Anexo x

Page 36

9770 ROUTE TRANSCANADIENNE ST. LAURENT, QUEBEC CANADA H4S 1V9 TEL (514)337-1000 FAX (514)333-3046 http://www.agatlabs.com

Quality Assurance CLIENT NAME: C.A.R.U

AGAT WORK ORDER: 11M532404

PROJECT NO:

ATTENTION TO: ALEJANDRO ARCELUS

SAMPLED BY:

SAMPLING SITE:UPM

Water Analysis RPT Date: 2012-02-16

PARAMETER

DUPLICATE Sample Id

Batch

Dup #1

Dup #2

REFERENCE MATERIAL RPD

Method Blank

Measure d Value

Acceptable Limits

METHOD BLANK Recovery

Acceptable Limits

MATRIX SPIKE Recovery

Acceptable Limits

Lower Upper

Lower Upper

Lower Upper

70% 130%

101%

70% 130%

Chlorate Chlorate

1

2723839

< 0.02

< 0.02

0.0%

< 0.02

105%

70% 130%

Inorganics Ammonia Total Kjeldahl Nitrogen Conductivity Chemical Oxygen Demand Total Mercury

1 1 1 1 1

NA NA 2738384 NA NA

NA NA 4010 NA NA

NA NA 4000 NA NA

0.0% 0.0% 0.2% 0.0% 0.0%

< 0.067 < 1.0 < 10 <5 < 0.0001

102% 94% 102% 93% 116%

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

87% 106% 106% 103% 107%

80% 80% 80% 90% 90%

120% 120% 120% 110% 110%

NA NA NA NA 105%

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

Nitrite plus Nitrate Total Phosphorous Total Suspended Solids Total Solids Sulphide

1 1 1 1 1

NA NA NA NA NA

NA NA NA NA NA

NA NA NA NA NA

0.0% 0.0% 0.0% 0.0% 0.0%

< 0.067 < 0.02 <2 < 25 < 0.02

116% 91% 95% NA 82%

80% 80% 50% 80% 80%

120% 120% 150% 120% 120%

101% 91% NA NA 104%

80% 120% 80% 120% 0% 0% 0% 0% 80% 120%

101% 99% NA NA 88%

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

Metals Calcium Magnesium Sodium Potassium Silicon

929 929 929 929 929

NA NA NA NA NA

NA NA NA NA NA

NA NA NA NA NA

0.0% 0.0% 0.0% 0.0% 0.0%

<2 <2 <2 <1 <2

91% 88% 86% 89% NA

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

98% 97% 95% 96% 117%

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

104% 103% 104% 103% NA

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

Chromium Copper Zinc Cadmium Nickel

929 929 929 929 929

NA NA NA NA NA

NA NA NA NA NA

NA NA NA NA NA

0.0% 0.0% 0.0% 0.0% 0.0%

< 0.01 < 0.003 < 0.003 < 0.0008 < 0.002

92% 101% 98% 101% 105%

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

101% 90% 88% 89% 94%

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

NA NA 85% 114% 81%

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

Lead Iron Selenium Arsenic Manganese

929 929 929 929 929

NA NA NA NA NA

NA NA NA NA NA

NA NA NA NA NA

0.0% 0.0% 0.0% 0.0% 0.0%

< 0.001 < 0.3 < 0.002 < 0.001 < 0.005

99% 120% 103% 99% NA

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

92% 104% 90% 93% 104%

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

NA 82% NA 101% NA

80% 80% 80% 80% 80%

120% 120% 120% 120% 120%

Boron

929

NA

NA

NA

0.0%

< 0.06

119%

80% 120%

93%

80% 120%

102%

80% 120%

Certified By: AGAT Laboratories’ procedure for signatures and signatories adheres strictly to the requirements of accreditation ISO 17025:2005 as required by CALA, SCC and MDDEP where applicable. All electronic signatures on AGAT certificates are password protected and all signatories meet their regional and scope of accreditation requirements and are approved by CALA, SCC and MDDEP.

QUALITY ASSURANCE REPORT

Page 8 of 9

This version replaces and cancels all previous versions, if applicable. Reproduction of this document is prohibited, in whole or part, unless authorised in writing by the laboratory. The results relate only to the samples analyzed


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