INTERNATIONAL JOURNAL ON ORANGE TECHNOLOGY https://journals.researchparks.org/index.php/IJOT
e-ISSN: 2615-8140 | p-ISSN: 2615-7071
Volume: 4 Issue: 6 |Jun 2022
Influence of Temperature and Duration of the Process on the Degree of Nickel Extraction Bekhzod Farmanov Ilkhomovich Senior Teacher of the Karshi Engineering and Economics Institute, Uzbekistan Tavashov Shakhzod Khujaxmatovich Assistant of the Karshi Engineering and Economics Institute, Uzbekistan --------------------------------------------------------------***-------------------------------------------------------------
Annotation: To date, in the global industry, special attention is paid to the synthesis of high-strength, with low hydraulic resistance, improved geometric and increased specific surface area of catalyst granules. In this aspect, an important task is to develop a technology for the production of our own highly efficient and durable catalysts based on the processing of spent industrial catalysts. To do this, it is necessary to substantiate a number of scientific solutions, including in the following areas: development of nickel extraction technology from spent industrial catalysts of the GIAP-8 series, technology for obtaining high-strength aluminum oxide carriers and scientific bases for obtaining a nickel-containing catalyst on an aluminum oxide carrier. Keywords: spent nickel-containing catalyst GIAP-8, nitric acid, degree of extraction, temperature, concentration, time. Studies of the effect of the extraction process temperature and duration on the degree of nickel extraction from the spent nickel-containing catalyst GIAP-8 were carried out using 30% nitric acid at a rate of 100% of stoichiometry. The effect of the norm of 30% nitric acid on the degree of nickel extraction was studied at a temperature of 30 ℃ and the duration of the process was 4 hours with constant stirring. The results obtained are shown in Table 1. Table 1. Wagging of the norm of 30% nitric acid on the chemical composition of the liquid phase and the degree of nickel extraction from the spent catalyst GIAP – 8 at a temperature of 30 ℃. № 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 © 2022, IJOT
Standard HNO3, % 80 80 80 90 90 90 100 100 100 110 110 110 120 120 120 |
S:L 1:0,30 1:0,30 1:0,29 1:0,34 1:0,34 1:0,32 1:0,37 1:0,37 1:0,36 1:0,41 1:0,41 1:0,39 1:0,45 1:0,45 1:0,43
Chemical composition, mass. % NiO Nnitr. HNO3 16,76 7,69 16,99 7,40 17,14 7,50 15,74 6,40 15,76 6,39 15,72 6,71 14,56 5,72 14,65 5,59 14,72 5,71 13,46 5,28 13,65 5,25 13,49 5,31 13,65 2,63 13,67 2,61 13,75 2,64
Research Parks Publishing (IDEAS Lab) www.researchparks.org
Degree of extraction, % 74,56 75,52 75,43 78,82 78,86 77,97 81,05 81,49 81,25 81,49 82,51 82,49 91,28 91,35 91,30 |
Page 6
Copyright (c) 2022 Author (s). This is an open-access article distributed under the terms of Creative Commons Attribution License (CC BY).To view a copy of this license, visit https://creativecommons.org/licenses/by/4.0/