasicThermocouples 321

11.8.2FundamentalThermocoupleLaws 322

11.9ThermocoupleMaterials 323

11.9.1AdvantagesandDisadvantagesofThermocoupleMaterials 324

11.9.2ThermocoupleVoltageMeasurement 325

11.10Multi-JunctionThermocoupleCircuits 326

11.11Thermopiles 327

11.12RadiativeTemperatureMeasurement 327 MultipleChoiceQuestionsofthisChapter 329 References 329

12QualitySystemsandStandards 331

12.1IntroductiontoQualityManagement 331

12.2QualityManagement 332

12.2.1TotalQualityManagement(TQM) 332

12.2.2QualityManagementSystem(QMS) 333

12.2.3TQMIsEssentialtoCompleteTQS 333

12.2.4ISO-BasedQMSCertification 333

12.3ComponentsofQualityManagement 334

12.3.1QualitySystem(QS) 334

12.3.2QualityAssurance(QA) 335

12.3.3QualityControl(QC) 335

12.3.4QualityAssessment 335

12.4SystemComponents 336

12.4.1QualityAudits 336

12.4.2PreventiveandCorrectiveAction 336

12.4.3OccupationalSafetyRequirements 337

12.4.4HousekeepingPractices 338

12.5QualityStandardsandGuides 338

MultipleChoiceQuestionsofthisChapter 339

References 340

13DigitalMetrologySetupsandIndustryRevolutionI4.0 341

13.1Introduction 341

13.1.1WhatIsaDigitalMeasurement? 341

13.1.2MetrologyandDigitalization 341

13.1.3ImplementationStrategy 343

13.2DataAcquisition 343

13.3SetupFundamentalsforMeasurementandDataAcquisition 344

13.3.1LengthMeasurementinOpenLoop 344

13.3.2ThermalMeasurementandData-AcquisitionConsiderations 345

13.3.3DataTransfertoCloud 349

13.3.4InternetofThings(IoT)Metrology 349

13.3.5Closed-LoopDataAnalysis-(In-ProcessInspection) 350

13.4DigitalTwinMetrologyInspection 352

MultipleChoiceQuestionsofthisChapter 354

References 354

Index 357

Preface

Thisbookisconceivedforengineersandtechniciansoperatinginvariousindustrialfields.Itisalso forstudentsofmechanical,production,andotherrelateddisciplinesinengineeringtofacilitate understandingoffundamentalsofmeasurements,instrumentsandgoverningrulesfollowedby learningvariousshop-floorrequiredmeasurementtechniques.

Thebookintroducesbasicneedsfrommath,statistics,andmeasurementprinciples.Itdiscusses errorsandtheirsourcesinmanufacturingwhiledescribingthevariousmeasurementinstruments. Simplephysicalparameterssuchasforce,torque,strain,temperature,andpressureareexplained. Thesubsequentchapterscovertolerancestack-ups,GD&T,calibrationprinciplesinvariousaspects ofmanufacturing,andqualitystandards.ASMEandISOarecitedaccordingtoneedsandtocorrespondingknowledgethroughoutthebook.EachchapterendswithasetofMCQswithanswer tablestohelppreparetechniciansandengineersforvariousqualificationdiplomasandcertificates. Thebookadoptsanillustrativeapproachtoexplaintheconceptswithsolvedexamplestosupport understanding.

Chapter1ofthebookintroducesthefundamentalunitsandconstantsneededinmetrologysupportedbytheinternationalvocabularyofmetrologyandinternationalstandards.

Chapter2emphasizesmetrologythatcoversallscales,startingfromnanoscaletolargescale.Differencesandrelationshipsbetweenscalesareintroducedtounderstandthedifferencesandpossible complementarity,whileChapter3introducesbasicmathandsciencebackgroundmainlytorefresh memoriesandbeareferenceincasethereisaneedtocheckinformation.Mathandscienceareof greatimportancewhendealingwithmeasurementsincetheinceptionofhumanity.

Chapter4definestheerroranditsvariouspossiblesources:howerrorpropagatesinmeasurement,errorsassociatedwithmotion,errorclassification,anderrorelimination.Anestimationof error,oruncertaintyanalysis,isatoolfordeterminingtheperformancecapabilityofmachinetools andhighlightingpotentialareasforperformanceandcostimprovement.

InChapter5,themeasurementandquantificationarethefundamentalconceptsofmetrology, includingthemeasurementsystemcharacteristics.Thisconsidersexplicitandinternationally accepteddefinitions,principles,andstandards.Thepurposeofanymeasurementsystemisto providetheuserwithanumericalvaluecorrespondingtothevariablebeingmeasuredbythe system.Whataretheinternationalrelatedstandards?Examplesoflengthmeasurement,parts, andmachineinspectionwithreverseengineeringareprovided.

OneofthemostsignificantchaptersisChapter6asitintroducesthetolerancestacksanalysismethods.Thischapterestablishesuniformpracticesforstatingandinterpretingdimensioning, tolerancing,andrelatedrequirementsforuseonengineeringdrawingsandinrelateddocuments underASMEY14.5.1.Abriefintroductiontogeometricdimensionandtolerancingisfollowedby

tolerancestacks.Thisistoassigntherighttolerancesandtomakesurethatnounnecessarytight toleranceisselected,leadingtocostlymanufacturing.

Chapter7introducestheprinciplesandfundamentalsofcalibrationundertheinternationalstandardsdefinitionsandagreements.Ittacklesrealcalibrationofmachinesandinstrumentsindetail forunderstandingoftheprocess.

Chapter8discussestheuncertaintybasedontheinternationalstandardsandrecentdevelopmentsfollowedbythepropagationoferrorwithreal-worldexamples.Thedoubtsurroundingthis measurementistheuncertaintyofmeasurement.Thebackgroundandfundamentaldefinitionof uncertaintyanderrorwillbediscussedlaterbasedoninternationalstandardswithallaspectsin generalpractice.

Mechanicalmeasurementforlengthandothersarediscussedintwochapters.

Chapter9coverssomeoftheinstrumentsusedfordisplacementandlengthmeasurements.From lengthmeasurementandcalibrationofinstrumentssuchasmicrometers,calipers,gages,ortape measures,tohigh-techoptics-basedscalesandcomparators.Theindustrialleadingdimensional instrumentcalibrationcapabilitiesareavailableandwelldesignedtoreduceriskandinaccuracy inmeasurements.Chapter10coversmechanicalinstrumentsmeasuringotherthanlengthmeasurands.Thechapterdiscussescalibration-relatedtechniques.Thesearefundamentalbasisinstrumentsthatmaybeneededbyanyengineeratanytime.

ThermodynamicpropertiesofanymaterialorsolutionaretreatedinChapter11.Theyarevaluablenotonlyforestimatingtheusefulnessofthematerialorthefeasibilityofreactionsinsolution, buttheyalsoprovideoneofthebestmethodsforinvestigatingtheoreticalaspectsrelatedtothe materialorsolutionstructure.Thermalpropertiesofmaterialscanbemeasureddirectlyorindirectly.Thisincludestemperature,developedpressure,calorimetry,andthermalconductivity.

Chapter12coversqualitymanagementandmetrologysincetheyareimportantcomponentsin metrologylabsandmanufacturingenterprises.Thischapterintroducesthedefinitionofmostcomponentsofqualitywiththerelatedinternationalstandardswithanoverallorganizationofthelab requirement.

ContemporarydigitalmetrologyisdiscussedinChapter13.Digitalmetrologyanditsrelationship tomanufacturingandI4.0areintroduced.Thischaptercoversthedigitalization,automation,and measurementsthatarebecomingextremelyimportantinthiseraofdigitalmanufacturinganddigitaltwinsmetrology(DTM).Themeasurementsystemisacombinationofreal-timecontrolsystem andsystemfordatatransmission.Digitalcomputingisthetoolfordataprocessing.Thetechnology readinessformostmeasurementinstrumentationexiststogetherwithvirtualinstrumentscapable ofbuildingfurthertheDTM.Sinceseveralappsforsmartphoneshavebeendeveloped,thelast appendixgivesashortpresentationof38apps.

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ThisbookhasanonlineappendicesextensioncoveringsmartphoneAppsrelatedtovariousmetrologyaspectsdiscussedinthebookandfoundinAppendixA,andatechnicaltermsglossaryin AppendixB.Thelinkiswww.wiley.com\go\mekid\metrologyandinstrumentation.

Acknowledgments

Thisbookislikeavesseloftimeandknowledgesincemuchofithasbeendedicatedtocompiling informationanddata,verifyingandcheckingnumerousexperiments,andensuringthatknowledge isdeliveredinasimplemannerthatcanbeeasilycapturedbyreaders.

Severalspecialistcompaniesintheareaofmetrologyandmanufacturinghavecontributed directlyorindirectlytothisbook;hence,Iamverythankfultoallofthem.

IacknowledgethecourtesyofFotofab(Chicago,USA),Leica(UK),andRenishaw(UK)touse someoftheirmaterials.

IamthankfultoOtilaPrianandNinaFernandezfromCREAFORM(AMETEK)fortheirreverse engineeringsamples;RossSnyder,ApplicationEngineerfromSigmetrix(Michigan,USA)forhis stack-upanalysiscontribution.IwouldalsoliketothankMr.NicolausSpinnerfromSPINNER WerkzeugmaschinenfabrikGmbHinSauerlach(Germany)forprovidingmewiththecalibration resultsofhismachines.

MythanksareextendedtomyManagingEditors:GabriellaRoblesandSarahLemorefromJohn Wiley&Sons,Inc.

IwouldalsoliketoacknowledgemyMScstudentUsmanKhanandourdepartmentalsecretary MinoThankachanforthehardworkofformattingthechapters.NottoforgetAbderrahmanMekid andKhawlaMekidfortheireditingandrevisions.

TheauthorwouldliketoacknowledgethesupportofKingFahdUniversityofPetroleumand Minerals(KFUPM)throughtheDeanshipofResearchOversightandCoordination(DROC)for theirsupportinresearchandresourcesmadeavailabletothisbookunderBW#191006.

October1,2021

AbouttheAuthor

SamirMekidisprofessorofmechanicalengineeringatKFUPMandcharteredengineerregistered withIMechE(UK)andASMEmember.PriortojoiningKFUPM,hewasassistantprofessorat UMIST(UK)andTheUniversityofManchester(UK).HehasworkedwithCaterpillarinthedesign departmentandhasbeenanexpertEUevaluatorforvariouscountriestoseveralEuropeanFrameworkProjectsPrograms,e.g.,FP6,FP7.HewasmemberoftheScientificAdvisoryBoardofthe CentreofExcellenceinMetrologyforMicroandNanotechnology(CEMMNT)intheUK.His areaofresearchincludesmachinedesign,manufacturinginstrumentation,metrology,mechatronics,smartmaterials,andsensorsdesign.Hehaspublishedover180publicationsinprofessional journalsandinternationalconferenceproceedingsandeditedthreebooks.Heholdsmorethan 30patents.

Duringhisongoingcareer,hetaughtseveralcoursesforundergraduateandgraduatestudents including:metrology,sensorsandactuators,togetherwithmachinedesign.Hehastrainedapproximatelyonehundredengineersthroughshortcoursesontolerancestack-ups,GD&T,manufacturingsystems,andmaterialsselection.HeiscurrentlytheFoundingDirectoroftheInterdisciplinary ResearchCenterforIntelligentManufacturingandRoboticsatKFUPM.

FundamentalUnitsandConstantsinMetrology

“Whenyoucanmeasurewhatyouarespeakingaboutandexpressitinnumbers,youknow somethingaboutit.”

—LordKelvin(1883).Source:PublicDomain.

1.1Introduction

Metrologyisthescienceofmeasurementwithvariousapplications.ItisderivedfromtheGreek words metro –measurementand Logy –science.TheBIMP(BureauofWeightsandMeasuresin France)definesmetrologyas“thescienceofmeasurementembracingbothexperimentalandtheoreticaldeterminationsatanylevelofuncertaintyinanyfieldofscienceandtechnology.”

Fivepivotsdefinethefunctionsofmetrology:

1)Toestablishtheunitsofmeasurements;

2)Toreplicatetheseunitsasstandards;

3)Toguaranteethemeasurementuniformity; 4)Todevelopmeasurementmethods;

5)Toinvestigatetheaccuracyofmethods-relatederrors.

Basedonthis,theobjectivesofmetrologyare:

1)Selectionofpropermeasuringinstrument; 2)Propermeasuringstandards; 3)Minimizinginspectioncost; 4)Definingprocesscapabilities; 5)Standardization;

6)Maintainingaccuracyandprecisionduringinspectionorascomponentofaninstrumentover timeofuse[1].

Therefore,twotypesofmetrologyexist:

1)Deterministic,orindustrial,metrology. 2)Legal,orscientific,metrology.

Measurementistheprocessofrevealingasingleormultiplevaluestothecharacteristicsofan objectorpropertybyconductingexperimentstodeterminethevalueofthisparticularproperty. Thesepropertiesmaybephysical,mechanical,orchemical,suchaslength,weight,force,strain, volume,angle,andmolls.

Object to measure

Measurand?

Measurement procedure?

Identify related

Principle

Method

System

Uncertainty?

Measurement results

Principle of measurementtechniques

Metrologyalsoincludesprecision,repeatability,andaccuracy,whichreferstohowaccurate themeasuredvalueis.Itestablishesawell-knownunderstandingofthemeasuringprocess andtherelatedunitsthatarecriticalinconnectingvarioushumanactivitiesandensuresthat thesemeasurementsarelinkedtoreferencestandards,whichiscommonlyreferredtoastraceability.Foraslongascivilizationhasexisted,measurementshavebeentaken.Itisnecessaryfor acountry’seconomicandsocialdevelopment.Itprovidesprecisemeasurementsthathavean impactontheeconomy,health,safety,andgeneralwell-being.Itcouldalsobealegalproblem. Asaresult,thetopicisalwaysindemand.

Thischapterwillintroducethefundamentalunitsandconstantsinmetrologythroughconversionsbetweenunitsandsystems.Toputmeasurementsintocontext,acompletemethodologyof theactofmeasurementbeginningwiththeobjecttomeasureandendingwiththeresultthatconstitutestheinformationneededfortheobjectisrequired.Thecompleteprocessissummarizedin Figure1.1.Thefiguredepictsasimplifiedmethodologyforproducingmeasurementresultswith minimalconditionssuchastheunitstobeknown,thecalibrationofthemeasurementinstruments, andtheuncertaintyofsuchmeasurements.Thisistocastthemajorityoftheaspectsthatengineers conductingmeasurementsmustbeawareof.Adimensionisanon-numericalmeasureofaphysical variable.Theunitisusedtoassociateaquantityormeasurementwithadimension.

Example1.1

Themassofanobjectisaprimarydimension,while15kgisassociatedwiththe quantity15ofmasswiththeunitofkg.Weneedacomparisonwithsomepreciseunitvalueto measurethequantityofanything.Bodyparts(Figure1.2)andnaturalsurroundingswereusedby earlyhumanstoprovidesuitablemeasuringinstruments.Elementarymeasuresbecameessential intheprimitivehumansocietiesfortaskssuchasbuildingdwellings,makingclothing,bartering forfood,andexchangingrawmaterials.

Figure1.1 Simplifiedmethodologyproducingmeasurementresults.

Figure1.2 VitruvianmanbyLeonardodaVincishowingninehistoricalunitsofmeasurement.

Source: WikimediaCommons

–AccordingtoearlyBabylonianandEgyptiantranscripts,lengthwasfirstmeasuredwiththeforearm(cubit),hand(palmandspan),andfinger(digit).

–Thecyclesofthecelestialbodiessuchasthesun,moon,andotherswereusedfortimemeasurements.

–Plantseedswereusedforthesakeofestablishingvolumemeasurement,whilewiththeexpansionofscalesforweighing,seedsandstonesbecamestandards.Assample,thecarobseedwas thebasemeasureforthecarat,whichisstillusedasamassunitinthegemstoneindustry.

Astradeandcommerceexpanded,itbecamenecessarytostandardizemeasurementsystems acrossmanycountries.Thisdecreasedthepossibilityofdisagreementsarisingfrommeasurement systemmisunderstandings.

Theinternationalsystemofunits,knownastheSI(fromFrench“SystèmeInternational”)unit system,distinguishesphysicalunitsintotwoclassesasshownbelow:

1)Baseorprimaryunits;and 2)Derivedunits.

Thesetwocategoriescoverthemostcommonlyusedunits,suchastime,temperature,length, mass,pressure,andflowrate.TheNationalInstituteofStandardsandTechnology(NIST)[2]introducedtheSIunits,whichcanbefoundatthishyperlink: SIunits (https://physics.nist.gov/cuu/ Units/).FormoreinformationontheSIunits,visitthewebsiteoftheinternationalstandardsorganizationknownastheBureauInternationaldesPoidsetMesures(BIPM).

Flemish Ell Cubit
Feet

Table1.1 Primaryunits.

MeasurementUnitsSymbolDescription

UnitoflengthmetermOnemeterisequaltothelengthofthepathtravelledbylight invacuumduringatimeintervalof1/299792458ofasecond.

UnitofmasskilogramkgOnekilogramisequaltotheunitofmasspresentedbythe internationalprototypeofthekilograminFigure1.2.Since 2019,thenewdefinitionbasedonPlanck’sconstanthas beenused.

UnitoftimesecondsOnesecondisequaltothedurationof9192631770periodsof theradiationcorrespondingtothetransitionbetweenthetwo hyperfinelevelsofthegroundstateofthecesium-133atom.

UnitofelectriccurrentampereAOneampereisdefinedasfollows:theconstantcurrentif maintainedintwostraightparallelconductorsofinfinite length,ofnegligiblecircularcross-section,andplaced1meter apartinvacuum,willproducebetweentheseconductorsa forceequalto2 × 10 7 newtonpermeteroflength.

Unitofthermodynamic temperature kelvinKOnekelvinisthefraction1/273.16ofthethermodynamic temperatureofthetriplepointofwater.

Unitofamountof substance molemolOnemoleistheamountofsubstanceofasystemcontaining asmanyelementaryentitiesasthereareatomsin0.012 kilogramofcarbon-12.

Whenthemoleisused,theelementaryentitiesmustbe specifiedandmaybeatoms,molecules,ions,electrons,other particles,orspecifiedgroupsofsuchparticles.

Unitofluminous intensity candelacdOnecandelaistheluminousintensitywithinonedirection,of asourcethatemitsmonochromaticradiationoffrequency 540 × 1012hertzandhavingaradiantintensityof1/683watt persteradianinthatdirection.

Aswillbedemonstratedlater,eachmeasurementunithasaprimaryquantitythatisusedby convention.Eachprimaryquantityhasonlyoneprimaryunit.Asaresult,everyprimaryunitcan bedecomposedorrecomposedfurther.Table1.1showsprimaryunitsofdifferentkindsofphysical quantities,symbols,andtheirdescriptions.Figure1.3depictsthekilogramprototypesafelyconservedinParisasareferenceunitofkgkeptconstantinquantityforcomparison.Thefollowing sectiondiscussesderivedunits,whichareshowninTable1.2.

Figure1.3 Thestandardkilogramformass.

Table1.2 Derivedunits.

DerivedquantitySiderivednewunitSymbolSIunitsSIbaseunits

ForcenewtonNmkgs

PowerwattWJ/sm2

ElectricchargecoulombCsA

ElectromotiveforcevoltVm2

ElectriccapacitancefaradFC/Vm

Electricresistanceohm

ElectricconductancesiemensSA/Vm

Velocitymeterpersecondm/s

Angularvelocityradianpersecond1/s

Massflowratekilogrampersecondkg/s

Flowrateliterpersecondl/s

Figure1.4 Theplatinum-iridiummeterbarreference. Source: WikimediaCommons

1FundamentalUnitsandConstantsinMetrology

TheInternationalPrototypeMeterbar,showninFigure1.4,ismadeof90%platinumand 10%iridiumalloyandservedastheSI(metricsystem)standardoflengthfrom1889until1960, whentheSIsystemswitchedtoanewdefinitionoflengthbasedonthewavelengthoflightemitted bykrypton-86.Thepracticallengthofthemeterwasdefinedbythedistancebetweentwofinelines ruledonthecentralribofthebarneartheendsmeasuredatthefreezingtemperatureofwater.

ThebarwasgivenanX(Tresca)cross-sectionalshapetoincreaseitsstiffness-to-weightratioand improveitsthermalaccommodationtimesothegraduationlinescouldbelocatedonthe“neutral” axisofthebarwherethechangeinlengthwithflexureisminimum.Theprototypewasmadein 1889,itslengthmadeequaltothepreviousFrenchstandard“MeteroftheArchives.”Atthesame time,twenty-nineidenticalcopiesweremade,whichwerecalibratedagainsttheprototypeand distributedtonationstoserveasnationalstandardsandpossiblyforcomparisonafterafewyears.

1.2CurrentDefinitionsoftheMainSIUnits

ThecurrentdefinitionofthebaseandprimaryunitsareshowninTable1.1.

1.3NewDefinitionofSevenBaseUnitsoftheSI

SevenbaseunitsoftheSIareknowntobethesecond,meter,kilogram,ampere,kelvin,mole,and candela.Somehavebeenbasedonphysicalconstantsforalongtime.Since1983,themeterhas beendefinedasthelengthofthepathtraveledbylightinvacuumoveratimeintervalof1/299 792458s.However,thefourthatmetrologistshaveagreedtoredefinerecentlywerepreviously basedonsomething—i.e.,anobject,experiment,orphenomenon—implyingthattheirvalueis notuniversal.

Asaresultofthisdecision[3],allsevenSIunitsarecurrentlydefinedintermsofphysicalconstants.

Themeter,symbolm,istheSIunitoflength.Itisdefinedbytakingthefixednumericalvalue ofthespeedoflightinvacuum, c,tobe299792458whenexpressedintheunitm•s 1 ,wherethe secondisdefinedintermsofthecesiumfrequency Δ�� Cs .Themetermaybeexpresseddirectlyin termsofthedefiningconstants(Eq.(1.1)):

1m = 9192631770 299792458 c Δ

Previously,onemeterwasdefinedasthelengthtraveledbylightin3.335641 × 10 9 s(basedon thespeedoflightinavacuum).Itwasalsodefinedas1,650,763.73wavelengthsinvacuumofthe orangeredlineofthespectrumofkrypton-86.

Mostaffectedisthekilogram,whichiscurrentlyfixedbya143-year-oldplatinumalloycylinder knownasthe“LeGrandK”andkeptattheInternationalBureauofWeightsandMeasures(BIPM) inParis.ThekilogramisnowdefinedbyPlanck’sconstant, h,recentlymeasuredwithextraordinary precision.Itsagreedvalueissetat6.62607015 × 10 34 kgm2 s 1 whenexpressedintheunitJs, whichisequaltokgm2 s 1 ,themeterandsecondbeingdefinedintermsofcand Δν.Thismeans thatthekilogramisdefinedintermsofPlanck’sconstantinsteadofthemassofacylinderofmetal calledInternationalPrototypeKilogram.

Meanwhile,theampereisdeterminedbytheelementaryelectriccharge,e,whichisgivenas 1.602176634 × 10 19 whenexpressedincoulombs.Thekelvinisdeterminedbythefixednumerical valueofBoltzmann’sconstant,k,whichis1.380649 × 10 23 whenexpressedinunitsofJK 1 ,and themoleisdeterminedbyAvogadro’sconstant(N A ),whichcontainsexactly6.02214076 × 1023

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