Appendix K: Laboratory Results
G0038:JJS:53217 Grafton DSI
May 2015
ABN – 50 005 085 521
e.mail : EnviroSales@eurofins.com.au
web : www.eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh Vic 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Sample Receipt Advice Company name:
Prensa QLD&WA
Contact name: Project name: Project ID: COC number: Turn around time: Date/Time received: Eurofins | mgt reference:
Jason Scott DSI 53217 Not provided 5 Day Apr 10, 2015 3:30 PM 453692
Sample information 䖵
A detailed list of analytes logged into our LIMS, is included in the attached summary table.
䖵
All samples have been received as described on the above COC.
䖵
COC has been completed correctly.
䖵
Attempt to chill was evident.
䖵
Appropriately preserved sample containers have been used.
䖵
All samples were received in good condition.
䖵
Samples have been provided with adequate time to commence analysis in accordance with the relevant holding times.
䖵
Appropriate sample containers have been used.
䖵
Sample containers for volatile analysis received with zero headspace.
䖶
Some samples have been subcontracted.
㻺㻛㻭
Custody Seals intact (if used).
Contact notes If you have any questions with respect to these samples please contact: Sarah Gould on Phone : (+61) (8) 8154 3100 or by e.mail: SarahGould@eurofins.com.au Results will be delivered electronically via e.mail to Jason Scott - jason.scott@prensa.com.au.
Environmental Laboratory Air Analysis Water Analysis Soil Contamination Analysis
NATA Accreditation Stack Emission Sampling & Analysis Trade Waste Sampling & Analysis Groundwater Sampling & Analysis
38 Years of Environmental Analysis & Experience
ABN – 50 005 085 521
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
. Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
Order No.: Report #: Phone: Fax:
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory Sample ID
Sample Date
Sampling Time
Matrix
LAB ID
53217BH1_0.15
Apr 09, 2015
3:00PM
Soil
B15-Ap07631
53217BH1_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07632
53217BH2_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07633
53217BH2_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07634
53217BH3_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07635
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH3_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07636
53217BH4_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07637
53217BH4_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07638
53217BH5_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07639
53217BH5_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07640
53217BH6_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07641
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH6_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07642
53217BH7_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07643
53217BH7_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07644
53217BH8_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07645
53217BH8_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07646
53217BH9_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07647
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH9_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07648
53217BH10_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07649
53217BH10_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07650
53217BH11_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07651
53217BH11_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07652
53217TB1_080415
Apr 08, 2015
Water
B15-Ap07653
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217FB1_080415
Apr 08, 2015
Water
B15-Ap07654
53217R1_080415
Apr 08, 2015
Water
B15-Ap07655
53217FB2_090415
Apr 09, 2015
3:00PM
Water
B15-Ap07656
53217R2_090415
Apr 09, 2015
3:00PM
Water
B15-Ap07657
53217BH1_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07658
53217BH1_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07659
X X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould
Soil
B15-Ap07660
53217BH1_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07661
53217BH1_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07662
53217MW1_4.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07663
53217MW1_5.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07664
53217MW1_6.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07665
X X X X X X
Cation Exchange Capacity
3:00PM
Moisture Set
Apr 09, 2015
BTEX and Naphthalene
53217BH1_1.3
X
Eurofins | mgt Suite 7
X
Eurofins | mgt Suite 10
X
External Laboratory
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould
Soil
B15-Ap07666
53217MW1_8.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07667
53217MW1_9.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07668
53217BH2_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07669
53217BH2_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07670
53217BH2_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07671
X X X X X X
Cation Exchange Capacity
3:00PM
Moisture Set
Apr 09, 2015
BTEX and Naphthalene
53217MW1_7.0
X
Eurofins | mgt Suite 7
X
Eurofins | mgt Suite 10
X
External Laboratory
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould
Soil
B15-Ap07672
53217BH3_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07673
53217BH3_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07674
53217BH3_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07675
53217BH3_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07676
53217MW2_4.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07677
X X X X X X
Cation Exchange Capacity
3:00PM
Moisture Set
Apr 09, 2015
BTEX and Naphthalene
53217BH2_3.0
X
Eurofins | mgt Suite 7
X
Eurofins | mgt Suite 10
X
External Laboratory
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould
Soil
B15-Ap07678
53217MW2_6.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07679
53217MW2_7.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07680
53217MW2_8.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07681
53217BH4_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07682
53217BH4_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07683
X X X X X X
Cation Exchange Capacity
3:00PM
Moisture Set
Apr 09, 2015
BTEX and Naphthalene
53217MW2_5.0
X
Eurofins | mgt Suite 7
X
Eurofins | mgt Suite 10
X
External Laboratory
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould
Soil
B15-Ap07684
53217BH4_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07685
53217BH5_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07686
53217BH5_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07687
53217BH5_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07688
53217BH5_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07689
X X X X X X
Cation Exchange Capacity
3:00PM
Moisture Set
Apr 09, 2015
BTEX and Naphthalene
53217BH4_2.0
X
Eurofins | mgt Suite 7
X
Eurofins | mgt Suite 10
X
External Laboratory
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould
Soil
B15-Ap07690
53217BH6_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07691
53217BH6_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07692
53217BH6_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07693
53217BH7_0.15
Apr 09, 2015
3:00PM
Soil
B15-Ap07694
53217BH7_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07695
X X X X X X
Cation Exchange Capacity
3:00PM
Moisture Set
Apr 09, 2015
BTEX and Naphthalene
53217BH6_1.0
X
Eurofins | mgt Suite 7
X
Eurofins | mgt Suite 10
X
External Laboratory
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould
Soil
B15-Ap07696
53217BH7_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07697
53217BH8_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07698
53217BH8_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07699
53217BH8_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07700
53217BH8_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07701
X X X X X X
Cation Exchange Capacity
3:00PM
Moisture Set
Apr 09, 2015
BTEX and Naphthalene
53217BH7_2.0
X
Eurofins | mgt Suite 7
X
Eurofins | mgt Suite 10
X
External Laboratory
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould
Soil
B15-Ap07702
53217MW3_7.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07703
53217MW3_8.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07704
53217BH9_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07705
53217BH9_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07706
53217BH9_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07707
X X X X X X
Cation Exchange Capacity
3:00PM
Moisture Set
Apr 09, 2015
BTEX and Naphthalene
53217MW3_6.0
X
Eurofins | mgt Suite 7
X
Eurofins | mgt Suite 10
X
External Laboratory
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould
Soil
B15-Ap07708
53217BH10_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07709
53217BH10_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07710
53217BH10_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07711
53217BH11_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07712
53217BH11_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07713
X X X X X X
Cation Exchange Capacity
3:00PM
Moisture Set
Apr 09, 2015
BTEX and Naphthalene
53217BH10_0.1
X
Eurofins | mgt Suite 7
X
Eurofins | mgt Suite 10
X
External Laboratory
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
ABN – 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 7
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH11_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07714
53217QC1_080415
Apr 08, 2015
3:00PM
Soil
B15-Ap07715
53217QC5_090415
Apr 09, 2015
3:00PM
Soil
B15-Ap07716
53217QC7_090415
Apr 09, 2015
3:00PM
Soil
B15-Ap07717
53217TB2_090415
Apr 09, 2015
3:00PM
Water
B15-Ap07718
53217QC3_080415
Apr 08, 2015
Soil
B15-Ap07719
X X X X X X
X
Certificate of Analysis NATA Accredited Accreditation Number 1261 Site Number 1254
PRENSA QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Accredited for compliance with ISO/IEC 17025. The results of the tests, calibrations and/or measurements included in this document are traceable to Australian/national standards.
Attention:
John Scott
Report
453692-S
Project name
DSI
Project ID
53217
Received Date
Apr 10, 2015
Sample Matrix
53217BH1_0.15 Soil
53217-BH1_1.5 53217-BH2_0.1 53217-BH2_0.5 Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07631
B15-Ap07632
B15-Ap07633
B15-Ap07634
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Client Sample ID
Date Sampled Test/Reference LOR Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Unit
TRH C6-C9
20
mg/kg
< 20
< 20
< 20
< 20
TRH C10-C14
20
mg/kg
< 20
< 20
< 20
< 20
TRH C15-C28 TRH C29-C36 TRH C10-36 (Total)
50 50 50
mg/kg mg/kg mg/kg
< 50 < 50 < 50
< 50 < 50 < 50
< 50 < 50 < 50
< 50 < 50 < 50
Benzene Toluene
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Ethylbenzene
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
m&p-Xylenes
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
o-Xylene 0.1 Xylenes - Total 0.3 4-Bromofluorobenzene (surr.) 1 Total Recoverable Hydrocarbons - 2013 NEPM Fractions
mg/kg mg/kg %
< 0.1 < 0.3 78
< 0.1 < 0.3 63
< 0.1 < 0.3 84
< 0.1 < 0.3 68
BTEX
NaphthaleneN02
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
TRH C6-C10
20
mg/kg
< 20
< 20
< 20
< 20
TRH C6-C10 less BTEX (F1)N04 TRH >C10-C16 TRH >C10-C16 less Naphthalene (F2)N01
20 50 50
mg/kg mg/kg mg/kg
< 20 < 50 < 50
< 20 < 50 < 50
< 20 < 50 < 50
< 20 < 50 < 50
TRH >C16-C34 TRH >C34-C40
100 100
mg/kg mg/kg
< 100 < 100
< 100 < 100
< 100 < 100
< 100 < 100
Benzo(a)pyrene TEQ (lower bound) *
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Benzo(a)pyrene TEQ (medium bound) * Benzo(a)pyrene TEQ (upper bound) *
0.5 0.5
mg/kg mg/kg
0.6 1.2
0.6 1.2
0.6 1.2
0.6 1.2
Acenaphthene Acenaphthylene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Anthracene Benz(a)anthracene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Benzo(a)pyrene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Benzo(b&j)fluorantheneN07 Benzo(g.h.i)perylene Benzo(k)fluoranthene
0.5 0.5 0.5
mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
Chrysene Dibenz(a.h)anthracene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Polycyclic Aromatic Hydrocarbons
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 1 of 47 Report Number: 453692-S
Sample Matrix
53217BH1_0.15 Soil
53217-BH1_1.5 53217-BH2_0.1 53217-BH2_0.5 Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07631
B15-Ap07632
B15-Ap07633
B15-Ap07634
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Client Sample ID
Date Sampled Test/Reference Polycyclic Aromatic Hydrocarbons
LOR
Unit
Fluoranthene Fluorene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Indeno(1.2.3-cd)pyrene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Naphthalene Phenanthrene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Pyrene Total PAH* 2-Fluorobiphenyl (surr.)
0.5 0.5 1
mg/kg mg/kg %
< 0.5 < 0.5 95
< 0.5 < 0.5 84
< 0.5 < 0.5 84
< 0.5 < 0.5 93
p-Terphenyl-d14 (surr.)
1
%
88
86
87
86
Chlordanes - Total 4.4'-DDD 4.4'-DDE
0.1 0.05 0.05
mg/kg mg/kg mg/kg
< 0.1 < 0.05 < 0.05
< 0.1 < 0.05 < 0.05
< 0.1 < 0.05 < 0.05
< 0.1 < 0.05 < 0.05
4.4'-DDT
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
a-BHC Aldrin
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
b-BHC
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
d-BHC Dieldrin
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Endosulfan I
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Endosulfan II Endosulfan sulphate
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Endrin
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Endrin aldehyde
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Endrin ketone g-BHC (Lindane) Heptachlor Heptachlor epoxide
0.05 0.05 0.05 0.05
mg/kg mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05 < 0.05
Hexachlorobenzene
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Methoxychlor
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
1 1 1
mg/kg % %
<1 103 100
<1 136 123
<1 112 106
<1 132 122
Bolstar
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Chlorpyrifos
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Demeton-O
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Diazinon Dichlorvos
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Disulfoton Ethion
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Ethoprop
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Fenitrothion
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Fensulfothion Fenthion Merphos
0.2 0.2 0.2
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
Methyl azinphos Methyl parathion
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Mevinphos
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Organochlorine Pesticides
Toxaphene Dibutylchlorendate (surr.) Tetrachloro-m-xylene (surr.) Organophosphorous Pesticides
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 2 of 47 Report Number: 453692-S
Sample Matrix
53217BH1_0.15 Soil
53217-BH1_1.5 53217-BH2_0.1 53217-BH2_0.5 Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07631
B15-Ap07632
B15-Ap07633
B15-Ap07634
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Client Sample ID
Date Sampled Test/Reference Organophosphorous Pesticides
LOR
Unit
Naled Phorate
0.5 0.2
mg/kg mg/kg
< 0.5 < 0.2
< 0.5 < 0.2
< 0.5 < 0.2
< 0.5 < 0.2
Ronnel
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Tokuthion Trichloronate
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
1
%
106
128
132
96
Aroclor-1016
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Aroclor-1221 Aroclor-1232
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Aroclor-1242 Aroclor-1248 Aroclor-1254
0.1 0.1 0.1
mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
Aroclor-1260
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Total PCB* Dibutylchlorendate (surr.)
0.1 1
mg/kg %
< 0.1 103
< 0.1 136
< 0.1 112
< 0.1 132
Tetrachloro-m-xylene (surr.)
1
%
100
123
106
122
% Clay* Conductivity (1:5 aqueous extract at 25째C)
1 10
% uS/cm
15 58
14 11
-
-
Triphenylphosphate (surr.) Polychlorinated Biphenyls
pH (1:5 Aqueous extract)
0.1
pH Units
7.1
7.1
-
-
% Moisture Heavy Metals
0.1
%
13
20
2.3
6.6
Arsenic Cadmium Chromium
2 0.4 5
mg/kg mg/kg mg/kg
6.4 < 0.4 11
6.6 < 0.4 15
<2 < 0.4 <5
7.5 < 0.4 11
Copper
5
mg/kg
9.8
13
<5
9.5
Iron
5
mg/kg
20000
24000
-
-
5 0.1
mg/kg mg/kg
37 < 0.1
8.3 < 0.1
<5 < 0.1
<5 < 0.1
5 5
mg/kg mg/kg
8.0 41
9.8 32
<5 5.4
7.6 34
0.05
meq/100g
12
13
-
-
Lead Mercury Nickel Zinc Ion Exchange Properties Cation Exchange Capacity
Client Sample ID
53217-BH3_0.1 53217-BH3_0.5 53217-BH4_0.5 53217-BH4_1.5
Sample Matrix
Soil
Eurofins | mgt Sample No.
B15-Ap07635
B15-Ap07636
B15-Ap07637
B15-Ap07638
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Test/Reference
LOR
Soil
Soil
Soil
Unit
Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9
20
mg/kg
< 20
< 20
< 20
< 20
TRH C10-C14 TRH C15-C28
20 50
mg/kg mg/kg
< 20 < 50
< 20 < 50
< 20 < 50
< 20 < 50
TRH C29-C36
50
mg/kg
< 50
< 50
< 50
< 50
TRH C10-36 (Total)
50
mg/kg
< 50
< 50
< 50
< 50
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 3 of 47 Report Number: 453692-S
Client Sample ID Sample Matrix
53217-BH3_0.1 53217-BH3_0.5 53217-BH4_0.5 53217-BH4_1.5 Soil Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07635
B15-Ap07636
B15-Ap07637
B15-Ap07638
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Test/Reference
LOR
Unit
Benzene Toluene Ethylbenzene
0.1 0.1 0.1
mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
m&p-Xylenes
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
o-Xylene Xylenes - Total
0.1 0.3
mg/kg mg/kg
< 0.1 < 0.3
< 0.1 < 0.3
< 0.1 < 0.3
< 0.1 < 0.3
1
%
60
53
58
79
NaphthaleneN02 TRH C6-C10
0.5 20
mg/kg mg/kg
< 0.5 < 20
< 0.5 < 20
< 0.5 < 20
< 0.5 < 20
TRH C6-C10 less BTEX (F1)N04
20
mg/kg
< 20
< 20
< 20
< 20
TRH >C10-C16 TRH >C10-C16 less Naphthalene (F2)N01
50 50
mg/kg mg/kg
< 50 < 50
< 50 < 50
< 50 < 50
< 50 < 50
TRH >C16-C34
100
mg/kg
< 100
< 100
< 100
< 100
TRH >C34-C40 Polycyclic Aromatic Hydrocarbons
100
mg/kg
< 100
< 100
< 100
< 100
Benzo(a)pyrene TEQ (lower bound) *
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Benzo(a)pyrene TEQ (medium bound) *
0.5
mg/kg
0.6
0.6
0.6
0.6
Benzo(a)pyrene TEQ (upper bound) *
0.5
mg/kg
1.2
1.2
1.2
1.2
Acenaphthene Acenaphthylene Anthracene
0.5 0.5 0.5
mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
Benz(a)anthracene Benzo(a)pyrene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Benzo(b&j)fluorantheneN07
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Benzo(g.h.i)perylene Benzo(k)fluoranthene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Chrysene Dibenz(a.h)anthracene Fluoranthene
0.5 0.5 0.5
mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
0.5 < 0.5 0.7
< 0.5 < 0.5 < 0.5
Fluorene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Indeno(1.2.3-cd)pyrene Naphthalene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Phenanthrene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Pyrene Total PAH*
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
0.7 1.9
< 0.5 < 0.5
2-Fluorobiphenyl (surr.)
1
%
86
79
83
85
p-Terphenyl-d14 (surr.) Organochlorine Pesticides
1
%
89
78
78
84
Chlordanes - Total
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
4.4'-DDD 4.4'-DDE 4.4'-DDT
0.05 0.05 0.05
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
a-BHC
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Aldrin
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
b-BHC d-BHC Dieldrin
0.05 0.05 0.05
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
Endosulfan I
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
BTEX
4-Bromofluorobenzene (surr.) Total Recoverable Hydrocarbons - 2013 NEPM Fractions
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 4 of 47 Report Number: 453692-S
Client Sample ID Sample Matrix
53217-BH3_0.1 53217-BH3_0.5 53217-BH4_0.5 53217-BH4_1.5 Soil Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07635
B15-Ap07636
B15-Ap07637
B15-Ap07638
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Test/Reference
LOR
Unit
Endosulfan II Endosulfan sulphate Endrin
0.05 0.05 0.05
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
Endrin aldehyde
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Endrin ketone g-BHC (Lindane)
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Heptachlor
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Heptachlor epoxide Hexachlorobenzene
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Methoxychlor
Organochlorine Pesticides
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Toxaphene Dibutylchlorendate (surr.)
1 1
mg/kg %
<1 127
<1 131
<1 113
<1 130
Tetrachloro-m-xylene (surr.)
1
%
117
116
105
119
Bolstar Chlorpyrifos
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Demeton-O Diazinon
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Dichlorvos Disulfoton
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Ethion
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Ethoprop Fenitrothion
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Fensulfothion
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Fenthion Merphos
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Methyl azinphos
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Methyl parathion Mevinphos Naled
0.2 0.2 0.5
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.5
< 0.2 < 0.2 < 0.5
< 0.2 < 0.2 < 0.5
< 0.2 < 0.2 < 0.5
Phorate Ronnel
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Tokuthion
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Trichloronate Triphenylphosphate (surr.) Polychlorinated Biphenyls
0.2 1
mg/kg %
< 0.2 129
< 0.2 86
< 0.2 92
< 0.2 92
Aroclor-1016
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Aroclor-1221 Aroclor-1232
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Aroclor-1242
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Aroclor-1248 Aroclor-1254
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Aroclor-1260 Total PCB* Dibutylchlorendate (surr.) Tetrachloro-m-xylene (surr.)
0.1 0.1 1 1
mg/kg mg/kg % %
< 0.1 < 0.1 127 117
< 0.1 < 0.1 131 116
< 0.1 < 0.1 113 105
< 0.1 < 0.1 130 119
% Moisture
0.1
%
5.0
9.1
10.0
15
Organophosphorous Pesticides
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 5 of 47 Report Number: 453692-S
Client Sample ID Sample Matrix
53217-BH3_0.1 53217-BH3_0.5 53217-BH4_0.5 53217-BH4_1.5 Soil Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07635
B15-Ap07636
B15-Ap07637
B15-Ap07638
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Test/Reference
LOR
Unit
2 0.4 5
mg/kg mg/kg mg/kg
5.1 < 0.4 5.8
<2 < 0.4 9.9
Copper
5
mg/kg
15
Lead Mercury
5 0.1
mg/kg mg/kg
10 < 0.1
Nickel
5
mg/kg
6.2
Zinc
5
mg/kg
29
Heavy Metals Arsenic Cadmium Chromium
12 < 0.4 15
8.6 < 0.4 13
7.9
39
12
5.9 < 0.1
400 0.7
31 < 0.1
7.3
8.8
9.7
30
160
54
Client Sample ID
53217-BH5_0.5 53217-BH5_1.5 53217-BH6_0.1 53217-BH6_0.5
Sample Matrix
Soil
Soil
Soil
Soil
Eurofins | mgt Sample No.
B15-Ap07639
B15-Ap07640
B15-Ap07641
B15-Ap07642
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Date Sampled Test/Reference LOR Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Unit
TRH C6-C9
20
mg/kg
< 20
< 20
< 20
< 20
TRH C10-C14
20
mg/kg
< 20
< 20
< 20
< 20
TRH C15-C28 TRH C29-C36 TRH C10-36 (Total)
50 50 50
mg/kg mg/kg mg/kg
< 50 < 50 < 50
< 50 < 50 < 50
< 50 < 50 < 50
< 50 < 50 < 50
Benzene Toluene
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Ethylbenzene m&p-Xylenes o-Xylene
0.1 0.2 0.1
mg/kg mg/kg mg/kg
< 0.1 < 0.2 < 0.1
< 0.1 < 0.2 < 0.1
< 0.1 < 0.2 < 0.1
< 0.1 < 0.2 < 0.1
Xylenes - Total 0.3 4-Bromofluorobenzene (surr.) 1 Total Recoverable Hydrocarbons - 2013 NEPM Fractions
mg/kg %
< 0.3 75
< 0.3 56
< 0.3 59
< 0.3 67
BTEX
NaphthaleneN02
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
TRH C6-C10 TRH C6-C10 less BTEX (F1)N04 TRH >C10-C16 TRH >C10-C16 less Naphthalene (F2)N01
20 20 50 50
mg/kg mg/kg mg/kg mg/kg
< 20 < 20 < 50 < 50
< 20 < 20 < 50 < 50
< 20 < 20 < 50 < 50
< 20 < 20 < 50 < 50
TRH >C16-C34 TRH >C34-C40
100 100
mg/kg mg/kg
< 100 < 100
< 100 < 100
< 100 < 100
< 100 < 100
Benzo(a)pyrene TEQ (lower bound) *
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Benzo(a)pyrene TEQ (medium bound) * Benzo(a)pyrene TEQ (upper bound) *
0.5 0.5
mg/kg mg/kg
0.6 1.2
0.6 1.2
0.6 1.2
0.6 1.2
Acenaphthene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Acenaphthylene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Anthracene Benz(a)anthracene Benzo(a)pyrene
0.5 0.5 0.5
mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
Benzo(b&j)fluorantheneN07 Benzo(g.h.i)perylene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Benzo(k)fluoranthene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Polycyclic Aromatic Hydrocarbons
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 6 of 47 Report Number: 453692-S
Client Sample ID Sample Matrix
53217-BH5_0.5 53217-BH5_1.5 53217-BH6_0.1 53217-BH6_0.5 Soil Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07639
B15-Ap07640
B15-Ap07641
B15-Ap07642
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Test/Reference
LOR
Unit
0.5 0.5 0.5
mg/kg mg/kg mg/kg
Polycyclic Aromatic Hydrocarbons Chrysene Dibenz(a.h)anthracene Fluoranthene
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
Fluorene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Indeno(1.2.3-cd)pyrene Naphthalene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Phenanthrene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Pyrene Total PAH*
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
2-Fluorobiphenyl (surr.)
1
%
99
90
108
80
p-Terphenyl-d14 (surr.) Organochlorine Pesticides
1
%
93
97
117
89
Chlordanes - Total
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
4.4'-DDD
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
4.4'-DDE 4.4'-DDT
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
a-BHC
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Aldrin
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
b-BHC d-BHC
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Dieldrin
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Endosulfan I Endosulfan II
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Endosulfan sulphate
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Endrin Endrin aldehyde
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Endrin ketone
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
g-BHC (Lindane) Heptachlor Heptachlor epoxide
0.05 0.05 0.05
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
Hexachlorobenzene Methoxychlor
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Toxaphene
1
mg/kg
<1
<1
<1
<1
Dibutylchlorendate (surr.) Tetrachloro-m-xylene (surr.)
1 1
% %
120 111
136 125
142 127
125 124
Bolstar
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Chlorpyrifos Demeton-O
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Diazinon
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Dichlorvos Disulfoton
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Ethion Ethoprop Fenitrothion Fensulfothion
0.2 0.2 0.2 0.2
mg/kg mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2 < 0.2
Fenthion Merphos
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Methyl azinphos
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Organophosphorous Pesticides
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 7 of 47 Report Number: 453692-S
Client Sample ID Sample Matrix
53217-BH5_0.5 53217-BH5_1.5 53217-BH6_0.1 53217-BH6_0.5 Soil Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07639
B15-Ap07640
B15-Ap07641
B15-Ap07642
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Test/Reference
LOR
Unit
Methyl parathion Mevinphos Naled
0.2 0.2 0.5
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.5
< 0.2 < 0.2 < 0.5
< 0.2 < 0.2 < 0.5
< 0.2 < 0.2 < 0.5
Phorate
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Ronnel Tokuthion
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Trichloronate
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
1
%
113
80
99
72
Aroclor-1016
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Aroclor-1221
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Aroclor-1232 Aroclor-1242
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Aroclor-1248
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Aroclor-1254 Aroclor-1260 Total PCB*
0.1 0.1 0.1
mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
Organophosphorous Pesticides
Triphenylphosphate (surr.) Polychlorinated Biphenyls
Dibutylchlorendate (surr.)
1
%
120
136
142
125
Tetrachloro-m-xylene (surr.)
1
%
111
125
127
124
% Moisture Heavy Metals
0.1
%
5.2
8.2
18
12
Arsenic Cadmium
2 0.4
mg/kg mg/kg
16 < 0.4
5.4 < 0.4
<2 7.7
4.6 < 0.4
Chromium
5
mg/kg
50
12
20
8.9
Copper Lead
5 5
mg/kg mg/kg
<5 <5
9.6 5.1
28 380
7.6 15
Mercury Nickel
0.1 5
mg/kg mg/kg
< 0.1 <5
< 0.1 8.6
0.2 10
< 0.1 6.3
5
mg/kg
<5
32
17000
59
Zinc
Client Sample ID
53217-BH7_0.5 53217-BH7_1.5 53217-BH8_0.1 53217-BH8_0.5
Sample Matrix
Soil
Eurofins | mgt Sample No.
B15-Ap07643
B15-Ap07644
B15-Ap07645
B15-Ap07646
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Test/Reference LOR Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Soil
Soil
Soil
Unit
TRH C6-C9
20
mg/kg
< 20
< 20
< 20
< 20
TRH C10-C14 TRH C15-C28
20 50
mg/kg mg/kg
< 20 < 50
< 20 < 50
< 20 110
< 20 < 50
TRH C29-C36
50
mg/kg
< 50
< 50
61
< 50
TRH C10-36 (Total)
50
mg/kg
< 50
< 50
170
< 50
Benzene Toluene
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Ethylbenzene
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
m&p-Xylenes o-Xylene
0.2 0.1
mg/kg mg/kg
< 0.2 < 0.1
< 0.2 < 0.1
< 0.2 < 0.1
< 0.2 < 0.1
BTEX
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 8 of 47 Report Number: 453692-S
Client Sample ID Sample Matrix
53217-BH7_0.5 53217-BH7_1.5 53217-BH8_0.1 53217-BH8_0.5 Soil Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07643
B15-Ap07644
B15-Ap07645
B15-Ap07646
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Test/Reference
LOR
Unit
BTEX Xylenes - Total 0.3 4-Bromofluorobenzene (surr.) 1 Total Recoverable Hydrocarbons - 2013 NEPM Fractions
mg/kg %
< 0.3 73
< 0.3 55
< 0.3 66
< 0.3 65
NaphthaleneN02
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
TRH C6-C10
20
mg/kg
< 20
< 20
< 20
< 20
TRH C6-C10 less BTEX (F1)N04 TRH >C10-C16 TRH >C10-C16 less Naphthalene (F2)N01 TRH >C16-C34 TRH >C34-C40
20 50 50 100 100
mg/kg mg/kg mg/kg mg/kg mg/kg
< 20 < 50 < 50 < 100 < 100
< 20 < 50 < 50 < 100 < 100
< 20 < 50 < 50 160 < 100
< 20 < 50 < 50 < 100 < 100
Benzo(a)pyrene TEQ (lower bound) *
0.5
mg/kg
< 0.5
< 0.5
3.8
1.2
Benzo(a)pyrene TEQ (medium bound) *
0.5
mg/kg
0.6
0.6
3.8
1.5
Benzo(a)pyrene TEQ (upper bound) * Acenaphthene
0.5 0.5
mg/kg mg/kg
1.2 < 0.5
1.2 < 0.5
3.8 < 0.5
1.8 < 0.5
Acenaphthylene Anthracene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 < 0.5
Benz(a)anthracene
0.5
mg/kg
< 0.5
< 0.5
1.9
0.7
Benzo(a)pyrene
0.5
mg/kg
< 0.5
< 0.5
2.5
1.0
Benzo(b&j)fluorantheneN07 Benzo(g.h.i)perylene Benzo(k)fluoranthene
0.5 0.5 0.5
mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
2.0 1.3 1.6
0.7 0.5 0.8
Chrysene Dibenz(a.h)anthracene Fluoranthene
0.5 0.5 0.5
mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
1.8 0.6 2.5
0.8 < 0.5 1.0
Fluorene Indeno(1.2.3-cd)pyrene
0.5 0.5
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
< 0.5 1.3
< 0.5 < 0.5
Naphthalene Phenanthrene Pyrene
0.5 0.5 0.5
mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
< 0.5 0.5 2.9
< 0.5 < 0.5 1.2
Total PAH*
0.5
mg/kg
< 0.5
< 0.5
19
6.7
1 1
% %
78 84
77 81
82 85
82 84
Chlordanes - Total 4.4'-DDD 4.4'-DDE 4.4'-DDT
0.1 0.05 0.05 0.05
mg/kg mg/kg mg/kg mg/kg
< 0.1 < 0.05 < 0.05 < 0.05
< 0.1 < 0.05 < 0.05 < 0.05
< 0.1 < 0.05 < 0.05 < 0.05
< 0.1 < 0.05 < 0.05 < 0.05
a-BHC Aldrin
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
b-BHC
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
d-BHC Dieldrin
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Endosulfan I
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Endosulfan II
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Endosulfan sulphate Endrin Endrin aldehyde
0.05 0.05 0.05
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
Endrin ketone
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Polycyclic Aromatic Hydrocarbons
2-Fluorobiphenyl (surr.) p-Terphenyl-d14 (surr.) Organochlorine Pesticides
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 9 of 47 Report Number: 453692-S
Client Sample ID Sample Matrix
53217-BH7_0.5 53217-BH7_1.5 53217-BH8_0.1 53217-BH8_0.5 Soil Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07643
B15-Ap07644
B15-Ap07645
B15-Ap07646
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Test/Reference
LOR
Unit
g-BHC (Lindane) Heptachlor Heptachlor epoxide
0.05 0.05 0.05
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
Hexachlorobenzene
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Methoxychlor Toxaphene
0.05 1
mg/kg mg/kg
< 0.05 <1
< 0.05 <1
< 0.05 <1
< 0.05 <1
Organochlorine Pesticides
Dibutylchlorendate (surr.)
1
%
118
123
112
87
Tetrachloro-m-xylene (surr.) Organophosphorous Pesticides
1
%
117
121
125
98
Bolstar
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Chlorpyrifos
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Demeton-O Diazinon
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Dichlorvos
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Disulfoton Ethion Ethoprop
0.2 0.2 0.2
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
Fenitrothion
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Fensulfothion Fenthion
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Merphos
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Methyl azinphos Methyl parathion
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Mevinphos
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Naled Phorate
0.5 0.2
mg/kg mg/kg
< 0.5 < 0.2
< 0.5 < 0.2
< 0.5 < 0.2
< 0.5 < 0.2
Ronnel
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Tokuthion Trichloronate Triphenylphosphate (surr.)
0.2 0.2 1
mg/kg mg/kg %
< 0.2 < 0.2 69
< 0.2 < 0.2 69
< 0.2 < 0.2 74
< 0.2 < 0.2 77
Aroclor-1016 Aroclor-1221 Aroclor-1232
0.1 0.1 0.1
mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
Aroclor-1242 Aroclor-1248
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Aroclor-1254
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Aroclor-1260 Total PCB*
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Polychlorinated Biphenyls
Dibutylchlorendate (surr.)
1
%
118
123
112
87
Tetrachloro-m-xylene (surr.)
1
%
117
121
125
98
0.1
%
11
9.0
17
6.1
% Moisture Heavy Metals Arsenic Cadmium Chromium Copper Lead
2
mg/kg
7.7
6.5
7.8
4.1
0.4 5
mg/kg mg/kg
< 0.4 18
< 0.4 11
0.4 13
< 0.4 8.8
5 5
mg/kg mg/kg
87 22
8.8 <5
23 69
11 27
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 10 of 47 Report Number: 453692-S
Client Sample ID Sample Matrix
53217-BH7_0.5 53217-BH7_1.5 53217-BH8_0.1 53217-BH8_0.5 Soil Soil Soil Soil
Eurofins | mgt Sample No.
B15-Ap07643
B15-Ap07644
B15-Ap07645
B15-Ap07646
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Test/Reference
LOR
Unit
0.1 5 5
mg/kg mg/kg mg/kg
Heavy Metals Mercury Nickel Zinc
0.3 9.1 140
< 0.1 6.0 55
Sample Matrix
5321753217-BH9_0.5 53217-BH9_1.0 BH10_1.5 Soil Soil Soil
53217BH10_3.0 Soil
Eurofins | mgt Sample No.
B15-Ap07647
B15-Ap07648
B15-Ap07649
B15-Ap07650
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Client Sample ID
Test/Reference
LOR
< 0.1 6.0 43
< 0.1 8.1 53
Unit
Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9
20
mg/kg
< 20
< 20
< 20
< 20
TRH C10-C14 TRH C15-C28 TRH C29-C36 TRH C10-36 (Total) BTEX
20 50 50 50
mg/kg mg/kg mg/kg mg/kg
< 20 210 150 360
< 20 < 50 < 50 < 50
< 20 < 50 < 50 < 50
< 20 < 50 < 50 < 50
Benzene
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Toluene
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Ethylbenzene m&p-Xylenes o-Xylene Xylenes - Total
0.1 0.2 0.1 0.3
mg/kg mg/kg mg/kg mg/kg
< 0.1 < 0.2 < 0.1 < 0.3
< 0.1 < 0.2 < 0.1 < 0.3
< 0.1 < 0.2 < 0.1 < 0.3
< 0.1 < 0.2 < 0.1 < 0.3
1
%
69
57
62
69
4-Bromofluorobenzene (surr.) Total Recoverable Hydrocarbons - 2013 NEPM Fractions NaphthaleneN02
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
TRH C6-C10 TRH C6-C10 less BTEX (F1)N04 TRH >C10-C16
20 20 50
mg/kg mg/kg mg/kg
< 20 < 20 < 50
< 20 < 20 < 50
< 20 < 20 < 50
< 20 < 20 < 50
TRH >C10-C16 less Naphthalene (F2)N01 TRH >C16-C34
50 100
mg/kg mg/kg
< 50 330
< 50 < 100
< 50 < 100
< 50 < 100
TRH >C34-C40
100
mg/kg
< 100
< 100
< 100
< 100
Benzo(a)pyrene TEQ (lower bound) * Benzo(a)pyrene TEQ (medium bound) *
0.5 0.5
mg/kg mg/kg
2.2 2.5
< 0.5 0.6
3.0 3.2
1.5 1.7
Benzo(a)pyrene TEQ (upper bound) * Acenaphthene Acenaphthylene
0.5 0.5 0.5
mg/kg mg/kg mg/kg
2.7 < 0.5 < 0.5
1.2 < 0.5 < 0.5
3.5 < 0.5 < 0.5
2.0 < 0.5 < 0.5
Anthracene
0.5
mg/kg
< 0.5
< 0.5
0.6
< 0.5
Benz(a)anthracene Benzo(a)pyrene
0.5 0.5
mg/kg mg/kg
1.5 1.7
< 0.5 < 0.5
2.0 2.3
1.1 1.1
Benzo(b&j)fluorantheneN07 Benzo(g.h.i)perylene Benzo(k)fluoranthene Chrysene
0.5 0.5 0.5 0.5
mg/kg mg/kg mg/kg mg/kg
1.2 1.2 1.3 1.4
< 0.5 < 0.5 < 0.5 < 0.5
1.4 1.2 1.9 1.9
0.8 0.7 1.0 1.2
Dibenz(a.h)anthracene Fluoranthene
0.5 0.5
mg/kg mg/kg
< 0.5 2.7
< 0.5 < 0.5
< 0.5 3.8
< 0.5 1.6
Fluorene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
< 0.5
Polycyclic Aromatic Hydrocarbons
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 11 of 47 Report Number: 453692-S
Sample Matrix
5321753217-BH9_0.5 53217-BH9_1.0 BH10_1.5 Soil Soil Soil
53217BH10_3.0 Soil
Eurofins | mgt Sample No.
B15-Ap07647
B15-Ap07648
B15-Ap07649
B15-Ap07650
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Client Sample ID
Date Sampled Test/Reference Polycyclic Aromatic Hydrocarbons
LOR
Unit
Indeno(1.2.3-cd)pyrene Naphthalene
0.5 0.5
mg/kg mg/kg
1.1 < 0.5
< 0.5 < 0.5
1.1 < 0.5
0.7 < 0.5
Phenanthrene
0.5
mg/kg
1.0
< 0.5
2.0
1.6
Pyrene Total PAH*
0.5 0.5
mg/kg mg/kg
2.4 16
< 0.5 < 0.5
3.7 22
1.4 11
1 1
% %
79 81
78 85
79 83
94 75
Chlordanes - Total 4.4'-DDD
0.1 0.05
mg/kg mg/kg
< 0.1 < 0.05
< 0.1 < 0.05
< 0.1 < 0.05
< 0.1 < 0.05
4.4'-DDE 4.4'-DDT a-BHC
0.05 0.05 0.05
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
Aldrin
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
b-BHC d-BHC
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Dieldrin
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Endosulfan I Endosulfan II
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Endosulfan sulphate
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Endrin Endrin aldehyde
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Endrin ketone
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
g-BHC (Lindane)
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Heptachlor Heptachlor epoxide
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
Hexachlorobenzene
0.05
mg/kg
< 0.05
< 0.05
< 0.05
< 0.05
Methoxychlor Toxaphene Dibutylchlorendate (surr.)
0.05 1 1
mg/kg mg/kg %
< 0.05 <1 112
< 0.05 <1 86
< 0.05 <1 99
< 0.05 <1 128
1
%
113
94
110
143
Bolstar
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Chlorpyrifos Demeton-O
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Diazinon
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Dichlorvos
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Disulfoton Ethion
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Ethoprop
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Fenitrothion Fensulfothion
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Fenthion
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
Merphos Methyl azinphos Methyl parathion
0.2 0.2 0.2
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
Mevinphos Naled
0.2 0.5
mg/kg mg/kg
< 0.2 < 0.5
< 0.2 < 0.5
< 0.2 < 0.5
< 0.2 < 0.5
Phorate
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
2-Fluorobiphenyl (surr.) p-Terphenyl-d14 (surr.) Organochlorine Pesticides
Tetrachloro-m-xylene (surr.) Organophosphorous Pesticides
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 12 of 47 Report Number: 453692-S
Sample Matrix
5321753217-BH9_0.5 53217-BH9_1.0 BH10_1.5 Soil Soil Soil
53217BH10_3.0 Soil
Eurofins | mgt Sample No.
B15-Ap07647
B15-Ap07648
B15-Ap07649
B15-Ap07650
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Apr 09, 2015
Client Sample ID
Date Sampled Test/Reference Organophosphorous Pesticides
LOR
Unit
Ronnel Tokuthion
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
< 0.2 < 0.2
Trichloronate
0.2
mg/kg
< 0.2
< 0.2
< 0.2
< 0.2
1
%
72
71
77
125
Aroclor-1016 Aroclor-1221
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Aroclor-1232 Aroclor-1242
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Aroclor-1248
0.1
mg/kg
< 0.1
< 0.1
< 0.1
< 0.1
Aroclor-1254 Aroclor-1260 Total PCB*
0.1 0.1 0.1
mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
1 1
% %
112 113
86 94
99 110
128 143
0.1
%
19
6.7
12
23
Triphenylphosphate (surr.) Polychlorinated Biphenyls
Dibutylchlorendate (surr.) Tetrachloro-m-xylene (surr.) % Moisture Heavy Metals Arsenic
2
mg/kg
15
3.9
8.5
8.7
0.4 5
mg/kg mg/kg
1.3 13
< 0.4 9.2
1.5 15
< 0.4 15
Copper
5
mg/kg
160
14
170
34
Lead Mercury Nickel
5 0.1 5
mg/kg mg/kg mg/kg
1200 0.4 23
46 < 0.1 7.8
410 0.4 14
180 0.2 17
5
mg/kg
2300
83
1500
140
Cadmium Chromium
Zinc
Client Sample ID
53217BH11_0.5
53217BH11_1.0
53217QC3_080415
Sample Matrix
Soil
Soil
Soil
Eurofins | mgt Sample No.
B15-Ap07651
B15-Ap07652
B15-Ap07719
Date Sampled
Apr 09, 2015
Apr 09, 2015
Apr 08, 2015
Test/Reference LOR Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Unit
TRH C6-C9
20
mg/kg
< 20
< 20
< 20
TRH C10-C14
20
mg/kg
< 20
< 20
< 20
TRH C15-C28 TRH C29-C36
50 50
mg/kg mg/kg
< 50 < 50
< 50 < 50
< 50 < 50
TRH C10-36 (Total)
50
mg/kg
< 50
< 50
< 50
Benzene Toluene
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Ethylbenzene
0.1
mg/kg
< 0.1
< 0.1
< 0.1
m&p-Xylenes o-Xylene Xylenes - Total
0.2 0.1 0.3
mg/kg mg/kg mg/kg
< 0.2 < 0.1 < 0.3
< 0.2 < 0.1 < 0.3
< 0.2 < 0.1 < 0.3
1
%
71
61
77
BTEX
4-Bromofluorobenzene (surr.)
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 13 of 47 Report Number: 453692-S
Sample Matrix
53217BH11_0.5 Soil
53217BH11_1.0 Soil
53217QC3_080415 Soil
Eurofins | mgt Sample No.
B15-Ap07651
B15-Ap07652
B15-Ap07719
Apr 09, 2015
Apr 09, 2015
Apr 08, 2015
Client Sample ID
Date Sampled Test/Reference LOR Total Recoverable Hydrocarbons - 2013 NEPM Fractions
Unit
NaphthaleneN02 TRH C6-C10
0.5 20
mg/kg mg/kg
< 0.5 < 20
< 0.5 < 20
< 0.5 < 20
TRH C6-C10 less BTEX (F1)N04
20
mg/kg
< 20
< 20
< 20
TRH >C10-C16 TRH >C10-C16 less Naphthalene (F2)N01
50 50
mg/kg mg/kg
< 50 < 50
< 50 < 50
< 50 < 50
TRH >C16-C34 TRH >C34-C40 Polycyclic Aromatic Hydrocarbons
100 100
mg/kg mg/kg
< 100 < 100
< 100 < 100
< 100 < 100
Benzo(a)pyrene TEQ (lower bound) * Benzo(a)pyrene TEQ (medium bound) * Benzo(a)pyrene TEQ (upper bound) * Acenaphthene Acenaphthylene
0.5 0.5 0.5 0.5 0.5
mg/kg mg/kg mg/kg mg/kg mg/kg
1.2 1.4 1.7 < 0.5 < 0.5
< 0.5 0.6 1.2 < 0.5 < 0.5
< 0.5 0.6 1.2 < 0.5 < 0.5
Anthracene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
Benz(a)anthracene Benzo(a)pyrene
0.5 0.5
mg/kg mg/kg
0.7 0.9
< 0.5 < 0.5
< 0.5 < 0.5
Benzo(b&j)fluorantheneN07
0.5
mg/kg
0.8
< 0.5
< 0.5
Benzo(g.h.i)perylene Benzo(k)fluoranthene
0.5 0.5
mg/kg mg/kg
0.5 0.8
< 0.5 < 0.5
< 0.5 < 0.5
Chrysene
0.5
mg/kg
0.8
< 0.5
< 0.5
Dibenz(a.h)anthracene Fluoranthene
0.5 0.5
mg/kg mg/kg
< 0.5 1.3
< 0.5 0.5
< 0.5 < 0.5
Fluorene
0.5
mg/kg
< 0.5
< 0.5
< 0.5
Indeno(1.2.3-cd)pyrene Naphthalene Phenanthrene
0.5 0.5 0.5
mg/kg mg/kg mg/kg
0.5 < 0.5 0.5
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
Pyrene
0.5
mg/kg
1.2
< 0.5
< 0.5
Total PAH* 2-Fluorobiphenyl (surr.) p-Terphenyl-d14 (surr.)
0.5 1 1
mg/kg % %
8.0 83 89
0.5 83 91
< 0.5 91 93
Chlordanes - Total 4.4'-DDD
0.1 0.05
mg/kg mg/kg
< 0.1 < 0.05
< 0.1 < 0.05
-
4.4'-DDE 4.4'-DDT
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
-
a-BHC
0.05
mg/kg
< 0.05
< 0.05
-
Aldrin
0.05
mg/kg
< 0.05
< 0.05
-
b-BHC d-BHC
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
-
Dieldrin
0.05
mg/kg
< 0.05
< 0.05
-
Endosulfan I Endosulfan II
0.05 0.05
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
-
Endosulfan sulphate
0.05
mg/kg
< 0.05
< 0.05
-
Endrin Endrin aldehyde Endrin ketone
0.05 0.05 0.05
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
-
g-BHC (Lindane) Heptachlor Heptachlor epoxide
0.05 0.05 0.05
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
-
Organochlorine Pesticides
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 14 of 47 Report Number: 453692-S
Sample Matrix
53217BH11_0.5 Soil
53217BH11_1.0 Soil
53217QC3_080415 Soil
Eurofins | mgt Sample No.
B15-Ap07651
B15-Ap07652
B15-Ap07719
Apr 09, 2015
Apr 09, 2015
Apr 08, 2015
Client Sample ID
Date Sampled Test/Reference Organochlorine Pesticides
LOR
Unit
Hexachlorobenzene Methoxychlor
0.05 0.05
mg/kg mg/kg
Toxaphene
1
mg/kg
Dibutylchlorendate (surr.) Tetrachloro-m-xylene (surr.) Organophosphorous Pesticides
1 1
% %
Bolstar
0.2
mg/kg
Chlorpyrifos Demeton-O
0.2 0.2
mg/kg mg/kg
Diazinon
0.2
Dichlorvos Disulfoton Ethion
0.2 0.2 0.2
Ethoprop Fenitrothion
< 0.05 < 0.05
-
<1
<1
-
124 130
131 126
-
< 0.2
< 0.2
-
< 0.2 < 0.2
< 0.2 < 0.2
-
mg/kg
< 0.2
< 0.2
-
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
-
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
-
Fensulfothion
0.2
mg/kg
< 0.2
< 0.2
-
Fenthion
0.2
mg/kg
< 0.2
< 0.2
-
Merphos Methyl azinphos
0.2 0.2
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
-
Methyl parathion
0.2
mg/kg
< 0.2
< 0.2
-
Mevinphos Naled
0.2 0.5
mg/kg mg/kg
< 0.2 < 0.5
< 0.2 < 0.5
-
Phorate
0.2
mg/kg
< 0.2
< 0.2
-
Ronnel Tokuthion Trichloronate
0.2 0.2 0.2
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
-
1
%
77
78
-
Aroclor-1016
0.1
mg/kg
< 0.1
< 0.1
-
Aroclor-1221
0.1
mg/kg
< 0.1
< 0.1
-
Aroclor-1232 Aroclor-1242 Aroclor-1248
0.1 0.1 0.1
mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
-
Aroclor-1254 Aroclor-1260
0.1 0.1
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
-
Total PCB*
-
Triphenylphosphate (surr.) Polychlorinated Biphenyls
< 0.05 < 0.05
0.1
mg/kg
< 0.1
< 0.1
Dibutylchlorendate (surr.)
1
%
124
131
-
Tetrachloro-m-xylene (surr.)
1
%
130
126
-
0.1
%
15
13
11
% Moisture Heavy Metals Arsenic
2
mg/kg
7.8
6.4
3.2
Cadmium Chromium Copper
0.4 5 5
mg/kg mg/kg mg/kg
< 0.4 14 170
< 0.4 14 32
< 0.4 19 92
Lead Mercury
5 0.1
mg/kg mg/kg
440 0.2
21 < 0.1
24 < 0.1
5 5
mg/kg mg/kg
12 170
11 490
6.6 32
Nickel Zinc
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 15 of 47 Report Number: 453692-S
Sample History Where samples are submitted/analysed over several days, the last date of extraction and analysis is reported. A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this, some of the method reference information on reports has changed. However, no substantive change has been made to our laboratory methods, and as such there is no change in the validity of current or previous results (regarding both quality and NATA accreditation). If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised results should testing be performed outside the recommended holding time.
Description
Testing Site
Extracted
Holding Time
Eurofins | mgt Suite 7 Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Melbourne
Apr 14, 2015
14 Day
Melbourne
Apr 14, 2015
14 Day
Melbourne
Apr 14, 2015
14 Day
Melbourne
Apr 14, 2015
28 Day
Melbourne
Apr 14, 2015
14 Day
Melbourne
Apr 14, 2015
14 Day
Melbourne
Apr 14, 2015
14 Day
Melbourne
Apr 14, 2015
28 Day
Brisbane
Apr 15, 2015
6 Month
Melbourne
Apr 14, 2015
7 Day
Melbourne
Apr 14, 2015
180 Day
Melbourne
Apr 14, 2015
7 Day
Ion Exchange Properties
Melbourne
Apr 15, 2015
% Moisture
Melbourne
Apr 13, 2015
- Method: TRH C6-C36 - LTM-ORG-2010
Total Recoverable Hydrocarbons - 2013 NEPM Fractions - Method: TRH C6-C40 - LTM-ORG-2010
Polycyclic Aromatic Hydrocarbons - Method: USEPA 8270 Polycyclic Aromatic Hydrocarbons
Metals M8 - Method: USEPA 6010/6020 Heavy Metals & USEPA 7470/71 Mercury
BTEX and Naphthalene BTEX - Method: TRH C6-C40 - LTM-ORG-2010
Eurofins | mgt Suite 10 Organochlorine Pesticides - Method: USEPA 8081 Organochlorine Pesticides
Organophosphorous Pesticides - Method: USEPA 8270 Organophosphorus Pesticides
Polychlorinated Biphenyls - Method: USEPA 8082 Polychlorinated Biphenyls
% Clay* - Method: LTM-GEN-7040
pH (1:5 Aqueous extract) - Method: LTM-GEN-7090 pH in soil by ISE
Heavy Metals - Method: USEPA 6010/6020 Heavy Metals
Conductivity (1:5 aqueous extract at 25째C) - Method: LM-LTM-INO-4010
14 Day
- Method: LTM-GEN-7080 Moisture
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 16 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
. Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
Order No.: Report #: Phone: Fax:
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory Sample ID
Sample Date
Sampling Time
Matrix
LAB ID
53217BH1_0.15
Apr 09, 2015
3:00PM
Soil
B15-Ap07631
53217BH1_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07632
53217BH2_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07633
53217BH2_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07634
53217BH3_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07635
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 17 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH3_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07636
53217BH4_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07637
53217BH4_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07638
53217BH5_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07639
53217BH5_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07640
53217BH6_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07641
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 18 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH6_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07642
53217BH7_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07643
53217BH7_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07644
53217BH8_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07645
53217BH8_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07646
53217BH9_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07647
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 19 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH9_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07648
53217BH10_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07649
53217BH10_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07650
53217BH11_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07651
53217BH11_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07652
53217TB1_080415
Apr 08, 2015
Water
B15-Ap07653
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
X
Page 20 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217FB1_080415
Apr 08, 2015
Water
B15-Ap07654
53217R1_080415
Apr 08, 2015
Water
B15-Ap07655
53217FB2_090415
Apr 09, 2015
3:00PM
Water
B15-Ap07656
53217R2_090415
Apr 09, 2015
3:00PM
Water
B15-Ap07657
53217BH1_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07658
53217BH1_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07659
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 21 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH1_1.3
Apr 09, 2015
3:00PM
Soil
B15-Ap07660
53217BH1_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07661
53217BH1_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07662
53217MW1_4.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07663
53217MW1_5.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07664
53217MW1_6.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07665
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 22 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217MW1_7.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07666
53217MW1_8.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07667
53217MW1_9.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07668
53217BH2_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07669
53217BH2_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07670
53217BH2_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07671
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 23 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH2_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07672
53217BH3_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07673
53217BH3_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07674
53217BH3_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07675
53217BH3_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07676
53217MW2_4.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07677
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 24 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217MW2_5.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07678
53217MW2_6.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07679
53217MW2_7.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07680
53217MW2_8.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07681
53217BH4_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07682
53217BH4_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07683
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 25 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH4_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07684
53217BH4_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07685
53217BH5_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07686
53217BH5_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07687
53217BH5_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07688
53217BH5_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07689
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 26 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH6_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07690
53217BH6_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07691
53217BH6_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07692
53217BH6_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07693
53217BH7_0.15
Apr 09, 2015
3:00PM
Soil
B15-Ap07694
53217BH7_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07695
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 27 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH7_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07696
53217BH7_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07697
53217BH8_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07698
53217BH8_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07699
53217BH8_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07700
53217BH8_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07701
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 28 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217MW3_6.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07702
53217MW3_7.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07703
53217MW3_8.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07704
53217BH9_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07705
53217BH9_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07706
53217BH9_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07707
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 29 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH10_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07708
53217BH10_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07709
53217BH10_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07710
53217BH10_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07711
53217BH11_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07712
53217BH11_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07713
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 30 of 47 Report Number: 453692-S
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH11_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07714
53217QC1_080415
Apr 08, 2015
3:00PM
Soil
B15-Ap07715
53217QC5_090415
Apr 09, 2015
3:00PM
Soil
B15-Ap07716
53217QC7_090415
Apr 09, 2015
3:00PM
Soil
B15-Ap07717
53217TB2_090415
Apr 09, 2015
3:00PM
Water
B15-Ap07718
53217QC3_080415
Apr 08, 2015
Soil
B15-Ap07719
X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
X
X
Page 31 of 47 Report Number: 453692-S
Eurofins | mgt Internal Quality Control Review and Glossary General 1.
Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on request.
2.
All soil results are reported on a dry basis, unless otherwise stated.
3.
Actual LORs are matrix dependant. Quoted LORs may be raised where sample extracts are diluted due to interferences.
4.
Results are uncorrected for matrix spikes or surrogate recoveries.
5.
SVOC analysis on waters are performed on homogenised, unfiltered samples, unless noted otherwise.
6.
Samples were analysed on an 'as received' basis. 7. This report replaces any interim results previously issued.
Holding Times Please refer to 'Sample Preservation and Container Guide' for holding times (QS3001). For samples received on the last day of holding time, notification of testing requirements should have been received at least 6 hours prior to sample receipt deadlines as stated on the Sample Receipt Advice. If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues, suitably qualified results may still be reported. Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control. **NOTE: pH duplicates are reported as a range NOT as RPD
UNITS mg/kg: milligrams per Kilogram
mg/l: milligrams per litre
ug/l: micrograms per litre
ppm: Parts per million
ppb: Parts per billion
%: Percentage
org/100ml: Organisms per 100 millilitres
NTU: Nephelometric Turbidity Units
MPN/100mL: Most Probable Number of organisms per 100 millilitres
TERMS Dry
Where a moisture has been determined on a solid sample the result is expressed on a dry basis.
LOR
Limit of Reporting.
SPIKE
Addition of the analyte to the sample and reported as percentage recovery.
RPD
Relative Percent Difference between two Duplicate pieces of analysis.
LCS
Laboratory Control Sample - reported as percent recovery
CRM
Certified Reference Material - reported as percent recovery
Method Blank
In the case of solid samples these are performed on laboratory certified clean sands. In the case of water samples these are performed on de-ionised water.
Surr - Surrogate
The addition of a like compound to the analyte target and reported as percentage recovery.
Duplicate
A second piece of analysis from the same sample and reported in the same units as the result to show comparison.
Batch Duplicate
A second piece of analysis from a sample outside of the clients batch of samples but run within the laboratory batch of analysis.
Batch SPIKE
Spike recovery reported on a sample from outside of the clients batch of samples but run within the laboratory batch of analysis.
USEPA
United States Environmental Protection Agency
APHA
American Public Health Association
ASLP
Australian Standard Leaching Procedure (AS4439.3)
TCLP
Toxicity Characteristic Leaching Procedure
COC
Chain of Custody
SRA
Sample Receipt Advice
CP
Client Parent - QC was performed on samples pertaining to this report
NCP
Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within
TEQ
Toxic Equivalency Quotient
QC - ACCEPTANCE CRITERIA RPD Duplicates: Global RPD Duplicates Acceptance Criteria is 30% however the following acceptance guidelines are equally applicable: Results <10 times the LOR : No Limit Results between 10-20 times the LOR : RPD must lie between 0-50% Results >20 times the LOR : RPD must lie between 0-30% Surrogate Recoveries : Recoveries must lie between 50-150% - Phenols 20-130%.
QC DATA GENERAL COMMENTS 1.
Where a result is reported as a less than (<), higher than the nominated LOR, this is due to either matrix interference, extract dilution required due to interferences or contaminant levels within
2.
Duplicate data shown within this report that states the word "BATCH" is a Batch Duplicate from outside of your sample batch, but within the laboratory sample batch at a 1:10 ratio. The Parent and Duplicate data shown is not data from your samples.
3.
Organochlorine Pesticide analysis - where reporting LCS data, Toxophene & Chlordane are not added to the LCS.
4.
Organochlorine Pesticide analysis - where reporting Spike data, Toxophene is not added to the Spike.
5.
Total Recoverable Hydrocarbons - where reporting Spike & LCS data, a single spike of commercial Hydrocarbon products in the range of C12-C30 is added and it's Total Recovery is reported in the C10-C14 cell of the Report.
6.
pH and Free Chlorine analysed in the laboratory - Analysis on this test must begin within 30 minutes of sampling.Therefore laboratory analysis is unlikely to be completed within holding time. Analysis will begin as soon as possible after sample receipt.
7.
Recovery Data (Spikes & Surrogates) - where chromatographic interference does not allow the determination of Recovery the term "INT" appears against that analyte.
8.
Polychlorinated Biphenyls are spiked only using Arochlor 1260 in Matrix Spikes and LCS's.
9.
For Matrix Spikes and LCS results a dash " -" in the report means that the specific analyte was not added to the QC sample.
the sample, high moisture content or insufficient sample provided.
10. Duplicate RPD's are calculated from raw analytical data thus it is possible to have two sets of data.
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 32 of 47 Report Number: 453692-S
Quality Control Results
Test
Acceptance Pass Qualifying Limits Limits Code
Units
Result 1
TRH C6-C9 TRH C10-C14 TRH C15-C28
mg/kg mg/kg mg/kg
< 20 < 20 < 50
20 20 50
Pass Pass Pass
TRH C29-C36 Method Blank BTEX
mg/kg
< 50
50
Pass
Benzene
mg/kg
< 0.1
0.1
Pass
Toluene Ethylbenzene m&p-Xylenes
mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.2
0.1 0.1 0.2
Pass Pass Pass
o-Xylene Xylenes - Total
mg/kg mg/kg
< 0.1 < 0.3
0.1 0.3
Pass Pass
Naphthalene TRH C6-C10
mg/kg mg/kg
< 0.5 < 20
0.5 20
Pass Pass
TRH C6-C10 less BTEX (F1) TRH >C10-C16 TRH >C16-C34
mg/kg mg/kg mg/kg
< 20 < 50 < 100
20 50 100
Pass Pass Pass
TRH >C34-C40
mg/kg
< 100
100
Pass
Method Blank Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Method Blank Total Recoverable Hydrocarbons - 2013 NEPM Fractions
Method Blank Polycyclic Aromatic Hydrocarbons Acenaphthene
mg/kg
< 0.5
0.5
Pass
Acenaphthylene Anthracene
mg/kg mg/kg
< 0.5 < 0.5
0.5 0.5
Pass Pass
Benz(a)anthracene
mg/kg
< 0.5
0.5
Pass
Benzo(a)pyrene Benzo(b&j)fluoranthene Benzo(g.h.i)perylene Benzo(k)fluoranthene Chrysene
mg/kg mg/kg mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5 < 0.5 < 0.5
0.5 0.5 0.5 0.5 0.5
Pass Pass Pass Pass Pass
Dibenz(a.h)anthracene
mg/kg
< 0.5
0.5
Pass
Fluoranthene Fluorene Indeno(1.2.3-cd)pyrene
mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5
0.5 0.5 0.5
Pass Pass Pass
Naphthalene Phenanthrene
mg/kg mg/kg
< 0.5 < 0.5
0.5 0.5
Pass Pass
Pyrene
mg/kg
< 0.5
0.5
Pass
Method Blank Organochlorine Pesticides Chlordanes - Total
mg/kg
< 0.1
0.1
Pass
4.4'-DDD
mg/kg
< 0.05
0.05
Pass
4.4'-DDE 4.4'-DDT a-BHC
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
0.05 0.05 0.05
Pass Pass Pass
Aldrin b-BHC
mg/kg mg/kg
< 0.05 < 0.05
0.05 0.05
Pass Pass
d-BHC
mg/kg
< 0.05
0.05
Pass
Dieldrin Endosulfan I
mg/kg mg/kg
< 0.05 < 0.05
0.05 0.05
Pass Pass
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 33 of 47 Report Number: 453692-S
Test
Acceptance Pass Qualifying Limits Limits Code 0.05 Pass
Units
Result 1
Endosulfan II
mg/kg
< 0.05
Endosulfan sulphate Endrin Endrin aldehyde
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
0.05 0.05 0.05
Pass Pass Pass
Endrin ketone
mg/kg
< 0.05
0.05
Pass
g-BHC (Lindane) Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor
mg/kg mg/kg mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05 < 0.05 < 0.05
0.05 0.05 0.05 0.05 0.05
Pass Pass Pass Pass Pass
Toxaphene
mg/kg
<1
1
Pass
Bolstar Chlorpyrifos Demeton-O
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2
0.2 0.2 0.2
Pass Pass Pass
Diazinon
mg/kg
< 0.2
0.2
Pass
Dichlorvos
mg/kg
< 0.2
0.2
Pass
Disulfoton Ethion
mg/kg mg/kg
< 0.2 < 0.2
0.2 0.2
Pass Pass
Ethoprop Fenitrothion Fensulfothion
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2
0.2 0.2 0.2
Pass Pass Pass
Fenthion
mg/kg
< 0.2
0.2
Pass
Merphos Methyl azinphos
mg/kg mg/kg
< 0.2 < 0.2
0.2 0.2
Pass Pass
Methyl parathion
mg/kg
< 0.2
0.2
Pass
Mevinphos Naled
mg/kg mg/kg
< 0.2 < 0.5
0.2 0.5
Pass Pass
Phorate
mg/kg
< 0.2
0.2
Pass
Ronnel Tokuthion
mg/kg mg/kg
< 0.2 < 0.2
0.2 0.2
Pass Pass
Trichloronate
mg/kg
< 0.2
0.2
Pass
Method Blank Organophosphorous Pesticides
Method Blank Polychlorinated Biphenyls Aroclor-1016
mg/kg
< 0.1
0.1
Pass
Aroclor-1221
mg/kg
< 0.1
0.1
Pass
Aroclor-1232 Aroclor-1242
mg/kg mg/kg
< 0.1 < 0.1
0.1 0.1
Pass Pass
Aroclor-1248 Aroclor-1254
mg/kg mg/kg
< 0.1 < 0.1
0.1 0.1
Pass Pass
Aroclor-1260 Total PCB*
mg/kg mg/kg
< 0.1 < 0.1
0.1 0.1
Pass Pass
Method Blank % Clay*
%
pass
1
N/A
Method Blank Heavy Metals Arsenic
mg/kg
<2
2
Pass
Cadmium Chromium Copper Iron
mg/kg mg/kg mg/kg mg/kg
< 0.4 <5 <5 <5
0.4 5 5 5
Pass Pass Pass Pass
Lead Mercury
mg/kg mg/kg
<5 < 0.1
5 0.1
Pass Pass
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 34 of 47 Report Number: 453692-S
Test
Acceptance Pass Qualifying Limits Limits Code 5 Pass
Units
Result 1
mg/kg
<5
mg/kg
<5
5
Pass
%
99
70-130
Pass
%
97
70-130
Pass
% %
103 102
70-130 70-130
Pass Pass
Ethylbenzene
%
106
70-130
Pass
m&p-Xylenes Xylenes - Total
% %
104 104
70-130 70-130
Pass Pass
Nickel Zinc LCS - % Recovery Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 TRH C10-C14 LCS - % Recovery BTEX Benzene Toluene
LCS - % Recovery Total Recoverable Hydrocarbons - 2013 NEPM Fractions Naphthalene
%
118
75-125
Pass
TRH C6-C10
%
100
70-130
Pass
TRH >C10-C16
%
96
70-130
Pass
% %
90 97
70-130 70-130
Pass Pass
Anthracene
%
97
70-130
Pass
Benz(a)anthracene
%
94
70-130
Pass
Benzo(a)pyrene Benzo(b&j)fluoranthene Benzo(g.h.i)perylene
% % %
103 105 87
70-130 70-130 70-130
Pass Pass Pass
Benzo(k)fluoranthene Chrysene
% %
96 93
70-130 70-130
Pass Pass
Dibenz(a.h)anthracene
%
96
70-130
Pass
Fluoranthene Fluorene Indeno(1.2.3-cd)pyrene
% % %
90 93 99
70-130 70-130 70-130
Pass Pass Pass
Naphthalene
%
93
70-130
Pass
Phenanthrene Pyrene
% %
87 92
70-130 70-130
Pass Pass
% % %
118 118 118
70-130 70-130 70-130
Pass Pass Pass
a-BHC Aldrin
% %
108 107
70-130 70-130
Pass Pass
b-BHC d-BHC
% %
126 121
70-130 70-130
Pass Pass
Dieldrin
%
102
70-130
Pass
Endosulfan I Endosulfan II
% %
109 112
70-130 70-130
Pass Pass
Endosulfan sulphate Endrin Endrin aldehyde
% % %
116 109 108
70-130 70-130 70-130
Pass Pass Pass
Endrin ketone
%
120
70-130
Pass
g-BHC (Lindane) Heptachlor
% %
114 129
70-130 70-130
Pass Pass
LCS - % Recovery Polycyclic Aromatic Hydrocarbons Acenaphthene Acenaphthylene
LCS - % Recovery Organochlorine Pesticides 4.4'-DDD 4.4'-DDE 4.4'-DDT
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 35 of 47 Report Number: 453692-S
Test
Acceptance Pass Qualifying Limits Limits Code 70-130 Pass
Units
Result 1
Heptachlor epoxide
%
109
Hexachlorobenzene Methoxychlor LCS - % Recovery
% %
98 117
70-130 70-130
Pass Pass
% % % % %
114 126 119 89 126
70-130 70-130 70-130 70-130 70-130
Pass Pass Pass Pass Pass
Polychlorinated Biphenyls Aroclor-1260
%
102
70-130
Pass
LCS - % Recovery Heavy Metals Arsenic
Organophosphorous Pesticides Diazinon Ethion Fenitrothion Methyl parathion Mevinphos LCS - % Recovery
%
106
80-120
Pass
Cadmium
%
102
80-120
Pass
Chromium
%
105
80-120
Pass
Copper Lead
% %
107 109
80-120 80-120
Pass Pass
Mercury Nickel Zinc
% % %
97 109 109
75-125 Pass 80-120 Pass 80-120 Pass Acceptance Pass Qualifying Limits Limits Code
Lab Sample ID
QA Source
Units
Result 1
B15-Ap07631
CP
%
Result 1 109
70-130
Pass
B15-Ap07631 B15-Ap07631
CP CP
% %
Result 1 82 75
75-125 75-125
Pass Pass
Copper
M15-Ap09017
NCP
%
78
75-125
Pass
Lead
M15-Ap09017
NCP
%
83
75-125
Pass
Mercury
B15-Ap07631
CP
%
108
70-130
Pass
Diazinon B15-Ap07632 CP Ethion B15-Ap07632 CP Fenitrothion B15-Ap07632 CP Methyl parathion B15-Ap07632 CP Mevinphos B15-Ap07632 CP Spike - % Recovery Total Recoverable Hydrocarbons - 1999 NEPM Fractions
% % % % %
70-130 70-130 70-130 70-130 70-130
Pass Pass Pass Pass Pass
TRH C6-C9 TRH C10-C14 Spike - % Recovery BTEX
70-130 70-130
Pass Pass
70-130 70-130
Pass Pass
Test Spike - % Recovery Polychlorinated Biphenyls Aroclor-1260 Spike - % Recovery Heavy Metals Arsenic Chromium
Spike - % Recovery Organophosphorous Pesticides
Benzene Toluene
Result 1 83 103 82 89 109 Result 1
B15-Ap07633 B15-Ap07633
CP CP
% %
B15-Ap07633 B15-Ap07633
CP CP
% %
87 87 Result 1 94 94
Ethylbenzene
B15-Ap07633
CP
%
96
70-130
Pass
m&p-Xylenes o-Xylene
B15-Ap07633 B15-Ap07633
CP CP
% %
100 97
70-130 70-130
Pass Pass
Xylenes - Total
B15-Ap07633
CP
%
99
70-130
Pass
Spike - % Recovery
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 36 of 47 Report Number: 453692-S
QA Source Total Recoverable Hydrocarbons - 2013 NEPM Fractions Test
Naphthalene TRH C6-C10 TRH >C10-C16
Lab Sample ID
Units
Result 1
Acceptance Pass Qualifying Limits Limits Code
Result 1
B15-Ap07633 B15-Ap07633 B15-Ap07633
CP CP CP
% % %
105 89 86
70-130 70-130 70-130
Pass Pass Pass
Polycyclic Aromatic Hydrocarbons Acenaphthene B15-Ap07639 Acenaphthylene B15-Ap07639
CP CP
% %
Result 1 90 83
70-130 70-130
Pass Pass
Spike - % Recovery
Anthracene Benz(a)anthracene
B15-Ap07639 B15-Ap07639
CP CP
% %
93 83
70-130 70-130
Pass Pass
Benzo(a)pyrene Benzo(b&j)fluoranthene
B15-Ap07639 B15-Ap07639
CP CP
% %
89 95
70-130 70-130
Pass Pass
Benzo(g.h.i)perylene Benzo(k)fluoranthene Chrysene
B15-Ap07639 B15-Ap07639 B15-Ap07639
CP CP CP
% % %
83 90 91
70-130 70-130 70-130
Pass Pass Pass
Dibenz(a.h)anthracene
B15-Ap07639
CP
%
104
70-130
Pass
Fluoranthene
B15-Ap07639
CP
%
73
70-130
Pass
Fluorene
B15-Ap07639
CP
%
86
70-130
Pass
Indeno(1.2.3-cd)pyrene
B15-Ap07639
CP
%
95
70-130
Pass
Naphthalene
B15-Ap07639
CP
%
87
70-130
Pass
Phenanthrene Pyrene
B15-Ap07639 B15-Ap07639
CP CP
% %
86 72
70-130 70-130
Pass Pass
B15-Ap07641
CP
%
Result 1 116
70-130
Pass
B15-Ap07642 B15-Ap07642
CP CP
% %
Result 1 104 114
70-130 70-130
Pass Pass
Fenitrothion
B15-Ap07642
CP
%
85
70-130
Pass
Methyl parathion
B15-Ap07642
CP
%
75
70-130
Pass
B15-Ap07642
CP
%
87
70-130
Pass
Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 B15-Ap07643 CP TRH C10-C14 B15-Ap07643 CP
% %
Result 1 75 93
70-130 70-130
Pass Pass
Spike - % Recovery BTEX Benzene
Spike - % Recovery Polychlorinated Biphenyls Aroclor-1260 Spike - % Recovery Organophosphorous Pesticides Diazinon Ethion
Mevinphos Spike - % Recovery
B15-Ap07643
CP
%
Result 1 80
70-130
Pass
B15-Ap07643
CP
%
86
70-130
Pass
B15-Ap07643
CP
%
89
70-130
Pass
B15-Ap07643 B15-Ap07643 B15-Ap07643
CP CP CP
% % %
94 91 93
70-130 70-130 70-130
Pass Pass Pass
Total Recoverable Hydrocarbons - 2013 NEPM Fractions Naphthalene B15-Ap07643 CP
%
Result 1 109
Toluene Ethylbenzene m&p-Xylenes o-Xylene Xylenes - Total Spike - % Recovery
70-130
Pass
B15-Ap07643
CP
%
76
70-130
Pass
B15-Ap07643
CP
%
92
70-130
Pass
4.4'-DDD
B15-Ap07645
CP
%
123
70-130
Pass
4.4'-DDE
B15-Ap07645
CP
%
113
70-130
Pass
4.4'-DDT
B15-Ap07645
CP
%
77
70-130
Pass
TRH C6-C10 TRH >C10-C16 Spike - % Recovery Organochlorine Pesticides
Result 1
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 37 of 47 Report Number: 453692-S
a-BHC
B15-Ap07645
QA Source CP
%
112
Aldrin
B15-Ap07645
CP
%
101
70-130
Pass
b-BHC d-BHC
B15-Ap07645 B15-Ap07645
CP CP
% %
114 99
70-130 70-130
Pass Pass
Dieldrin
B15-Ap07645
CP
%
100
70-130
Pass
Endosulfan I
B15-Ap07645
CP
%
90
70-130
Pass
Endosulfan II Endosulfan sulphate Endrin Endrin aldehyde
B15-Ap07645 B15-Ap07645 B15-Ap07645 B15-Ap07645
CP CP CP CP
% % % %
101 91 106 80
70-130 70-130 70-130 70-130
Pass Pass Pass Pass
Endrin ketone
B15-Ap07645
CP
%
126
70-130
Pass
g-BHC (Lindane)
B15-Ap07645
CP
%
106
70-130
Pass
Heptachlor
B15-Ap07645
CP
%
102
70-130
Pass
Heptachlor epoxide Hexachlorobenzene Methoxychlor
B15-Ap07645 B15-Ap07645 B15-Ap07645
CP CP CP
% % %
86 94 91
70-130 70-130 70-130
Pass Pass Pass
Acenaphthene Acenaphthylene Anthracene Benz(a)anthracene
B15-Ap07649 B15-Ap07649 B15-Ap07649 B15-Ap07649
CP CP CP CP
% % % %
70-130 70-130 70-130 70-130
Pass Pass Pass Pass
Benzo(a)pyrene
B15-Ap07649
CP
%
82
70-130
Pass
Benzo(b&j)fluoranthene
B15-Ap07649
CP
%
110
70-130
Pass
Benzo(g.h.i)perylene
B15-Ap07649
CP
%
74
70-130
Pass
Benzo(k)fluoranthene
B15-Ap07649
CP
%
85
70-130
Pass
Chrysene
B15-Ap07649
CP
%
88
70-130
Pass
Dibenz(a.h)anthracene Fluoranthene
B15-Ap07649 B15-Ap07649
CP CP
% %
89 71
70-130 70-130
Pass Pass
Fluorene
B15-Ap07649
CP
%
85
70-130
Pass
Indeno(1.2.3-cd)pyrene Naphthalene
B15-Ap07649 B15-Ap07649
CP CP
% %
87 87
70-130 70-130
Pass Pass
Phenanthrene
B15-Ap07649
CP
%
71
70-130
Pass
Pyrene
B15-Ap07649
CP
%
73
70-130
Pass
B15-Ap07651
CP
%
70-130
Pass
Arsenic
B15-Ap07651
CP
%
89
75-125
Pass
Cadmium
B15-Ap07651
CP
%
86
75-125
Pass
Chromium Mercury
B15-Ap07651 B15-Ap07651
CP CP
% %
87 108
75-125 70-130
Pass Pass
Test
Lab Sample ID
Units
Result 1
Spike - % Recovery Polycyclic Aromatic Hydrocarbons
Result 1
Spike - % Recovery Polychlorinated Biphenyls Aroclor-1260
Acceptance Pass Qualifying Limits Limits Code 70-130 Pass
81 88 83 90
Result 1
Spike - % Recovery Heavy Metals
114 Result 1
Nickel
B15-Ap07651
CP
%
86
75-125
Pass
Zinc
B15-Ap07651
CP
%
78
75-125
Pass
Diazinon
B15-Ap07652
CP
%
93
70-130
Pass
Ethion Fenitrothion Methyl parathion Mevinphos
B15-Ap07652 B15-Ap07652 B15-Ap07652 B15-Ap07652
CP CP CP CP
% % % %
118 90 76 80
70-130 70-130 70-130 70-130
Pass Pass Pass Pass
Spike - % Recovery Organophosphorous Pesticides
Result 1
Spike - % Recovery Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Result 1
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 38 of 47 Report Number: 453692-S
Units
Result 1
B15-Ap07719
QA Source CP
%
70
B15-Ap07719
CP
%
88
Benzene
B15-Ap07719
CP
%
77
70-130
Pass
Toluene
B15-Ap07719
CP
%
80
70-130
Pass
Ethylbenzene m&p-Xylenes o-Xylene Xylenes - Total
B15-Ap07719 B15-Ap07719 B15-Ap07719 B15-Ap07719
CP CP CP CP
% % % %
79 78 78 78
70-130 70-130 70-130 70-130
Pass Pass Pass Pass
Total Recoverable Hydrocarbons - 2013 NEPM Fractions Naphthalene B15-Ap07719 CP
%
Result 1 118
70-130
Pass
% %
70 81
Units
Result 1
Test TRH C6-C9 TRH C10-C14 Spike - % Recovery
Lab Sample ID
BTEX
Acceptance Pass Qualifying Limits Limits Code 70-130 Pass 70-130
Pass
Result 1
Spike - % Recovery
TRH C6-C10 TRH >C10-C16 Test
B15-Ap07719 B15-Ap07719 Lab Sample ID
CP CP QA Source
Duplicate Polycyclic Aromatic Hydrocarbons
70-130 Pass 70-130 Pass Acceptance Pass Qualifying Limits Limits Code
Result 1
Result 2
Acenaphthene
B15-Ap07631
CP
mg/kg
< 0.5
< 0.5
RPD <1
30%
Pass
Acenaphthylene Anthracene Benz(a)anthracene
B15-Ap07631 B15-Ap07631 B15-Ap07631
CP CP CP
mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
<1 <1 <1
30% 30% 30%
Pass Pass Pass
Benzo(a)pyrene Benzo(b&j)fluoranthene
B15-Ap07631 B15-Ap07631
CP CP
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
<1 <1
30% 30%
Pass Pass
Benzo(g.h.i)perylene
B15-Ap07631
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Benzo(k)fluoranthene
B15-Ap07631
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Chrysene
B15-Ap07631
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Dibenz(a.h)anthracene
B15-Ap07631
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Fluoranthene
B15-Ap07631
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Fluorene Indeno(1.2.3-cd)pyrene
B15-Ap07631 B15-Ap07631
CP CP
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
<1 <1
30% 30%
Pass Pass
Naphthalene
B15-Ap07631
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Phenanthrene Pyrene
B15-Ap07631 B15-Ap07631
CP CP
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
<1 <1
30% 30%
Pass Pass
B15-Ap07631 B15-Ap07631 B15-Ap07631
CP CP CP
mg/kg mg/kg mg/kg
Result 1 < 0.2 < 0.2 < 0.2
Result 2 < 0.2 < 0.2 < 0.2
RPD <1 <1 <1
30% 30% 30%
Pass Pass Pass
Duplicate Organophosphorous Pesticides Bolstar Chlorpyrifos Demeton-O Diazinon
B15-Ap07631
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Dichlorvos
B15-Ap07631
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Disulfoton
B15-Ap07631
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Ethion
B15-Ap07631
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Ethoprop Fenitrothion Fensulfothion
B15-Ap07631 B15-Ap07631 B15-Ap07631
CP CP CP
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
<1 <1 <1
30% 30% 30%
Pass Pass Pass
Fenthion
B15-Ap07631
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Merphos
B15-Ap07631
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Methyl azinphos
B15-Ap07631
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Methyl parathion
B15-Ap07631
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Mevinphos Naled Phorate
B15-Ap07631 B15-Ap07631 B15-Ap07631
CP CP CP
mg/kg mg/kg mg/kg
< 0.2 < 0.5 < 0.2
< 0.2 < 0.5 < 0.2
<1 <1 <1
30% 30% 30%
Pass Pass Pass
Ronnel
B15-Ap07631
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 39 of 47 Report Number: 453692-S
Duplicate Organophosphorous Pesticides Tokuthion
B15-Ap07631
CP
mg/kg
Result 1 < 0.2
Result 2 < 0.2
RPD <1
30%
Pass
B15-Ap07631
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
B15-Ma14573
NCP
%
Result 1 55
Result 2 53
RPD 5.0
30%
Pass
S15-Ap07539 M15-Ap07868
NCP NCP
uS/cm pH Units
550 8.0
540 8.0
<1 pass
30% 30%
Pass Pass
Result 1
Result 2
RPD
Arsenic
B15-Ap07631
CP
mg/kg
6.4
6.2
3.0
30%
Pass
Cadmium
B15-Ap07631
CP
mg/kg
< 0.4
< 0.4
<1
30%
Pass
Chromium
B15-Ap07631
CP
mg/kg
11
11
2.0
30%
Pass
Copper Iron Lead
B15-Ap07631 B15-Ap07631 B15-Ap07631
CP CP CP
mg/kg mg/kg mg/kg
9.8 20000 37
9.8 19000 38
<1 <1 3.0
30% 30% 30%
Pass Pass Pass
Mercury
B15-Ap07631
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
Nickel
B15-Ap07631
CP
mg/kg
8.0
8.3
3.0
30%
Pass
Zinc B15-Ap07631 CP Duplicate Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 B15-Ap07632 CP
mg/kg
41
42
4.0
30%
Pass
mg/kg
Result 1 < 20
Result 2 < 20
RPD <1
30%
Pass
< 20 < 50 < 50
< 20 < 50 < 50
<1 <1 <1
30% 30% 30%
Pass Pass Pass
Trichloronate Duplicate % Clay* Conductivity (1:5 aqueous extract at 25째C) pH (1:5 Aqueous extract) Duplicate Heavy Metals
TRH C10-C14 TRH C15-C28 TRH C29-C36
B15-Ap07632 B15-Ap07632 B15-Ap07632
CP CP CP
mg/kg mg/kg mg/kg
Result 1
Result 2
RPD
Benzene Toluene Ethylbenzene
B15-Ap07632 B15-Ap07632 B15-Ap07632
CP CP CP
mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
<1 <1 <1
30% 30% 30%
Pass Pass Pass
m&p-Xylenes o-Xylene
B15-Ap07632 B15-Ap07632
CP CP
mg/kg mg/kg
< 0.2 < 0.1
< 0.2 < 0.1
<1 <1
30% 30%
Pass Pass
Xylenes - Total
B15-Ap07632
Duplicate BTEX
CP
mg/kg
< 0.3
< 0.3
<1
30%
Pass
Duplicate Total Recoverable Hydrocarbons - 2013 NEPM Fractions Naphthalene B15-Ap07632 CP TRH C6-C10 B15-Ap07632 CP TRH C6-C10 less BTEX (F1) B15-Ap07632 CP TRH >C10-C16 B15-Ap07632 CP TRH >C16-C34 B15-Ap07632 CP TRH >C34-C40 B15-Ap07632 CP
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
Result 1 < 0.5 < 20 < 20 < 50 < 100 < 100
Result 2 < 0.5 < 20 < 20 < 50 < 100 < 100
RPD <1 <1 <1 <1 <1 <1
30% 30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass Pass
Duplicate Organochlorine Pesticides Chlordanes - Total 4.4'-DDD 4.4'-DDE 4.4'-DDT
B15-Ap07634 B15-Ap07634 B15-Ap07634 B15-Ap07634
CP CP CP CP
mg/kg mg/kg mg/kg mg/kg
Result 1 < 0.1 < 0.05 < 0.05 < 0.05
Result 2 < 0.1 < 0.05 < 0.05 < 0.05
RPD <1 <1 <1 <1
30% 30% 30% 30%
Pass Pass Pass Pass
a-BHC
B15-Ap07634
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Aldrin b-BHC d-BHC
B15-Ap07634 B15-Ap07634 B15-Ap07634
CP CP CP
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
<1 <1 <1
30% 30% 30%
Pass Pass Pass
Dieldrin
B15-Ap07634
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Endosulfan I
B15-Ap07634
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Endosulfan II
B15-Ap07634
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 40 of 47 Report Number: 453692-S
Duplicate Organochlorine Pesticides Endosulfan sulphate Endrin
B15-Ap07634
CP
mg/kg
Result 1 < 0.05
Result 2 < 0.05
RPD <1
30%
Pass
B15-Ap07634
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Endrin aldehyde
B15-Ap07634
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Endrin ketone g-BHC (Lindane)
B15-Ap07634 B15-Ap07634
CP CP
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
<1 <1
30% 30%
Pass Pass
Heptachlor Heptachlor epoxide
B15-Ap07634 B15-Ap07634
CP CP
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
<1 <1
30% 30%
Pass Pass
Hexachlorobenzene
B15-Ap07634
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Methoxychlor
B15-Ap07634
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
B15-Ap07634
CP
mg/kg
<1
<1
<1
30%
Pass
B15-Ap07634
CP
mg/kg
Result 1 < 0.1
Result 2 < 0.1
RPD <1
30%
Pass
Aroclor-1221
B15-Ap07634
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
Aroclor-1232
B15-Ap07634
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
Aroclor-1242 Aroclor-1248
B15-Ap07634 B15-Ap07634
CP CP
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
<1 <1
30% 30%
Pass Pass
Aroclor-1254 Aroclor-1260 Total PCB*
B15-Ap07634 B15-Ap07634 B15-Ap07634
CP CP CP
mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
<1 <1 <1
30% 30% 30%
Pass Pass Pass
Polycyclic Aromatic Hydrocarbons Acenaphthene B15-Ap07638 Acenaphthylene B15-Ap07638
CP CP
mg/kg mg/kg
Result 1 < 0.5 < 0.5
Result 2 < 0.5 < 0.5
RPD <1 <1
30% 30%
Pass Pass
Toxaphene Duplicate Polychlorinated Biphenyls Aroclor-1016
Duplicate
Anthracene Benz(a)anthracene
B15-Ap07638 B15-Ap07638
CP CP
mg/kg mg/kg
< 0.5 < 0.5
< 0.5 < 0.5
<1 <1
30% 30%
Pass Pass
Benzo(a)pyrene Benzo(b&j)fluoranthene Benzo(g.h.i)perylene
B15-Ap07638 B15-Ap07638 B15-Ap07638
CP CP CP
mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5
<1 <1 <1
30% 30% 30%
Pass Pass Pass
Benzo(k)fluoranthene Chrysene Dibenz(a.h)anthracene Fluoranthene Fluorene
B15-Ap07638 B15-Ap07638 B15-Ap07638 B15-Ap07638 B15-Ap07638
CP CP CP CP CP
mg/kg mg/kg mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5 < 0.5 < 0.5
< 0.5 < 0.5 < 0.5 < 0.5 < 0.5
<1 <1 <1 <1 <1
30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass
Indeno(1.2.3-cd)pyrene
B15-Ap07638
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Naphthalene
B15-Ap07638
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Phenanthrene
B15-Ap07638
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Pyrene
B15-Ap07638
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
B15-Ap07638
CP
mg/kg
Result 1 < 0.2
Result 2 < 0.2
RPD <1
30%
Pass
Chlorpyrifos
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Demeton-O
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Diazinon
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Dichlorvos
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Disulfoton
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Ethion Ethoprop Fenitrothion
B15-Ap07638 B15-Ap07638 B15-Ap07638
CP CP CP
mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2
<1 <1 <1
30% 30% 30%
Pass Pass Pass
Fensulfothion
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Fenthion
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Merphos
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Methyl azinphos
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Methyl parathion
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Duplicate Organophosphorous Pesticides Bolstar
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 41 of 47 Report Number: 453692-S
Duplicate Organophosphorous Pesticides Mevinphos
B15-Ap07638
CP
mg/kg
Result 1 < 0.2
Result 2 < 0.2
RPD <1
30%
Pass
Naled
B15-Ap07638
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Phorate
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Ronnel Tokuthion
B15-Ap07638 B15-Ap07638
CP CP
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
<1 <1
30% 30%
Pass Pass
B15-Ap07638
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Result 1
Result 2
RPD
Chlordanes - Total
B15-Ap07640
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
4.4'-DDD
B15-Ap07640
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
4.4'-DDE 4.4'-DDT
B15-Ap07640 B15-Ap07640
CP CP
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
<1 <1
30% 30%
Pass Pass
a-BHC
B15-Ap07640
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Aldrin
B15-Ap07640
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
b-BHC
B15-Ap07640
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
d-BHC
B15-Ap07640
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Dieldrin
B15-Ap07640
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Endosulfan I Endosulfan II
B15-Ap07640 B15-Ap07640
CP CP
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
<1 <1
30% 30%
Pass Pass
Endosulfan sulphate
B15-Ap07640
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Endrin
B15-Ap07640
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Endrin aldehyde Endrin ketone g-BHC (Lindane)
B15-Ap07640 B15-Ap07640 B15-Ap07640
CP CP CP
mg/kg mg/kg mg/kg
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
<1 <1 <1
30% 30% 30%
Pass Pass Pass
Heptachlor
B15-Ap07640
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Heptachlor epoxide Hexachlorobenzene
B15-Ap07640 B15-Ap07640
CP CP
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
<1 <1
30% 30%
Pass Pass
Methoxychlor
B15-Ap07640
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
B15-Ap07640
CP
mg/kg
<1
<1
<1
30%
Pass
B15-Ap07640
CP
mg/kg
Result 1 < 0.1
Result 2 < 0.1
RPD <1
30%
Pass
B15-Ap07640 B15-Ap07640 B15-Ap07640 B15-Ap07640 B15-Ap07640 B15-Ap07640 B15-Ap07640
CP CP CP CP CP CP CP
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1
<1 <1 <1 <1 <1 <1 <1
30% 30% 30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass Pass Pass
B15-Ap07640
CP
%
Result 1 8.2
Result 2 8.3
RPD 1.0
30%
Pass
B15-Ap07640
CP
mg/kg
Result 1 5.4
Result 2 4.1
RPD 29
30%
Pass
Cadmium
B15-Ap07640
CP
mg/kg
< 0.4
< 0.4
<1
30%
Pass
Chromium Copper
B15-Ap07640 B15-Ap07640
CP CP
mg/kg mg/kg
12 9.6
12 9.5
1.0 2.0
30% 30%
Pass Pass
Lead
B15-Ap07640
CP
mg/kg
5.1
<5
6.0
30%
Pass
Mercury
B15-Ap07640
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
Trichloronate Duplicate Organochlorine Pesticides
Toxaphene Duplicate Polychlorinated Biphenyls Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260 Total PCB* Duplicate % Moisture Duplicate Heavy Metals Arsenic
Nickel
B15-Ap07640
CP
mg/kg
8.6
8.6
1.0
30%
Pass
Zinc
B15-Ap07640
CP
mg/kg
32
29
11
30%
Pass
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 42 of 47 Report Number: 453692-S
Duplicate Heavy Metals Arsenic
B15-Ap07641
CP
mg/kg
Result 1 <2
Result 2 2.6
RPD 53
30%
Fail
Cadmium
B15-Ap07641
CP
mg/kg
7.7
7.5
3.0
30%
Pass
Chromium
B15-Ap07641
CP
mg/kg
20
19
3.0
30%
Pass
Copper Lead
B15-Ap07641 B15-Ap07641
CP CP
mg/kg mg/kg
28 380
27 390
2.0 3.0
30% 30%
Pass Pass
Mercury Nickel
B15-Ap07641 B15-Ap07641
CP CP
mg/kg mg/kg
0.2 10
0.2 10
11 1.0
30% 30%
Pass Pass
Zinc
B15-Ap07641
CP
mg/kg
17000
17000
3.0
30%
Pass
Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 B15-Ap07642 CP TRH C10-C14 B15-Ap07642 CP TRH C15-C28 B15-Ap07642 CP TRH C29-C36 B15-Ap07642 CP
mg/kg mg/kg mg/kg mg/kg
Result 1 < 20 < 20 < 50 < 50
Result 2 < 20 < 20 < 50 < 50
RPD <1 <1 <1 <1
30% 30% 30% 30%
Pass Pass Pass Pass
Q15
Duplicate
Duplicate BTEX Benzene
B15-Ap07642
CP
mg/kg
Result 1 < 0.1
Result 2 < 0.1
RPD <1
30%
Pass
Toluene Ethylbenzene m&p-Xylenes
B15-Ap07642 B15-Ap07642 B15-Ap07642
CP CP CP
mg/kg mg/kg mg/kg
< 0.1 < 0.1 < 0.2
< 0.1 < 0.1 < 0.2
<1 <1 <1
30% 30% 30%
Pass Pass Pass
o-Xylene
B15-Ap07642
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
B15-Ap07642
CP
mg/kg
< 0.3
< 0.3
<1
30%
Pass
Xylenes - Total Duplicate
Total Recoverable Hydrocarbons - 2013 NEPM Fractions
Result 1
Result 2
RPD
Naphthalene
B15-Ap07642
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
TRH C6-C10 TRH C6-C10 less BTEX (F1)
B15-Ap07642 B15-Ap07642
CP CP
mg/kg mg/kg
< 20 < 20
< 20 < 20
<1 <1
30% 30%
Pass Pass
TRH >C10-C16
B15-Ap07642
CP
mg/kg
< 50
< 50
<1
30%
Pass
TRH >C16-C34
B15-Ap07642
CP
mg/kg
< 100
< 100
<1
30%
Pass
B15-Ap07642
CP
mg/kg
< 100
< 100
<1
30%
Pass
Result 1
Result 2
RPD
Chlordanes - Total 4.4'-DDD 4.4'-DDE 4.4'-DDT a-BHC Aldrin b-BHC d-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan sulphate Endrin Endrin aldehyde Endrin ketone g-BHC (Lindane)
B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644 B15-Ap07644
CP CP CP CP CP CP CP CP CP CP CP CP CP CP CP CP
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
< 0.1 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05
< 0.1 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05
<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1
30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass
Heptachlor
B15-Ap07644
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Heptachlor epoxide
B15-Ap07644
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Hexachlorobenzene
B15-Ap07644
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Methoxychlor
B15-Ap07644
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Toxaphene
B15-Ap07644
CP
mg/kg
<1
<1
<1
30%
Pass
TRH >C34-C40 Duplicate Organochlorine Pesticides
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 43 of 47 Report Number: 453692-S
Duplicate Polychlorinated Biphenyls Aroclor-1016
B15-Ap07644
CP
mg/kg
Result 1 < 0.1
Result 2 < 0.1
RPD <1
30%
Pass
Aroclor-1221
B15-Ap07644
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
Aroclor-1232
B15-Ap07644
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
Aroclor-1242 Aroclor-1248
B15-Ap07644 B15-Ap07644
CP CP
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
<1 <1
30% 30%
Pass Pass
Aroclor-1254 Aroclor-1260
B15-Ap07644 B15-Ap07644
CP CP
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
<1 <1
30% 30%
Pass Pass
Total PCB*
B15-Ap07644
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
Polycyclic Aromatic Hydrocarbons Acenaphthene Acenaphthylene Anthracene Benz(a)anthracene Benzo(a)pyrene Benzo(b&j)fluoranthene Benzo(g.h.i)perylene Benzo(k)fluoranthene Chrysene Dibenz(a.h)anthracene Fluoranthene Fluorene Indeno(1.2.3-cd)pyrene Naphthalene Phenanthrene Pyrene
B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648
CP CP CP CP CP CP CP CP CP CP CP CP CP CP CP CP
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
Result 1 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
Result 2 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
RPD <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1
30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass
Duplicate Organophosphorous Pesticides Bolstar
B15-Ap07648
CP
mg/kg
Result 1 < 0.2
Result 2 < 0.2
RPD <1
30%
Pass
Chlorpyrifos
B15-Ap07648
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Demeton-O
B15-Ap07648
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Diazinon
B15-Ap07648
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Dichlorvos Disulfoton
B15-Ap07648 B15-Ap07648
CP CP
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
<1 <1
30% 30%
Pass Pass
Ethion
B15-Ap07648
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Ethoprop
B15-Ap07648
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Fenitrothion
B15-Ap07648
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Fensulfothion
B15-Ap07648
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Duplicate
Fenthion
B15-Ap07648
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648 B15-Ap07648
CP CP CP CP CP CP CP CP CP
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
< 0.2 < 0.2 < 0.2 < 0.2 < 0.5 < 0.2 < 0.2 < 0.2 < 0.2
< 0.2 < 0.2 < 0.2 < 0.2 < 0.5 < 0.2 < 0.2 < 0.2 < 0.2
<1 <1 <1 <1 <1 <1 <1 <1 <1
30% 30% 30% 30% 30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass Pass Pass Pass Pass
B15-Ap07650
CP
mg/kg
Result 1 < 0.1
Result 2 < 0.1
RPD <1
30%
Pass
4.4'-DDD
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
4.4'-DDE
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
4.4'-DDT
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Merphos Methyl azinphos Methyl parathion Mevinphos Naled Phorate Ronnel Tokuthion Trichloronate Duplicate Organochlorine Pesticides Chlordanes - Total
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 44 of 47 Report Number: 453692-S
Duplicate Organochlorine Pesticides a-BHC
B15-Ap07650
CP
mg/kg
Result 1 < 0.05
Result 2 < 0.05
RPD <1
30%
Pass
Aldrin
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
b-BHC
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
d-BHC Dieldrin
B15-Ap07650 B15-Ap07650
CP CP
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
<1 <1
30% 30%
Pass Pass
Endosulfan I Endosulfan II
B15-Ap07650 B15-Ap07650
CP CP
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
<1 <1
30% 30%
Pass Pass
Endosulfan sulphate
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Endrin
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Endrin aldehyde
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Endrin ketone g-BHC (Lindane)
B15-Ap07650 B15-Ap07650
CP CP
mg/kg mg/kg
< 0.05 < 0.05
< 0.05 < 0.05
<1 <1
30% 30%
Pass Pass
Heptachlor
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Heptachlor epoxide
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Hexachlorobenzene
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
Methoxychlor
B15-Ap07650
CP
mg/kg
< 0.05
< 0.05
<1
30%
Pass
B15-Ap07650
CP
mg/kg
<1
<1
<1
30%
Pass
B15-Ap07650
CP
mg/kg
Result 1 < 0.1
Result 2 < 0.1
RPD <1
30%
Pass
Aroclor-1221
B15-Ap07650
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
Aroclor-1232
B15-Ap07650
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
Aroclor-1242 Aroclor-1248
B15-Ap07650 B15-Ap07650
CP CP
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
<1 <1
30% 30%
Pass Pass
Aroclor-1254
B15-Ap07650
CP
mg/kg
< 0.1
< 0.1
<1
30%
Pass
Aroclor-1260 Total PCB* Duplicate
B15-Ap07650 B15-Ap07650
CP CP
mg/kg mg/kg
< 0.1 < 0.1
< 0.1 < 0.1
<1 <1
30% 30%
Pass Pass
Result 1
Result 2
RPD
% Moisture Duplicate Heavy Metals
B15-Ap07650
CP
%
23
25
8.0
30%
Pass
Result 1
Result 2
RPD
Mercury B15-Ap07650 Duplicate Polycyclic Aromatic Hydrocarbons
CP
mg/kg
0.2
0.2
19
30%
Pass
30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass
Toxaphene Duplicate Polychlorinated Biphenyls Aroclor-1016
Result 1
Result 2
RPD
Acenaphthene Acenaphthylene Anthracene Benz(a)anthracene Benzo(a)pyrene Benzo(b&j)fluoranthene Benzo(g.h.i)perylene Benzo(k)fluoranthene Chrysene Dibenz(a.h)anthracene Fluoranthene Fluorene Indeno(1.2.3-cd)pyrene
B15-Ap07651 B15-Ap07651 B15-Ap07651 B15-Ap07651 B15-Ap07651 B15-Ap07651 B15-Ap07651 B15-Ap07651 B15-Ap07651 B15-Ap07651 B15-Ap07651 B15-Ap07651 B15-Ap07651
CP CP CP CP CP CP CP CP CP CP CP CP CP
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
< 0.5 < 0.5 < 0.5 0.7 0.9 0.8 0.5 0.8 0.8 < 0.5 1.3 < 0.5 0.5
< 0.5 < 0.5 < 0.5 0.8 1.0 0.9 0.5 1.0 0.8 < 0.5 1.4 < 0.5 0.6
<1 <1 <1 13 12 16 6.0 29 10 <1 9.0 <1 6.0
Naphthalene
B15-Ap07651
CP
mg/kg
< 0.5
< 0.5
<1
30%
Phenanthrene
B15-Ap07651
CP
mg/kg
0.5
0.7
32
30%
Fail
Pyrene
B15-Ap07651
CP
mg/kg
1.2
1.3
10
30%
Pass
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Q15
Page 45 of 47 Report Number: 453692-S
Duplicate Organophosphorous Pesticides Bolstar
B15-Ap07651
CP
mg/kg
Result 1 < 0.2
Result 2 < 0.2
RPD <1
30%
Pass
Chlorpyrifos
B15-Ap07651
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Demeton-O
B15-Ap07651
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Diazinon Dichlorvos
B15-Ap07651 B15-Ap07651
CP CP
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
<1 <1
30% 30%
Pass Pass
Disulfoton Ethion
B15-Ap07651 B15-Ap07651
CP CP
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
<1 <1
30% 30%
Pass Pass
Ethoprop
B15-Ap07651
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Fenitrothion
B15-Ap07651
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Fensulfothion
B15-Ap07651
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Fenthion Merphos
B15-Ap07651 B15-Ap07651
CP CP
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
<1 <1
30% 30%
Pass Pass
Methyl azinphos
B15-Ap07651
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Methyl parathion
B15-Ap07651
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Mevinphos
B15-Ap07651
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Naled
B15-Ap07651
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
Phorate
B15-Ap07651
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
Ronnel Tokuthion
B15-Ap07651 B15-Ap07651
CP CP
mg/kg mg/kg
< 0.2 < 0.2
< 0.2 < 0.2
<1 <1
30% 30%
Pass Pass
B15-Ap07651
CP
mg/kg
< 0.2
< 0.2
<1
30%
Pass
B15-Ap07651 B15-Ap07651
CP CP
mg/kg mg/kg
Result 1 7.8 < 0.4
Result 2 6.5 < 0.4
RPD 18 <1
30% 30%
Pass Pass
Chromium Copper
B15-Ap07651 B15-Ap07651
CP CP
mg/kg mg/kg
14 170
13 170
1.0 1.0
30% 30%
Pass Pass
Lead Mercury Nickel
B15-Ap07651 B15-Ap07651 B15-Ap07651
CP CP CP
mg/kg mg/kg mg/kg
440 0.2 12
440 0.2 12
1.0 <1 1.0
30% 30% 30%
Pass Pass Pass
Zinc
B15-Ap07651
CP
mg/kg
170
150
17
30%
Pass
Result 1
Result 2
RPD
< 20
< 20
<1
30%
Pass
Result 1
Result 2
RPD
< 0.1 < 0.1 < 0.1 < 0.2 < 0.1 < 0.3
< 0.1 < 0.1 < 0.1 < 0.2 < 0.1 < 0.3
<1 <1 <1 <1 <1 <1
30% 30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass Pass
Trichloronate Duplicate Heavy Metals Arsenic Cadmium
Duplicate Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 Duplicate BTEX
B15-Ap07652
CP
mg/kg
Benzene Toluene Ethylbenzene m&p-Xylenes o-Xylene Xylenes - Total Duplicate
B15-Ap07652 B15-Ap07652 B15-Ap07652 B15-Ap07652 B15-Ap07652 B15-Ap07652
CP CP CP CP CP CP
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
Total Recoverable Hydrocarbons - 2013 NEPM Fractions
Result 1
Result 2
RPD
Naphthalene
B15-Ap07652
CP
mg/kg
< 0.5
< 0.5
<1
30%
Pass
TRH C6-C10
B15-Ap07652
CP
mg/kg
< 20
< 20
<1
30%
Pass
TRH C6-C10 less BTEX (F1)
B15-Ap07652
CP
mg/kg
< 20
< 20
<1
30%
Pass
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 46 of 47 Report Number: 453692-S
Comments Sample Integrity Custody Seals Intact (if used)
N/A
Attempt to Chill was evident
Yes
Sample correctly preserved
Yes
Appropriate sample containers have been used
Yes
Sample containers for volatile analysis received with minimal headspace
Yes
Samples received within HoldingTime
Yes
Some samples have been subcontracted
No
Qualifier Codes/Comments Code Description N01
F2 is determined by arithmetically subtracting the "naphthalene" value from the ">C10-C16" value. The naphthalene value used in this calculation is obtained from volatiles (Purge & Trap analysis).
N02
Where we have reported both volatile (P&T GCMS) and semivolatile (GCMS) naphthalene data, results may not be identical. Provided correct sample handling protocols have been followed, any observed differences in results are likely to be due to procedural differences within each methodology. Results determined by both techniques have passed all QAQC acceptance criteria, and are entirely technically valid.
N04
F1 is determined by arithmetically subtracting the "Total BTEX" value from the "C6-C10" value. The "Total BTEX" value is obtained by summing the concentrations of BTEX analytes. The "C6-C10" value is obtained by quantitating against a standard of mixed aromatic/aliphatic analytes.
N07
Please note:- These two PAH isomers closely co-elute using the most contemporary analytical methods and both the reported concentration (and the TEQ) apply specifically to the total of the two co-eluting PAHs
Q15
The RPD reported passes Eurofins | mgt's Acceptance Criteria as stipulated in SOP 05. Refer to Glossary Page of this report for further details
Authorised By Sarah Gould
Analytical Services Manager
Carroll Lee
Senior Analyst-Organic (VIC)
Carroll Lee
Senior Analyst-Volatile (VIC)
Emily Rosenberg
Senior Analyst-Metal (VIC)
Huong Le
Senior Analyst-Inorganic (VIC)
Richard Corner
Senior Analyst-Inorganic (QLD)
Glenn Jackson National Laboratory Manager - Indicates Not Requested * Indicates NATA accreditation does not cover the performance of this service Uncertainty data is available on request Eurofins | mgt shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretation given in this report. In no case shall Eurofins | mgt be liable for consequential damages including, but not limited to, lost profits, damages for failure to meet deadlines and lost production arising from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 47 of 47 Report Number: 453692-S
Certificate of Analysis NATA Accredited Accreditation Number 1261 Site Number 1254
PRENSA QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Accredited for compliance with ISO/IEC 17025. The results of the tests, calibrations and/or measurements included in this document are traceable to Australian/national standards.
Attention:
John Scott
Report
453692-W
Project name
DSI
Project ID
53217
Received Date
Apr 10, 2015
Sample Matrix
53217TB1_080415 Water
53217R1_080415 Water
53217R2_090415 Water
Eurofins | mgt Sample No.
B15-Ap07653
B15-Ap07655
B15-Ap07657
Apr 08, 2015
Apr 08, 2015
Apr 09, 2015
Client Sample ID
Date Sampled Test/Reference LOR Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Unit
TRH C6-C9
0.02
mg/L
-
< 0.02
< 0.02
TRH C10-C14
0.05
mg/L
-
< 0.05
< 0.05
TRH C15-C28 TRH C29-C36 TRH C10-36 (Total)
0.1 0.1 0.1
mg/L mg/L mg/L
-
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
Total Recoverable Hydrocarbons - 2013 NEPM Fractions NaphthaleneN02 TRH C6-C10
0.02 0.02
mg/L mg/L
< 0.02 < 0.02
< 0.02 < 0.02
< 0.02 < 0.02
TRH C6-C10 less BTEX (F1)N04
0.02
mg/L
-
< 0.02
< 0.02
TRH >C10-C16
0.05
mg/L
-
< 0.05
< 0.05
TRH >C10-C16 less Naphthalene (F2)N01 TRH >C16-C34 TRH >C34-C40 BTEX
0.05 0.1 0.1
mg/L mg/L mg/L
-
< 0.05 < 0.1 < 0.1
< 0.05 < 0.1 < 0.1
Benzene
0.001
mg/L
< 0.001
< 0.001
< 0.001
Toluene
0.001
mg/L
< 0.001
< 0.001
< 0.001
Ethylbenzene m&p-Xylenes o-Xylene
0.001 0.002 0.001
mg/L mg/L mg/L
< 0.001 < 0.002 < 0.001
< 0.001 < 0.002 < 0.001
< 0.001 < 0.002 < 0.001
Xylenes - Total 4-Bromofluorobenzene (surr.)
0.003 1
mg/L %
< 0.003 97
< 0.003 108
< 0.003 101
Acenaphthene
0.001
mg/L
-
< 0.001
< 0.001
Acenaphthylene Anthracene
0.001 0.001
mg/L mg/L
-
< 0.001 < 0.001
< 0.001 < 0.001
Benz(a)anthracene Benzo(a)pyrene
0.001 0.001
mg/L mg/L
-
< 0.001 < 0.001
< 0.001 < 0.001
Benzo(b&j)fluorantheneN07 Benzo(g.h.i)perylene
0.001 0.001
mg/L mg/L
-
< 0.001 < 0.001
< 0.001 < 0.001
Benzo(k)fluoranthene
0.001
mg/L
-
< 0.001
< 0.001
Chrysene Dibenz(a.h)anthracene Fluoranthene
0.001 0.001 0.001
mg/L mg/L mg/L
-
< 0.001 < 0.001 < 0.001
< 0.001 < 0.001 < 0.001
Fluorene Indeno(1.2.3-cd)pyrene
0.001 0.001
mg/L mg/L
-
< 0.001 < 0.001
< 0.001 < 0.001
Polycyclic Aromatic Hydrocarbons
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 1 of 24 Report Number: 453692-W
Sample Matrix
53217TB1_080415 Water
53217R1_080415 Water
53217R2_090415 Water
Eurofins | mgt Sample No.
B15-Ap07653
B15-Ap07655
B15-Ap07657
Apr 08, 2015
Apr 08, 2015
Apr 09, 2015
Client Sample ID
Date Sampled Test/Reference Polycyclic Aromatic Hydrocarbons
LOR
Unit
Naphthalene Phenanthrene
0.001 0.001
mg/L mg/L
-
< 0.001 < 0.001
< 0.001 < 0.001
Pyrene
0.001
mg/L
-
< 0.001
< 0.001
Total PAH* 2-Fluorobiphenyl (surr.)
0.001 1
mg/L %
-
< 0.001 60
< 0.001 126
p-Terphenyl-d14 (surr.) Heavy Metals
1
%
-
76
145
Arsenic
0.001
mg/L
-
< 0.001
< 0.001
Cadmium Chromium
0.0002 0.001
mg/L mg/L
-
< 0.0002 < 0.001
< 0.0002 < 0.001
Copper Lead Mercury
0.001 0.001 0.0001
mg/L mg/L mg/L
-
< 0.001 < 0.001 < 0.0001
< 0.001 < 0.001 < 0.0001
Nickel
0.001
mg/L
-
< 0.001
< 0.001
Zinc
0.001
mg/L
-
< 0.001
< 0.001
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 2 of 24 Report Number: 453692-W
Sample History Where samples are submitted/analysed over several days, the last date of extraction and analysis is reported. A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this, some of the method reference information on reports has changed. However, no substantive change has been made to our laboratory methods, and as such there is no change in the validity of current or previous results (regarding both quality and NATA accreditation). If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised results should testing be performed outside the recommended holding time.
Description
Testing Site
Extracted
Holding Time
Eurofins | mgt Suite 7 Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Melbourne
Apr 15, 2015
7 Day
Melbourne
Apr 15, 2015
7 Day
Melbourne
Apr 15, 2015
7 Day
Melbourne
Apr 13, 2015
28 Day
Brisbane
Apr 13, 2015
14 Day
Brisbane
Apr 13, 2015
14 Day
- Method: TRH C6-C36 - LTM-ORG-2010
Total Recoverable Hydrocarbons - 2013 NEPM Fractions - Method: TRH C6-C40 - LTM-ORG-2010
Polycyclic Aromatic Hydrocarbons - Method: USEPA 8270 Polycyclic Aromatic Hydrocarbons
Metals M8 - Method: USEPA 6010/6020 Heavy Metals & USEPA 7470/71 Mercury
BTEX and Naphthalene Naphthalene - Method: USEPA 8260B - MGT 350A Volatile Organics by GCMS
BTEX - Method: TRH C6-C40 - LTM-ORG-2010
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 3 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
. Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
Order No.: Report #: Phone: Fax:
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory Sample ID
Sample Date
Sampling Time
Matrix
LAB ID
53217BH1_0.15
Apr 09, 2015
3:00PM
Soil
B15-Ap07631
53217BH1_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07632
53217BH2_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07633
53217BH2_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07634
53217BH3_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07635
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 4 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH3_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07636
53217BH4_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07637
53217BH4_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07638
53217BH5_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07639
53217BH5_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07640
53217BH6_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07641
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 5 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH6_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07642
53217BH7_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07643
53217BH7_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07644
53217BH8_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07645
53217BH8_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07646
53217BH9_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07647
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 6 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH9_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07648
53217BH10_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07649
53217BH10_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07650
53217BH11_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07651
53217BH11_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07652
53217TB1_080415
Apr 08, 2015
Water
B15-Ap07653
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
X
Page 7 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217FB1_080415
Apr 08, 2015
Water
B15-Ap07654
53217R1_080415
Apr 08, 2015
Water
B15-Ap07655
53217FB2_090415
Apr 09, 2015
3:00PM
Water
B15-Ap07656
53217R2_090415
Apr 09, 2015
3:00PM
Water
B15-Ap07657
53217BH1_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07658
53217BH1_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07659
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 8 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH1_1.3
Apr 09, 2015
3:00PM
Soil
B15-Ap07660
53217BH1_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07661
53217BH1_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07662
53217MW1_4.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07663
53217MW1_5.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07664
53217MW1_6.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07665
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 9 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217MW1_7.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07666
53217MW1_8.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07667
53217MW1_9.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07668
53217BH2_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07669
53217BH2_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07670
53217BH2_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07671
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 10 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH2_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07672
53217BH3_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07673
53217BH3_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07674
53217BH3_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07675
53217BH3_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07676
53217MW2_4.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07677
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 11 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217MW2_5.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07678
53217MW2_6.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07679
53217MW2_7.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07680
53217MW2_8.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07681
53217BH4_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07682
53217BH4_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07683
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 12 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH4_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07684
53217BH4_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07685
53217BH5_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07686
53217BH5_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07687
53217BH5_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07688
53217BH5_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07689
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 13 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH6_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07690
53217BH6_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07691
53217BH6_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07692
53217BH6_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07693
53217BH7_0.15
Apr 09, 2015
3:00PM
Soil
B15-Ap07694
53217BH7_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07695
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 14 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH7_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07696
53217BH7_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07697
53217BH8_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07698
53217BH8_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07699
53217BH8_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07700
53217BH8_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07701
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 15 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217MW3_6.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07702
53217MW3_7.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07703
53217MW3_8.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07704
53217BH9_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07705
53217BH9_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07706
53217BH9_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07707
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 16 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH10_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07708
53217BH10_0.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07709
53217BH10_1.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07710
53217BH10_2.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07711
53217BH11_0.1
Apr 09, 2015
3:00PM
Soil
B15-Ap07712
53217BH11_1.5
Apr 09, 2015
3:00PM
Soil
B15-Ap07713
X X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 17 of 24 Report Number: 453692-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI 53217
e.mail : EnviroSales@eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
453692 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 10, 2015 3:30 PM Apr 17, 2015 5 Day Jason Scott
Eurofins | mgt Client Manager: Sarah Gould Eurofins | mgt Suite 7
BTEX and Naphthalene
Moisture Set
Cation Exchange Capacity
X
Eurofins | mgt Suite 10
X
Total Recoverable Hydrocarbons
Brisbane Laboratory - NATA Site # 20794
Metals M8
X
Polychlorinated Biphenyls
X
Polycyclic Aromatic Hydrocarbons
pH (1:5 Aqueous extract)
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
TRH C6-C10
Iron
HOLD
HOLD
% Clay*
X
Sample Detail
X
X
X
X
X
X
X
X
X
X
X
X
X
X
External Laboratory 53217BH11_3.0
Apr 09, 2015
3:00PM
Soil
B15-Ap07714
53217QC1_080415
Apr 08, 2015
3:00PM
Soil
B15-Ap07715
53217QC5_090415
Apr 09, 2015
3:00PM
Soil
B15-Ap07716
53217QC7_090415
Apr 09, 2015
3:00PM
Soil
B15-Ap07717
53217TB2_090415
Apr 09, 2015
3:00PM
Water
B15-Ap07718
53217QC3_080415
Apr 08, 2015
Soil
B15-Ap07719
X X X X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
X
X
Page 18 of 24 Report Number: 453692-W
Eurofins | mgt Internal Quality Control Review and Glossary General 1.
Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on request.
2.
All soil results are reported on a dry basis, unless otherwise stated.
3.
Actual LORs are matrix dependant. Quoted LORs may be raised where sample extracts are diluted due to interferences.
4.
Results are uncorrected for matrix spikes or surrogate recoveries.
5.
SVOC analysis on waters are performed on homogenised, unfiltered samples, unless noted otherwise.
6.
Samples were analysed on an 'as received' basis. 7. This report replaces any interim results previously issued.
Holding Times Please refer to 'Sample Preservation and Container Guide' for holding times (QS3001). For samples received on the last day of holding time, notification of testing requirements should have been received at least 6 hours prior to sample receipt deadlines as stated on the Sample Receipt Advice. If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues, suitably qualified results may still be reported. Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control. **NOTE: pH duplicates are reported as a range NOT as RPD
UNITS mg/kg: milligrams per Kilogram
mg/l: milligrams per litre
ug/l: micrograms per litre
ppm: Parts per million
ppb: Parts per billion
%: Percentage
org/100ml: Organisms per 100 millilitres
NTU: Nephelometric Turbidity Units
MPN/100mL: Most Probable Number of organisms per 100 millilitres
TERMS Dry
Where a moisture has been determined on a solid sample the result is expressed on a dry basis.
LOR
Limit of Reporting.
SPIKE
Addition of the analyte to the sample and reported as percentage recovery.
RPD
Relative Percent Difference between two Duplicate pieces of analysis.
LCS
Laboratory Control Sample - reported as percent recovery
CRM
Certified Reference Material - reported as percent recovery
Method Blank
In the case of solid samples these are performed on laboratory certified clean sands. In the case of water samples these are performed on de-ionised water.
Surr - Surrogate
The addition of a like compound to the analyte target and reported as percentage recovery.
Duplicate
A second piece of analysis from the same sample and reported in the same units as the result to show comparison.
Batch Duplicate
A second piece of analysis from a sample outside of the clients batch of samples but run within the laboratory batch of analysis.
Batch SPIKE
Spike recovery reported on a sample from outside of the clients batch of samples but run within the laboratory batch of analysis.
USEPA
United States Environmental Protection Agency
APHA
American Public Health Association
ASLP
Australian Standard Leaching Procedure (AS4439.3)
TCLP
Toxicity Characteristic Leaching Procedure
COC
Chain of Custody
SRA
Sample Receipt Advice
CP
Client Parent - QC was performed on samples pertaining to this report
NCP
Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within
TEQ
Toxic Equivalency Quotient
QC - ACCEPTANCE CRITERIA RPD Duplicates: Global RPD Duplicates Acceptance Criteria is 30% however the following acceptance guidelines are equally applicable: Results <10 times the LOR : No Limit Results between 10-20 times the LOR : RPD must lie between 0-50% Results >20 times the LOR : RPD must lie between 0-30% Surrogate Recoveries : Recoveries must lie between 50-150% - Phenols 20-130%.
QC DATA GENERAL COMMENTS 1.
Where a result is reported as a less than (<), higher than the nominated LOR, this is due to either matrix interference, extract dilution required due to interferences or contaminant levels within
2.
Duplicate data shown within this report that states the word "BATCH" is a Batch Duplicate from outside of your sample batch, but within the laboratory sample batch at a 1:10 ratio. The Parent and Duplicate data shown is not data from your samples.
3.
Organochlorine Pesticide analysis - where reporting LCS data, Toxophene & Chlordane are not added to the LCS.
4.
Organochlorine Pesticide analysis - where reporting Spike data, Toxophene is not added to the Spike.
5.
Total Recoverable Hydrocarbons - where reporting Spike & LCS data, a single spike of commercial Hydrocarbon products in the range of C12-C30 is added and it's Total Recovery is reported in the C10-C14 cell of the Report.
6.
pH and Free Chlorine analysed in the laboratory - Analysis on this test must begin within 30 minutes of sampling.Therefore laboratory analysis is unlikely to be completed within holding time. Analysis will begin as soon as possible after sample receipt.
7.
Recovery Data (Spikes & Surrogates) - where chromatographic interference does not allow the determination of Recovery the term "INT" appears against that analyte.
8.
Polychlorinated Biphenyls are spiked only using Arochlor 1260 in Matrix Spikes and LCS's.
9.
For Matrix Spikes and LCS results a dash " -" in the report means that the specific analyte was not added to the QC sample.
the sample, high moisture content or insufficient sample provided.
10. Duplicate RPD's are calculated from raw analytical data thus it is possible to have two sets of data.
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 19 of 24 Report Number: 453692-W
Quality Control Results
Test
Acceptance Pass Qualifying Limits Limits Code
Units
Result 1
mg/L mg/L mg/L
< 0.02 < 0.05 < 0.1
0.02 0.05 0.1
Pass Pass Pass
mg/L
< 0.1
0.1
Pass
Naphthalene
mg/L
< 0.02
0.02
Pass
Naphthalene TRH C6-C10 TRH C6-C10
mg/L mg/L mg/L
< 0.02 < 0.02 < 0.02
0.02 0.02 0.02
Pass Pass Pass
TRH C6-C10 less BTEX (F1) TRH >C10-C16
mg/L mg/L
< 0.02 < 0.05
0.02 0.05
Pass Pass
TRH >C16-C34
mg/L
< 0.1
0.1
Pass
TRH >C34-C40
mg/L
< 0.1
0.1
Pass
Benzene Toluene Ethylbenzene
mg/L mg/L mg/L
< 0.001 < 0.001 < 0.001
0.001 0.001 0.001
Pass Pass Pass
m&p-Xylenes
mg/L
< 0.002
0.002
Pass
o-Xylene Xylenes - Total Method Blank
mg/L mg/L
< 0.001 < 0.003
0.001 0.003
Pass Pass
Method Blank Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 TRH C10-C14 TRH C15-C28 TRH C29-C36 Method Blank Total Recoverable Hydrocarbons - 2013 NEPM Fractions
Method Blank BTEX
Polycyclic Aromatic Hydrocarbons Acenaphthene
mg/L
< 0.001
0.001
Pass
Acenaphthylene
mg/L
< 0.001
0.001
Pass
Anthracene Benz(a)anthracene Benzo(a)pyrene Benzo(b&j)fluoranthene Benzo(g.h.i)perylene
mg/L mg/L mg/L mg/L mg/L
< 0.001 < 0.001 < 0.001 < 0.001 < 0.001
0.001 0.001 0.001 0.001 0.001
Pass Pass Pass Pass Pass
Benzo(k)fluoranthene
mg/L
< 0.001
0.001
Pass
Chrysene Dibenz(a.h)anthracene Fluoranthene
mg/L mg/L mg/L
< 0.001 < 0.001 < 0.001
0.001 0.001 0.001
Pass Pass Pass
Fluorene Indeno(1.2.3-cd)pyrene
mg/L mg/L
< 0.001 < 0.001
0.001 0.001
Pass Pass
Naphthalene
mg/L
< 0.001
0.001
Pass
Phenanthrene
mg/L
< 0.001
0.001
Pass
Pyrene Method Blank
mg/L
< 0.001
0.001
Pass
Arsenic Cadmium Chromium
mg/L mg/L mg/L
< 0.001 < 0.0002 < 0.001
0.001 0.0002 0.001
Pass Pass Pass
Copper Lead
mg/L mg/L
< 0.001 < 0.001
0.001 0.001
Pass Pass
Mercury
mg/L
< 0.0001
0.0001
Pass
Nickel Zinc
mg/L mg/L
< 0.001 < 0.001
0.001 0.001
Pass Pass
Heavy Metals
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 20 of 24 Report Number: 453692-W
Test
Acceptance Pass Qualifying Limits Limits Code
Units
Result 1
% %
103 93
70-130 70-130
Pass Pass
% % %
98 107 94
70-130 70-130 70-130
Pass Pass Pass
Benzene Toluene
% %
102 110
70-130 70-130
Pass Pass
Ethylbenzene m&p-Xylenes Xylenes - Total
% % %
112 104 105
70-130 70-130 70-130
Pass Pass Pass
Acenaphthene Acenaphthylene
% %
83 97
70-130 70-130
Pass Pass
Anthracene Benz(a)anthracene Benzo(a)pyrene
% % %
104 112 110
70-130 70-130 70-130
Pass Pass Pass
Benzo(b&j)fluoranthene
%
93
70-130
Pass
Benzo(g.h.i)perylene Benzo(k)fluoranthene
% %
91 97
70-130 70-130
Pass Pass
Chrysene
%
98
70-130
Pass
Dibenz(a.h)anthracene Fluoranthene
% %
89 117
70-130 70-130
Pass Pass
Fluorene
%
89
70-130
Pass
Indeno(1.2.3-cd)pyrene Naphthalene
% %
91 85
70-130 70-130
Pass Pass
Phenanthrene
%
74
70-130
Pass
Pyrene
%
111
70-130
Pass
Arsenic
%
96
80-120
Pass
Cadmium Chromium
% %
94 93
80-120 80-120
Pass Pass
Copper Lead
% %
94 96
80-120 80-120
Pass Pass
Mercury Nickel
% %
102 93
75-125 80-120
Pass Pass
%
95
Units
Result 1
LCS - % Recovery Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 TRH C10-C14 LCS - % Recovery Total Recoverable Hydrocarbons - 2013 NEPM Fractions TRH C6-C10 TRH C6-C10 TRH >C10-C16 LCS - % Recovery BTEX
LCS - % Recovery Polycyclic Aromatic Hydrocarbons
LCS - % Recovery Heavy Metals
Zinc Test
Lab Sample ID
QA Source
80-120 Pass Acceptance Pass Qualifying Limits Limits Code
Spike - % Recovery Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C10-C14 Spike - % Recovery
B15-Ma24113
NCP
Result 1 %
Total Recoverable Hydrocarbons - 2013 NEPM Fractions TRH >C10-C16 Spike - % Recovery
NCP
%
M15-Ap06664
NCP
%
86
Pass
70-130
Pass
70-130
Pass
Result 1 92
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
70-130
Result 1
B15-Ma24113
Polycyclic Aromatic Hydrocarbons Acenaphthene
84
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 21 of 24 Report Number: 453692-W
Acenaphthylene
M15-Ap06664
QA Source NCP
%
99
Anthracene
M15-Ap06664
NCP
%
98
70-130
Pass
Benz(a)anthracene Benzo(a)pyrene
M15-Ap06664 M15-Ap06664
NCP NCP
% %
117 96
70-130 70-130
Pass Pass
Benzo(b&j)fluoranthene
M15-Ap06664
NCP
%
80
70-130
Pass
Benzo(g.h.i)perylene
M15-Ap06664
NCP
%
82
70-130
Pass
Benzo(k)fluoranthene Chrysene Dibenz(a.h)anthracene Fluoranthene
M15-Ap06664 M15-Ap06664 M15-Ap06664 M15-Ap06664
NCP NCP NCP NCP
% % % %
85 105 76 118
70-130 70-130 70-130 70-130
Pass Pass Pass Pass
Test
Lab Sample ID
Units
Acceptance Pass Qualifying Limits Limits Code 70-130 Pass
Result 1
Fluorene
M15-Ap06664
NCP
%
102
70-130
Pass
Indeno(1.2.3-cd)pyrene
M15-Ap06664
NCP
%
78
70-130
Pass
Naphthalene
M15-Ap06664
NCP
%
79
70-130
Pass
M15-Ap06664 M15-Ap06664
NCP NCP
% %
95 113
70-130 70-130
Pass Pass
Arsenic
M15-Ap07579
NCP
%
96
75-125
Pass
Cadmium
M15-Ap07579
NCP
%
94
75-125
Pass
Chromium
M15-Ap07579
NCP
%
93
75-125
Pass
Copper Lead
M15-Ap07579 M15-Ap07579
NCP NCP
% %
93 95
75-125 75-125
Pass Pass
Mercury
M15-Ap07579
NCP
%
100
70-130
Pass
Nickel
M15-Ap07579
NCP
%
93
75-125
Pass
M15-Ap07579
NCP
%
94
75-125
Pass
70-130
Pass
70-130
Pass
Phenanthrene Pyrene Spike - % Recovery Heavy Metals
Result 1
Zinc Spike - % Recovery
Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 Spike - % Recovery
B15-Ap07656
CP
Result 1 %
Total Recoverable Hydrocarbons - 2013 NEPM Fractions TRH C6-C10 Spike - % Recovery
90 Result 1
B15-Ap07656
CP
%
Benzene
B15-Ap07656
CP
%
96
70-130
Pass
Toluene Ethylbenzene
B15-Ap07656 B15-Ap07656
CP CP
% %
96 97
70-130 70-130
Pass Pass
m&p-Xylenes
B15-Ap07656
CP
%
95
70-130
Pass
o-Xylene
B15-Ap07656
CP
%
94
70-130
Pass
Xylenes - Total
B15-Ap07656
CP QA Source
%
95
Units
Result 1
mg/L
Result 1 < 0.02
Result 2 < 0.02
RPD <1
30%
Pass
mg/L mg/L mg/L
< 0.05 < 0.1 < 0.1
< 0.05 < 0.1 < 0.1
<1 <1 <1
30% 30% 30%
Pass Pass Pass
mg/L
Result 1 < 0.02
Result 2 < 0.02
RPD <1
BTEX
99 Result 1
Test
Lab Sample ID
Duplicate Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 B15-Ap07655 CP TRH C10-C14 TRH C15-C28 TRH C29-C36
M15-Ma24098 M15-Ma24098 M15-Ma24098
NCP NCP NCP
70-130 Pass Acceptance Pass Qualifying Limits Limits Code
Duplicate Total Recoverable Hydrocarbons - 2013 NEPM Fractions Naphthalene B15-Ap07655 CP
30%
Pass
TRH C6-C10
B15-Ap07655
CP
mg/L
< 0.02
< 0.02
<1
30%
Pass
TRH C6-C10 less BTEX (F1) TRH >C10-C16
B15-Ap07655 M15-Ma24098
CP NCP
mg/L mg/L
< 0.02 < 0.05
< 0.02 < 0.05
<1 <1
30% 30%
Pass Pass
TRH >C16-C34
M15-Ma24098
NCP
mg/L
< 0.1
< 0.1
<1
30%
Pass
TRH >C34-C40
M15-Ma24098
NCP
mg/L
< 0.1
< 0.1
<1
30%
Pass
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 22 of 24 Report Number: 453692-W
Duplicate BTEX Benzene
B15-Ap07655
CP
mg/L
Result 1 < 0.001
Result 2 < 0.001
RPD <1
30%
Pass
Toluene
B15-Ap07655
CP
mg/L
< 0.001
< 0.001
<1
30%
Pass
Ethylbenzene
B15-Ap07655
CP
mg/L
< 0.001
< 0.001
<1
30%
Pass
m&p-Xylenes o-Xylene
B15-Ap07655 B15-Ap07655
CP CP
mg/L mg/L
< 0.002 < 0.001
< 0.002 < 0.001
<1 <1
30% 30%
Pass Pass
Xylenes - Total Duplicate
B15-Ap07655
CP
mg/L
< 0.003
< 0.003
<1
30%
Pass
Result 1
Result 2
RPD
Acenaphthene
M15-Ap06650
NCP
mg/L
< 0.001
< 0.001
<1
30%
Pass
Acenaphthylene
M15-Ap06650
NCP
mg/L
< 0.001
< 0.001
<1
30%
Pass
Anthracene Benz(a)anthracene
M15-Ap06650 M15-Ap06650
NCP NCP
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
<1 <1
30% 30%
Pass Pass
Benzo(a)pyrene
M15-Ap06650
NCP
mg/L
< 0.001
< 0.001
<1
30%
Pass
Benzo(b&j)fluoranthene
M15-Ap06650
NCP
mg/L
< 0.001
< 0.001
<1
30%
Pass
Benzo(g.h.i)perylene
M15-Ap06650
NCP
mg/L
< 0.001
< 0.001
<1
30%
Pass
Benzo(k)fluoranthene
M15-Ap06650
NCP
mg/L
< 0.001
< 0.001
<1
30%
Pass
Chrysene
M15-Ap06650
NCP
mg/L
< 0.001
< 0.001
<1
30%
Pass
Dibenz(a.h)anthracene Fluoranthene
M15-Ap06650 M15-Ap06650
NCP NCP
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
<1 <1
30% 30%
Pass Pass Pass
Polycyclic Aromatic Hydrocarbons
Fluorene
M15-Ap06650
NCP
mg/L
< 0.001
< 0.001
<1
30%
Indeno(1.2.3-cd)pyrene
M15-Ap06650
NCP
mg/L
< 0.001
< 0.001
<1
30%
Pass
M15-Ap06650 M15-Ap06650 M15-Ap06650
NCP NCP NCP
mg/L mg/L mg/L
< 0.001 < 0.001 < 0.001
< 0.001 < 0.001 < 0.001
<1 <1 <1
30% 30% 30%
Pass Pass Pass
M15-Ap07579 M15-Ap07579 M15-Ap07579 M15-Ap07579 M15-Ap07579 M15-Ap07579 M15-Ap07579
NCP NCP NCP NCP NCP NCP NCP
mg/L mg/L mg/L mg/L mg/L mg/L mg/L
Result 1 < 0.001 < 0.0002 < 0.001 < 0.001 < 0.001 < 0.0001 < 0.001
Result 2 < 0.001 < 0.0002 < 0.001 < 0.001 < 0.001 < 0.0001 < 0.001
RPD <1 <1 <1 <1 <1 <1 <1
30% 30% 30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass Pass Pass
Naphthalene Phenanthrene Pyrene Duplicate Heavy Metals Arsenic Cadmium Chromium Copper Lead Mercury Nickel
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 23 of 24 Report Number: 453692-W
Comments Sample Integrity Custody Seals Intact (if used)
N/A
Attempt to Chill was evident
Yes
Sample correctly preserved
Yes
Appropriate sample containers have been used
Yes
Sample containers for volatile analysis received with minimal headspace
Yes
Samples received within HoldingTime
Yes
Some samples have been subcontracted
No
Qualifier Codes/Comments Code Description N01
F2 is determined by arithmetically subtracting the "naphthalene" value from the ">C10-C16" value. The naphthalene value used in this calculation is obtained from volatiles (Purge & Trap analysis).
N02
Where we have reported both volatile (P&T GCMS) and semivolatile (GCMS) naphthalene data, results may not be identical. Provided correct sample handling protocols have been followed, any observed differences in results are likely to be due to procedural differences within each methodology. Results determined by both techniques have passed all QAQC acceptance criteria, and are entirely technically valid.
N04
F1 is determined by arithmetically subtracting the "Total BTEX" value from the "C6-C10" value. The "Total BTEX" value is obtained by summing the concentrations of BTEX analytes. The "C6-C10" value is obtained by quantitating against a standard of mixed aromatic/aliphatic analytes.
N07
Please note:- These two PAH isomers closely co-elute using the most contemporary analytical methods and both the reported concentration (and the TEQ) apply specifically to the total of the two co-eluting PAHs
Authorised By Sarah Gould
Analytical Services Manager
Carroll Lee
Senior Analyst-Organic (VIC)
Emily Rosenberg
Senior Analyst-Metal (VIC)
Richard Corner
Senior Analyst-Volatile (QLD)
Glenn Jackson National Laboratory Manager - Indicates Not Requested * Indicates NATA accreditation does not cover the performance of this service Uncertainty data is available on request Eurofins | mgt shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretation given in this report. In no case shall Eurofins | mgt be liable for consequential damages including, but not limited to, lost profits, damages for failure to meet deadlines and lost production arising from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 20, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 24 of 24 Report Number: 453692-W
CERTIFICATE OF ANALYSIS
126496
Client: Prensa Pty Ltd Level 1, 261-271 Wattletree Rd Malvern VIC 3144 Attention:
John Scott, Anthony Plumb
Sample log in details: Your Reference: No. of samples: Date samples received / completed instructions received
53217, DSI 4 Soils 13/04/2015
/
14/04/2015
Analysis Details: Please refer to the following pages for results, methodology summary and quality control data. Samples were analysed as received from the client. Results relate specifically to the samples as received. Results are reported on a dry weight basis for solids and on an as received basis for other matrices. Please refer to the last page of this report for any comments relating to the results. Report Details: Date results requested by: / Issue Date: 21/04/15 / 17/04/15 Date of Preliminary Report: Not Issued NATA accreditation number 2901. This document shall not be reproduced except in full. Accredited for compliance with ISO/IEC 17025. Tests not covered by NATA are denoted with *. Results Approved By:
Envirolab Reference: Revision No:
126496 R 00
Page 1 of 11
Client Reference:
53217, DSI
vTRH(C6-C10)/BTEXN in Soil Our Reference:
UNITS
126496-2
Your Reference
-------------
53217-QC4080415
Date Sampled
------------
9/04/2015
Type of sample
Soil
Date extracted
-
15/04/2015
Date analysed
-
16/04/2015
TRHC 6 - C 9
mg/kg
<25
TRHC 6 - C 10
mg/kg
<25
vTPH C6 - C 10 less BTEX (F1)
mg/kg
<25
Benzene
mg/kg
<0.2
Toluene
mg/kg
<0.5
Ethylbenzene
mg/kg
<1
m+p-xylene
mg/kg
<2
o-Xylene
mg/kg
<1
naphthalene
mg/kg
<1
Surrogate aaa-Trifluorotoluene
%
89
Envirolab Reference: Revision No:
126496 R 00
Page 2 of 11
Client Reference:
53217, DSI
svTRH (C10-C40) in Soil Our Reference:
UNITS
126496-2
Your Reference
-------------
53217-QC4080415
Date Sampled
------------
9/04/2015
Type of sample
Soil
Date extracted
-
15/04/2015
Date analysed
-
16/04/2015
TRHC 10 - C 14
mg/kg
<50
TRHC 15 - C 28
mg/kg
<100
TRHC 29 - C 36
mg/kg
<100
TRH >C10-C 16
mg/kg
<50
TRH >C10 - C 16 less Naphthalene (F2)
mg/kg
<50
TRH >C16-C 34
mg/kg
<100
TRH >C34-C 40
mg/kg
<100
%
82
Surrogate o-Terphenyl
Envirolab Reference: Revision No:
126496 R 00
Page 3 of 11
Client Reference:
53217, DSI
PAHs in Soil Our Reference:
UNITS
126496-2
Your Reference
-------------
53217-QC4080415
Date Sampled
------------
9/04/2015
Type of sample
Soil
Date extracted
-
15/04/2015
Date analysed
-
15/04/2015
Naphthalene
mg/kg
<0.1
Acenaphthylene
mg/kg
<0.1
Acenaphthene
mg/kg
<0.1
Fluorene
mg/kg
<0.1
Phenanthrene
mg/kg
<0.1
Anthracene
mg/kg
<0.1
Fluoranthene
mg/kg
<0.1
Pyrene
mg/kg
<0.1
Benzo(a)anthracene
mg/kg
<0.1
Chrysene
mg/kg
<0.1
Benzo(b,j+k)fluoranthene
mg/kg
<0.2
Benzo(a)pyrene
mg/kg
<0.05
Indeno(1,2,3-c,d)pyrene
mg/kg
<0.1
Dibenzo(a,h)anthracene
mg/kg
<0.1
Benzo(g,h,i)perylene
mg/kg
<0.1
Benzo(a)pyrene TEQ calc (zero)
mg/kg
<0.5
Benzo(a)pyrene TEQ calc(half)
mg/kg
<0.5
Benzo(a)pyrene TEQ calc(PQL)
mg/kg
<0.5
Total Positive PAHs
mg/kg
NIL (+)VE
Surrogate p-Terphenyl-d14
%
97
Envirolab Reference: Revision No:
126496 R 00
Page 4 of 11
Client Reference:
53217, DSI
Acid Extractable metals in soil Our Reference:
UNITS
126496-2
Your Reference
-------------
53217-QC4080415
Date Sampled
------------
9/04/2015
Type of sample
Soil
Date digested
-
15/04/2015
Date analysed
-
15/04/2015
Arsenic
mg/kg
5
Cadmium
mg/kg
<0.4
Chromium
mg/kg
21
Copper
mg/kg
100
Lead
mg/kg
25
Mercury
mg/kg
<0.1
Nickel
mg/kg
7
Zinc
mg/kg
41
Envirolab Reference: Revision No:
126496 R 00
Page 5 of 11
Client Reference:
53217, DSI
Moisture Our Reference:
UNITS
126496-2
Your Reference
-------------
53217-QC4080415
Date Sampled
------------
9/04/2015
Type of sample
Soil
Date prepared
-
15/04/2015
Date analysed
-
16/04/2015
Moisture
%
16
Envirolab Reference: Revision No:
126496 R 00
Page 6 of 11
Client Reference: Method ID
53217, DSI
Methodology Summary
Org-016
Soil samples are extracted with methanol and spiked into water prior to analysing by purge and trap GC-MS. Water samples are analysed directly by purge and trap GC-MS. F1 = (C6-C10)-BTEX as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater.
Org-014
Soil samples are extracted with methanol and spiked into water prior to analysing by purge and trap GC-MS.
Org-003
Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed by GC-FID. F2 = (>C10-C16)-Naphthalene as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater (HSLs Tables 1A (3, 4)). Note Naphthalene is determined from the VOC analysis.
Org-012 subset
Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed by GC-MS. Benzo(a)pyrene TEQ as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater 2013. For soil results:1. ‘TEQ PQL’ values are assuming all contributing PAHs reported as <PQL are actually at the PQL. This is the most conservative approach and can give false positive TEQs given that PAHs that contribute to the TEQ calculation may not be present. 2. ‘TEQ zero’ values are assuming all contributing PAHs reported as <PQL are zero. This is the least conservative approach and is more susceptible to false negative TEQs when PAHs that contribute to the TEQ calculation are present but below PQL. 3. ‘TEQ half PQL’ values are assuming all contributing PAHs reported as <PQL are half the stipulated PQL. Hence a mid-point between the most and least conservative approaches above. Note, the Total +ve PAHs PQL is reflective of the lowest individual PQL and is therefore" Total +ve PAHs" is simply a sum of the positive individual PAHs.
Metals-020 ICPAES
Determination of various metals by ICP-AES.
Metals-021 CVAAS
Determination of Mercury by Cold Vapour AAS.
Inorg-008
Moisture content determined by heating at 105+/-5 deg C for a minimum of 12 hours.
Envirolab Reference: Revision No:
126496 R 00
Page 7 of 11
Client Reference: QUALITY CONTROL
UNITS
PQL
METHOD
53217, DSI
Blank
Duplicate Sm#
vTRH(C6-C10)/BTEXN in Soil
Duplicate results
Spike Sm#
Spike % Recovery
Base ll Duplicate ll %RPD
Date extracted
-
15/04/2 015
[NT]
[NT]
LCS-6
15/04/2015
Date analysed
-
16/04/2 015
[NT]
[NT]
LCS-6
16/04/2015
TRHC 6 - C 9
mg/kg
25
Org-016
<25
[NT]
[NT]
LCS-6
98%
TRHC 6 - C 10
mg/kg
25
Org-016
<25
[NT]
[NT]
LCS-6
98%
Benzene
mg/kg
0.2
Org-016
<0.2
[NT]
[NT]
LCS-6
93%
Toluene
mg/kg
0.5
Org-016
<0.5
[NT]
[NT]
LCS-6
94%
Ethylbenzene
mg/kg
1
Org-016
<1
[NT]
[NT]
LCS-6
95%
m+p-xylene
mg/kg
2
Org-016
<2
[NT]
[NT]
LCS-6
103%
o-Xylene
mg/kg
1
Org-016
<1
[NT]
[NT]
LCS-6
94%
naphthalene
mg/kg
1
Org-014
<1
[NT]
[NT]
[NR]
[NR]
Surrogate aaaTrifluorotoluene
%
Org-016
97
[NT]
[NT]
LCS-6
101%
Spike Sm#
Spike % Recovery
QUALITY CONTROL
UNITS
PQL
METHOD
Blank
Duplicate Sm#
svTRH (C10-C40) in Soil
Duplicate results Base ll Duplicate ll %RPD
Date extracted
-
15/04/2 015
[NT]
[NT]
LCS-6
15/04/2015
Date analysed
-
15/04/2 015
[NT]
[NT]
LCS-6
15/04/2015
TRHC 10 - C 14
mg/kg
50
Org-003
<50
[NT]
[NT]
LCS-6
102%
TRHC 15 - C 28
mg/kg
100
Org-003
<100
[NT]
[NT]
LCS-6
91%
TRHC 29 - C 36
mg/kg
100
Org-003
<100
[NT]
[NT]
LCS-6
108%
TRH >C10-C 16
mg/kg
50
Org-003
<50
[NT]
[NT]
LCS-6
102%
TRH >C16-C 34
mg/kg
100
Org-003
<100
[NT]
[NT]
LCS-6
91%
TRH >C34-C 40
mg/kg
100
Org-003
<100
[NT]
[NT]
LCS-6
108%
Org-003
78
[NT]
[NT]
LCS-6
92%
Spike Sm#
Spike % Recovery
Surrogate o-Terphenyl QUALITY CONTROL
% UNITS
PQL
METHOD
Blank
Duplicate Sm#
PAHs in Soil
Duplicate results Base ll Duplicate ll %RPD
Date extracted
-
15/04/2 015
[NT]
[NT]
LCS-6
15/04/2015
Date analysed
-
15/04/2 015
[NT]
[NT]
LCS-6
15/04/2015
Naphthalene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
LCS-6
101%
Acenaphthylene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
[NR]
[NR]
Acenaphthene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
[NR]
[NR]
Fluorene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
LCS-6
95%
Phenanthrene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
LCS-6
97%
Anthracene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
[NR]
[NR]
Fluoranthene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
LCS-6
93%
Envirolab Reference: Revision No:
126496 R 00
Page 8 of 11
Client Reference: QUALITY CONTROL
UNITS
PQL
METHOD
53217, DSI
Blank
Duplicate Sm#
PAHs in Soil
Duplicate results
Spike Sm#
Spike % Recovery
Base ll Duplicate ll %RPD
Pyrene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
LCS-6
96%
Benzo(a)anthracene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
[NR]
[NR]
Chrysene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
LCS-6
92%
Benzo(b,j+k) fluoranthene
mg/kg
0.2
Org-012 subset
<0.2
[NT]
[NT]
[NR]
[NR]
Benzo(a)pyrene
mg/kg
0.05
Org-012 subset
<0.05
[NT]
[NT]
LCS-6
119%
Indeno(1,2,3-c,d)pyrene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
[NR]
[NR]
Dibenzo(a,h)anthracene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
[NR]
[NR]
Benzo(g,h,i)perylene
mg/kg
0.1
Org-012 subset
<0.1
[NT]
[NT]
[NR]
[NR]
Surrogate p-Terphenyld14
%
Org-012 subset
100
[NT]
[NT]
LCS-6
101%
Spike Sm#
Spike % Recovery
QUALITY CONTROL
UNITS
PQL
METHOD
Blank
Duplicate Sm#
Acid Extractable metals in soil
Duplicate results Base ll Duplicate ll %RPD
Date digested
-
15/04/2 015
[NT]
[NT]
LCS-1
15/04/2015
Date analysed
-
15/04/2 015
[NT]
[NT]
LCS-1
15/04/2015
Arsenic
mg/kg
4
Metals-020 ICP-AES
<4
[NT]
[NT]
LCS-1
120%
Cadmium
mg/kg
0.4
Metals-020 ICP-AES
<0.4
[NT]
[NT]
LCS-1
114%
Chromium
mg/kg
1
Metals-020 ICP-AES
<1
[NT]
[NT]
LCS-1
119%
Copper
mg/kg
1
Metals-020 ICP-AES
<1
[NT]
[NT]
LCS-1
119%
Lead
mg/kg
1
Metals-020 ICP-AES
<1
[NT]
[NT]
LCS-1
113%
Mercury
mg/kg
0.1
Metals-021 CV-AAS
<0.1
[NT]
[NT]
LCS-1
92%
Nickel
mg/kg
1
Metals-020 ICP-AES
<1
[NT]
[NT]
LCS-1
116%
Zinc
mg/kg
1
Metals-020 ICP-AES
<1
[NT]
[NT]
LCS-1
116%
Envirolab Reference: Revision No:
126496 R 00
Page 9 of 11
Client Reference:
53217, DSI
Report Comments:
Asbestos ID was analysed by Approved Identifier: Asbestos ID was authorised by Approved Signatory:
INS: Insufficient sample for this test NA: Test not required <: Less than
Envirolab Reference: Revision No:
126496 R 00
Not applicable for this job Not applicable for this job
PQL: Practical Quantitation Limit RPD: Relative Percent Difference >: Greater than
NT: Not tested NA: Test not required LCS: Laboratory Control Sample
Page 10 of 11
Client Reference:
53217, DSI
Quality Control Definitions Blank: This is the component of the analytical signal which is not derived from the sample but from reagents, glassware etc, can be determined by processing solvents and reagents in exactly the same manner as for samples. Duplicate : This is the complete duplicate analysis of a sample from the process batch. If possible, the sample selected should be one where the analyte concentration is easily measurable. Matrix Spike : A portion of the sample is spiked with a known concentration of target analyte. The purpose of the matrix spike is to monitor the performance of the analytical method used and to determine whether matrix interferences exist. LCS (Laboratory Control Sample) : This comprises either a standard reference material or a control matrix (such as a blank sand or water) fortified with analytes representative of the analyte class. It is simply a check sample. Surrogate Spike: Surrogates are known additions to each sample, blank, matrix spike and LCS in a batch, of compounds which are similar to the analyte of interest, however are not expected to be found in real samples. Laboratory Acceptance Criteria Duplicate sample and matrix spike recoveries may not be reported on smaller jobs, however, were analysed at a frequency to meet or exceed NEPM requirements. All samples are tested in batches of 20. The duplicate sample RPD and matrix spike recoveries for the batch were within the laboratory acceptance criteria. Filters, swabs, wipes, tubes and badges will not have duplicate data as the whole sample is generally extracted during sample extraction. Spikes for Physical and Aggregate Tests are not applicable. For VOCs in water samples, three vials are required for duplicate or spike analysis. Duplicates: <5xPQL - any RPD is acceptable; >5xPQL - 0-50% RPD is acceptable. Matrix Spikes, LCS and Surrogate recoveries: Generally 70-130% for inorganics/metals; 60-140% for organics (+/-50% surrogates) and 10-140% for labile SVOCs (including labile surrogates), ultra trace organics and speciated phenols is acceptable. In circumstances where no duplicate and/or sample spike has been reported at 1 in 10 and/or 1 in 20 samples respectively, the sample volume submitted was insufficient in order to satisfy laboratory QA/QC protocols. When samples are received where certain analytes are outside of recommended technical holding times (THTs), the analysis has proceeded. Where analytes are on the verge of breaching THTs, every effort will be made to analyse within the THT or as soon as practicable.
Envirolab Reference: Revision No:
126496 R 00
Page 11 of 11
ABN – 50 005 085 521
e.mail : EnviroSales@eurofins.com.au
web : www.eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh Vic 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Sample Receipt Advice Company name:
Prensa QLD&WA
Contact name: Project name: Project ID: COC number: Turn around time: Date/Time received: Eurofins | mgt reference:
John Scott DSI GRAFTON 53217 Not provided 5 Day Apr 17, 2015 1:15 PM 454407
Sample information 䖵
A detailed list of analytes logged into our LIMS, is included in the attached summary table.
䖵
All samples have been received as described on the above COC.
䖵
COC has been completed correctly.
䖵
Attempt to chill was evident.
䖵
Appropriately preserved sample containers have been used.
䖵
All samples were received in good condition.
䖵
Samples have been provided with adequate time to commence analysis in accordance with the relevant holding times.
䖵
Appropriate sample containers have been used.
䖵
Sample containers for volatile analysis received with zero headspace.
䖶
Some samples have been subcontracted.
㻺㻛㻭
Custody Seals intact (if used).
Contact notes If you have any questions with respect to these samples please contact: Sarah Gould on Phone : (+61) (8) 8154 3100 or by e.mail: SarahGould@eurofins.com.au Results will be delivered electronically via e.mail to John Scott - john.scott@prensa.com.au.
Environmental Laboratory Air Analysis Water Analysis Soil Contamination Analysis
NATA Accreditation Stack Emission Sampling & Analysis Trade Waste Sampling & Analysis Groundwater Sampling & Analysis
38 Years of Environmental Analysis & Experience
ABN â&#x20AC;&#x201C; 50 005 085 521
e.mail : EnviroSales@eurofins.com.au
web : www.eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
. Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI GRAFTON 53217
Order No.: Report #: Phone: Fax:
Received: Due: Priority: Contact Name:
454407 07 3291 9700
Apr 17, 2015 1:15 PM Apr 24, 2015 5 Day John Scott
Eurofins | mgt Client Manager: Sarah Gould
X
X
X
X
X
X
BTEX and Naphthalene
X
Eurofins | mgt Suite 10 (filtered metals)
X
Total Recoverable Hydrocarbons
X
BTEX
Brisbane Laboratory - NATA Site # 20794
Metals M8 filtered
X
Polychlorinated Biphenyls
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
Polycyclic Aromatic Hydrocarbons
TRH C6-C10
HOLD
Sample Detail
X
External Laboratory Sample ID
Sample Date
Sampling Time
Matrix
LAB ID
53217_MW1_1 Apr 16, 2015 60415
4:00PM
Water
B15-Ap13034
53217_MW2_1 Apr 16, 2015 60415
4:00PM
Water
B15-Ap13035
53217_MW3_1 Apr 16, 2015 60415
4:00PM
Water
B15-Ap13036
53217_QC9_1 Apr 16, 2015 60415
4:00PM
Water
B15-Ap13037
53217_TB3_16 Apr 16, 2015 0415
4:00PM
Water
B15-Ap13038
X X
X
X
X
X
X
X X
X X
X
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI GRAFTON 53217
e.mail : EnviroSales@eurofins.com.au
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
454407 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 17, 2015 1:15 PM Apr 24, 2015 5 Day John Scott
Eurofins | mgt Client Manager: Sarah Gould
Water
B15-Ap13039
53217_FB3_16 Apr 16, 2015 0415
4:00PM
Water
B15-Ap13040
X X
X
X
X
X
X
BTEX and Naphthalene
4:00PM
X
Eurofins | mgt Suite 10 (filtered metals)
53217_R3_160 Apr 16, 2015 415
X
Total Recoverable Hydrocarbons
X
External Laboratory
X
BTEX
Brisbane Laboratory - NATA Site # 20794
Metals M8 filtered
X
Polychlorinated Biphenyls
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
Polycyclic Aromatic Hydrocarbons
TRH C6-C10
HOLD
Sample Detail
X
Certificate of Analysis NATA Accredited Accreditation Number 1261 Site Number 1254
PRENSA QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Accredited for compliance with ISO/IEC 17025. The results of the tests, calibrations and/or measurements included in this document are traceable to Australian/national standards.
Attention:
John Scott
Report
454407-W
Project name
DSI GRAFTON
Project ID
53217
Received Date
Apr 17, 2015
Sample Matrix
53217_MW1_1 53217_MW2_1 53217_MW3_1 53217_QC9_16 60415 60415 60415 0415 Water Water Water Water
Eurofins | mgt Sample No.
B15-Ap13034
B15-Ap13035
B15-Ap13036
B15-Ap13037
Apr 16, 2015
Apr 16, 2015
Apr 16, 2015
Apr 16, 2015
Client Sample ID
Date Sampled Test/Reference LOR Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Unit
TRH C6-C9
0.02
mg/L
< 0.02
< 0.02
< 0.02
< 0.02
TRH C10-C14
0.05
mg/L
< 0.05
< 0.05
< 0.05
< 0.05
TRH C15-C28 TRH C29-C36 TRH C10-36 (Total)
0.1 0.1 0.1
mg/L mg/L mg/L
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
Benzene Toluene
0.001 0.001
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
Ethylbenzene
0.001
mg/L
< 0.001
< 0.001
< 0.001
< 0.001
m&p-Xylenes
0.002
mg/L
< 0.002
< 0.002
< 0.002
< 0.002
o-Xylene 0.001 Xylenes - Total 0.003 4-Bromofluorobenzene (surr.) 1 Total Recoverable Hydrocarbons - 2013 NEPM Fractions
mg/L mg/L %
< 0.001 < 0.003 99
< 0.001 < 0.003 97
< 0.001 < 0.003 92
< 0.001 < 0.003 100
NaphthaleneN02
0.02
mg/L
< 0.02
< 0.02
< 0.02
< 0.02
TRH C6-C10
0.02
mg/L
< 0.02
< 0.02
< 0.02
< 0.02
TRH C6-C10 less BTEX (F1)N04 TRH >C10-C16 TRH >C10-C16 less Naphthalene (F2)N01
0.02 0.05 0.05
mg/L mg/L mg/L
< 0.02 < 0.05 < 0.05
< 0.02 < 0.05 < 0.05
< 0.02 < 0.05 < 0.05
< 0.02 < 0.05 < 0.05
TRH >C16-C34 TRH >C34-C40
0.1 0.1
mg/L mg/L
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
Acenaphthene
0.001
mg/L
< 0.001
< 0.001
< 0.001
< 0.001
Acenaphthylene Anthracene
0.001 0.001
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
Benz(a)anthracene Benzo(a)pyrene
0.001 0.001
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
Benzo(b&j)fluorantheneN07 Benzo(g.h.i)perylene
0.001 0.001
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
Benzo(k)fluoranthene
0.001
mg/L
< 0.001
< 0.001
< 0.001
< 0.001
Chrysene Dibenz(a.h)anthracene Fluoranthene
0.001 0.001 0.001
mg/L mg/L mg/L
< 0.001 < 0.001 < 0.001
< 0.001 < 0.001 < 0.001
< 0.001 < 0.001 < 0.001
< 0.001 < 0.001 < 0.001
Fluorene Indeno(1.2.3-cd)pyrene
0.001 0.001
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
BTEX
Polycyclic Aromatic Hydrocarbons
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 1 of 14 Report Number: 454407-W
Sample Matrix
53217_MW1_1 53217_MW2_1 53217_MW3_1 53217_QC9_16 60415 60415 60415 0415 Water Water Water Water
Eurofins | mgt Sample No.
B15-Ap13034
B15-Ap13035
B15-Ap13036
B15-Ap13037
Apr 16, 2015
Apr 16, 2015
Apr 16, 2015
Apr 16, 2015
Client Sample ID
Date Sampled Test/Reference Polycyclic Aromatic Hydrocarbons
LOR
Unit
Naphthalene Phenanthrene
0.001 0.001
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
Pyrene
0.001
mg/L
< 0.001
< 0.001
< 0.001
< 0.001
Total PAH* 2-Fluorobiphenyl (surr.)
0.001 1
mg/L %
< 0.001 61
< 0.001 90
< 0.001 83
< 0.001 76
1
%
71
100
86
100
p-Terphenyl-d14 (surr.) Organochlorine Pesticides Chlordanes - Total
0.001
mg/L
< 0.001
< 0.001
< 0.001
-
4.4'-DDD 4.4'-DDE
0.0001 0.0001
mg/L mg/L
< 0.0001 < 0.0001
< 0.0001 < 0.0001
< 0.0001 < 0.0001
-
4.4'-DDT a-BHC Aldrin
0.0001 0.0001 0.0001
mg/L mg/L mg/L
< 0.0001 < 0.0001 < 0.0001
< 0.0001 < 0.0001 < 0.0001
< 0.0001 < 0.0001 < 0.0001
-
b-BHC
0.0001
mg/L
< 0.0001
< 0.0001
< 0.0001
-
d-BHC Dieldrin
0.0001 0.0001
mg/L mg/L
< 0.0001 < 0.0001
< 0.0001 < 0.0001
< 0.0001 < 0.0001
-
Endosulfan I
0.0001
mg/L
< 0.0001
< 0.0001
< 0.0001
-
Endosulfan II Endosulfan sulphate
0.0001 0.0001
mg/L mg/L
< 0.0001 < 0.0001
< 0.0001 < 0.0001
< 0.0001 < 0.0001
-
Endrin Endrin aldehyde Endrin ketone
0.0001 0.0001 0.0001
mg/L mg/L mg/L
< 0.0001 < 0.0001 < 0.0001
< 0.0001 < 0.0001 < 0.0001
< 0.0001 < 0.0001 < 0.0001
-
g-BHC (Lindane)
0.0001
mg/L
< 0.0001
< 0.0001
< 0.0001
-
Heptachlor
0.0001
mg/L
< 0.0001
< 0.0001
< 0.0001
-
Heptachlor epoxide Hexachlorobenzene
0.0001 0.0001
mg/L mg/L
< 0.0001 < 0.0001
< 0.0001 < 0.0001
< 0.0001 < 0.0001
-
Methoxychlor
0.0001
mg/L
< 0.0001
< 0.0001
< 0.0001
-
0.01 1
mg/L %
< 0.01 80
< 0.01 83
< 0.01 63
-
1
%
88
61
51
-
Bolstar Chlorpyrifos
0.002 0.002
mg/L mg/L
< 0.002 < 0.002
< 0.002 < 0.002
< 0.002 < 0.002
-
Demeton-O Diazinon
0.002 0.002
mg/L mg/L
< 0.002 < 0.002
< 0.002 < 0.002
< 0.002 < 0.002
-
Dichlorvos
0.002
mg/L
< 0.002
< 0.002
< 0.002
-
Disulfoton
0.002
mg/L
< 0.002
< 0.002
< 0.002
-
Ethion Ethoprop
0.002 0.002
mg/L mg/L
< 0.002 < 0.002
< 0.002 < 0.002
< 0.002 < 0.002
-
Fenitrothion
0.002
mg/L
< 0.002
< 0.002
< 0.002
-
Fensulfothion Fenthion
0.002 0.002
mg/L mg/L
< 0.002 < 0.002
< 0.002 < 0.002
< 0.002 < 0.002
-
Merphos
0.002
mg/L
< 0.002
< 0.002
< 0.002
-
Methyl azinphos Methyl parathion Mevinphos
0.002 0.002 0.002
mg/L mg/L mg/L
< 0.002 < 0.002 < 0.002
< 0.002 < 0.002 < 0.002
< 0.002 < 0.002 < 0.002
-
Naled Phorate Ronnel
0.002 0.002 0.002
mg/L mg/L mg/L
< 0.002 < 0.002 < 0.002
< 0.002 < 0.002 < 0.002
< 0.002 < 0.002 < 0.002
-
Toxaphene Dibutylchlorendate (surr.) Tetrachloro-m-xylene (surr.) Organophosphorous Pesticides
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 2 of 14 Report Number: 454407-W
Sample Matrix
53217_MW1_1 53217_MW2_1 53217_MW3_1 53217_QC9_16 60415 60415 60415 0415 Water Water Water Water
Eurofins | mgt Sample No.
B15-Ap13034
B15-Ap13035
B15-Ap13036
B15-Ap13037
Apr 16, 2015
Apr 16, 2015
Apr 16, 2015
Apr 16, 2015
Client Sample ID
Date Sampled Test/Reference Organophosphorous Pesticides
LOR
Unit
Tokuthion Trichloronate
0.002 0.002
mg/L mg/L
< 0.002 < 0.002
< 0.002 < 0.002
< 0.002 < 0.002
-
1
%
64
52
57
-
Aroclor-1016
0.001
mg/L
< 0.001
< 0.001
< 0.001
-
Aroclor-1221 Aroclor-1232
0.001 0.001
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
-
Aroclor-1242
0.001
mg/L
< 0.001
< 0.001
< 0.001
-
Aroclor-1248 Aroclor-1254
0.001 0.001
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
< 0.001 < 0.001
-
Aroclor-1260 Total PCB* Dibutylchlorendate (surr.)
0.001 0.001 1
mg/L mg/L %
< 0.001 < 0.001 80
< 0.001 < 0.001 83
< 0.001 < 0.001 63
-
1
%
88
61
51
-
Triphenylphosphate (surr.) Polychlorinated Biphenyls
Tetrachloro-m-xylene (surr.) Heavy Metals Arsenic (filtered)
0.001
mg/L
< 0.001
< 0.001
0.002
< 0.001
Cadmium (filtered) Chromium (filtered)
0.0002 0.001
mg/L mg/L
< 0.0002 < 0.001
< 0.0002 < 0.001
0.0004 < 0.001
< 0.0002 < 0.001
Copper (filtered) Lead (filtered) Mercury (filtered)
0.001 0.001 0.0001
mg/L mg/L mg/L
0.007 < 0.001 < 0.0001
0.007 < 0.001 < 0.0001
0.014 < 0.001 < 0.0001
0.007 < 0.001 < 0.0001
Nickel (filtered) Zinc (filtered)
0.001 0.001
mg/L mg/L
0.006 0.080
0.005 0.064
0.010 0.14
0.005 0.060
Sample Matrix
53217_TB3_16 0415 Water
Eurofins | mgt Sample No.
B15-Ap13038
Date Sampled
Apr 16, 2015
Client Sample ID
Test/Reference BTEX
LOR
Unit
Benzene Toluene Ethylbenzene
0.001 0.001 0.001
mg/L mg/L mg/L
< 0.001 < 0.001 < 0.001
m&p-Xylenes o-Xylene
0.002 0.001
mg/L mg/L
< 0.002 < 0.001
Xylenes - Total
0.003
mg/L
< 0.003
1
%
103
0.02
mg/L
< 0.02
4-Bromofluorobenzene (surr.) Total Recoverable Hydrocarbons - 2013 NEPM Fractions TRH C6-C10
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 3 of 14 Report Number: 454407-W
Sample History Where samples are submitted/analysed over several days, the last date of extraction and analysis is reported. A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this, some of the method reference information on reports has changed. However, no substantive change has been made to our laboratory methods, and as such there is no change in the validity of current or previous results (regarding both quality and NATA accreditation). If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised results should testing be performed outside the recommended holding time.
Description
Testing Site
Extracted
Holding Time
Eurofins | mgt Suite 10 (filtered metals) Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Melbourne
Apr 23, 2015
7 Day
Melbourne
Apr 23, 2015
7 Day
Melbourne
Apr 23, 2015
7 Day
Melbourne
Apr 23, 2015
7 Day
Melbourne
Apr 23, 2015
7 Day
Melbourne
Apr 23, 2015
28 Day
Brisbane
Apr 17, 2015
14 Day
Melbourne
Apr 23, 2015
7 Day
- Method: TRH C6-C36 - LTM-ORG-2010
Total Recoverable Hydrocarbons - 2013 NEPM Fractions - Method: TRH C6-C40 - LTM-ORG-2010
Polycyclic Aromatic Hydrocarbons - Method: USEPA 8270 Polycyclic Aromatic Hydrocarbons
Organochlorine Pesticides - Method: USEPA 8081 Organochlorine Pesticides
Organophosphorous Pesticides - Method: USEPA 8270 Organophosphorus Pesticides
Metals M8 filtered - Method: USEPA 6010/6020 Heavy Metals & USEPA 7470/71 Mercury
BTEX and Naphthalene BTEX - Method: TRH C6-C40 - LTM-ORG-2010
Polychlorinated Biphenyls - Method: USEPA 8082 Polychlorinated Biphenyls
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 4 of 14 Report Number: 454407-W
ABN â&#x20AC;&#x201C; 50 005 085 521
e.mail : EnviroSales@eurofins.com.au
web : www.eurofins.com.au
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
. Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI GRAFTON 53217
Order No.: Report #: Phone: Fax:
Received: Due: Priority: Contact Name:
454407 07 3291 9700
Apr 17, 2015 1:15 PM Apr 24, 2015 5 Day John Scott
Eurofins | mgt Client Manager: Sarah Gould
X
X
X
X
X
X
BTEX and Naphthalene
X
Eurofins | mgt Suite 10 (filtered metals)
X
Total Recoverable Hydrocarbons
X
BTEX
Brisbane Laboratory - NATA Site # 20794
Metals M8 filtered
X
Polychlorinated Biphenyls
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
Polycyclic Aromatic Hydrocarbons
TRH C6-C10
HOLD
Sample Detail
X
External Laboratory Sample ID
Sample Date
Sampling Time
Matrix
LAB ID
53217_MW1_1 Apr 16, 2015 60415
4:00PM
Water
B15-Ap13034
53217_MW2_1 Apr 16, 2015 60415
4:00PM
Water
B15-Ap13035
53217_MW3_1 Apr 16, 2015 60415
4:00PM
Water
B15-Ap13036
53217_QC9_1 Apr 16, 2015 60415
4:00PM
Water
B15-Ap13037
53217_TB3_16 Apr 16, 2015 0415
4:00PM
Water
B15-Ap13038
X X
X
X
X
X
X
X X
X
X
X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 5 of 14 Report Number: 454407-W
ABN â&#x20AC;&#x201C; 50 005 085 521
Company Name: Address:
Prensa QLD&WA Level 2, 15 Mayneview St Milton QLD 4064
Project Name: Project ID:
DSI GRAFTON 53217
e.mail : EnviroSales@eurofins.com.au
web : www.eurofins.com.au
Order No.: Report #: Phone: Fax:
Melbourne 3-5 Kingston Town Close Oakleigh VIC 3166 Phone : +61 3 8564 5000 NATA # 1261 Site # 1254 & 14271
Sydney Unit F3, Building F 16 Mars Road Lane Cove West NSW 2066 Phone : +61 2 9900 8400 NATA # 1261 Site # 18217
Received: Due: Priority: Contact Name:
454407 07 3291 9700
Brisbane 1/21 Smallwood Place Murarrie QLD 4172 Phone : +61 7 3902 4600 NATA # 1261 Site # 20794
Apr 17, 2015 1:15 PM Apr 24, 2015 5 Day John Scott
Eurofins | mgt Client Manager: Sarah Gould
X
X
X
X
X
BTEX and Naphthalene
X
Eurofins | mgt Suite 10 (filtered metals)
X
Total Recoverable Hydrocarbons
X
X
BTEX
Brisbane Laboratory - NATA Site # 20794
Metals M8 filtered
X
Polychlorinated Biphenyls
Laboratory where analysis is conducted Melbourne Laboratory - NATA Site # 1254 & 14271 Sydney Laboratory - NATA Site # 18217
Polycyclic Aromatic Hydrocarbons
TRH C6-C10
HOLD
Sample Detail
X
External Laboratory 53217_R3_160 Apr 16, 2015 415
4:00PM
Water
B15-Ap13039
53217_FB3_16 Apr 16, 2015 0415
4:00PM
Water
B15-Ap13040
X X
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported:Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 6 of 14 Report Number: 454407-W
Eurofins | mgt Internal Quality Control Review and Glossary General 1.
Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on request.
2.
All soil results are reported on a dry basis, unless otherwise stated.
3.
Actual LORs are matrix dependant. Quoted LORs may be raised where sample extracts are diluted due to interferences.
4.
Results are uncorrected for matrix spikes or surrogate recoveries.
5.
SVOC analysis on waters are performed on homogenised, unfiltered samples, unless noted otherwise.
6.
Samples were analysed on an 'as received' basis. 7. This report replaces any interim results previously issued.
Holding Times Please refer to 'Sample Preservation and Container Guide' for holding times (QS3001). For samples received on the last day of holding time, notification of testing requirements should have been received at least 6 hours prior to sample receipt deadlines as stated on the Sample Receipt Advice. If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues, suitably qualified results may still be reported. Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control. **NOTE: pH duplicates are reported as a range NOT as RPD
UNITS mg/kg: milligrams per Kilogram
mg/l: milligrams per litre
ug/l: micrograms per litre
ppm: Parts per million
ppb: Parts per billion
%: Percentage
org/100ml: Organisms per 100 millilitres
NTU: Nephelometric Turbidity Units
MPN/100mL: Most Probable Number of organisms per 100 millilitres
TERMS Dry
Where a moisture has been determined on a solid sample the result is expressed on a dry basis.
LOR
Limit of Reporting.
SPIKE
Addition of the analyte to the sample and reported as percentage recovery.
RPD
Relative Percent Difference between two Duplicate pieces of analysis.
LCS
Laboratory Control Sample - reported as percent recovery
CRM
Certified Reference Material - reported as percent recovery
Method Blank
In the case of solid samples these are performed on laboratory certified clean sands. In the case of water samples these are performed on de-ionised water.
Surr - Surrogate
The addition of a like compound to the analyte target and reported as percentage recovery.
Duplicate
A second piece of analysis from the same sample and reported in the same units as the result to show comparison.
Batch Duplicate
A second piece of analysis from a sample outside of the clients batch of samples but run within the laboratory batch of analysis.
Batch SPIKE
Spike recovery reported on a sample from outside of the clients batch of samples but run within the laboratory batch of analysis.
USEPA
United States Environmental Protection Agency
APHA
American Public Health Association
ASLP
Australian Standard Leaching Procedure (AS4439.3)
TCLP
Toxicity Characteristic Leaching Procedure
COC
Chain of Custody
SRA
Sample Receipt Advice
CP
Client Parent - QC was performed on samples pertaining to this report
NCP
Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within
TEQ
Toxic Equivalency Quotient
QC - ACCEPTANCE CRITERIA RPD Duplicates: Global RPD Duplicates Acceptance Criteria is 30% however the following acceptance guidelines are equally applicable: Results <10 times the LOR : No Limit Results between 10-20 times the LOR : RPD must lie between 0-50% Results >20 times the LOR : RPD must lie between 0-30% Surrogate Recoveries : Recoveries must lie between 50-150% - Phenols 20-130%.
QC DATA GENERAL COMMENTS 1.
Where a result is reported as a less than (<), higher than the nominated LOR, this is due to either matrix interference, extract dilution required due to interferences or contaminant levels within
2.
Duplicate data shown within this report that states the word "BATCH" is a Batch Duplicate from outside of your sample batch, but within the laboratory sample batch at a 1:10 ratio. The Parent and Duplicate data shown is not data from your samples.
3.
Organochlorine Pesticide analysis - where reporting LCS data, Toxophene & Chlordane are not added to the LCS.
4.
Organochlorine Pesticide analysis - where reporting Spike data, Toxophene is not added to the Spike.
5.
Total Recoverable Hydrocarbons - where reporting Spike & LCS data, a single spike of commercial Hydrocarbon products in the range of C12-C30 is added and it's Total Recovery is reported in the C10-C14 cell of the Report.
6.
pH and Free Chlorine analysed in the laboratory - Analysis on this test must begin within 30 minutes of sampling.Therefore laboratory analysis is unlikely to be completed within holding time. Analysis will begin as soon as possible after sample receipt.
7.
Recovery Data (Spikes & Surrogates) - where chromatographic interference does not allow the determination of Recovery the term "INT" appears against that analyte.
8.
Polychlorinated Biphenyls are spiked only using Arochlor 1260 in Matrix Spikes and LCS's.
9.
For Matrix Spikes and LCS results a dash " -" in the report means that the specific analyte was not added to the QC sample.
the sample, high moisture content or insufficient sample provided.
10. Duplicate RPD's are calculated from raw analytical data thus it is possible to have two sets of data.
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 7 of 14 Report Number: 454407-W
Quality Control Results
Test
Acceptance Pass Qualifying Limits Limits Code
Units
Result 1
TRH C6-C9 TRH C10-C14 TRH C15-C28
mg/L mg/L mg/L
< 0.02 < 0.05 < 0.1
0.02 0.05 0.1
Pass Pass Pass
TRH C29-C36 Method Blank BTEX
mg/L
< 0.1
0.1
Pass
Benzene
mg/L
< 0.001
0.001
Pass
Toluene Ethylbenzene m&p-Xylenes
mg/L mg/L mg/L
< 0.001 < 0.001 < 0.002
0.001 0.001 0.002
Pass Pass Pass
o-Xylene Xylenes - Total
mg/L mg/L
< 0.001 < 0.003
0.001 0.003
Pass Pass
Naphthalene TRH C6-C10
mg/L mg/L
< 0.02 < 0.02
0.02 0.02
Pass Pass
TRH C6-C10 less BTEX (F1) TRH >C10-C16 TRH >C16-C34
mg/L mg/L mg/L
< 0.02 < 0.05 < 0.1
0.02 0.05 0.1
Pass Pass Pass
TRH >C34-C40
mg/L
< 0.1
0.1
Pass
Method Blank Total Recoverable Hydrocarbons - 1999 NEPM Fractions
Method Blank Total Recoverable Hydrocarbons - 2013 NEPM Fractions
Method Blank Polycyclic Aromatic Hydrocarbons Acenaphthene
mg/L
< 0.001
0.001
Pass
Acenaphthylene Anthracene
mg/L mg/L
< 0.001 < 0.001
0.001 0.001
Pass Pass
Benz(a)anthracene
mg/L
< 0.001
0.001
Pass
Benzo(a)pyrene Benzo(b&j)fluoranthene Benzo(g.h.i)perylene Benzo(k)fluoranthene Chrysene
mg/L mg/L mg/L mg/L mg/L
< 0.001 < 0.001 < 0.001 < 0.001 < 0.001
0.001 0.001 0.001 0.001 0.001
Pass Pass Pass Pass Pass
Dibenz(a.h)anthracene
mg/L
< 0.001
0.001
Pass
Fluoranthene Fluorene Indeno(1.2.3-cd)pyrene
mg/L mg/L mg/L
< 0.001 < 0.001 < 0.001
0.001 0.001 0.001
Pass Pass Pass
Naphthalene Phenanthrene
mg/L mg/L
< 0.001 < 0.001
0.001 0.001
Pass Pass
Pyrene
mg/L
< 0.001
0.001
Pass
Method Blank Organochlorine Pesticides Chlordanes - Total
mg/L
< 0.001
0.001
Pass
4.4'-DDD
mg/L
< 0.0001
0.0001
Pass
4.4'-DDE 4.4'-DDT a-BHC
mg/L mg/L mg/L
< 0.0001 < 0.0001 < 0.0001
0.0001 0.0001 0.0001
Pass Pass Pass
Aldrin b-BHC
mg/L mg/L
< 0.0001 < 0.0001
0.0001 0.0001
Pass Pass
d-BHC
mg/L
< 0.0001
0.0001
Pass
Dieldrin Endosulfan I
mg/L mg/L
< 0.0001 < 0.0001
0.0001 0.0001
Pass Pass
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 8 of 14 Report Number: 454407-W
Test
Acceptance Pass Qualifying Limits Limits Code 0.0001 Pass
Units
Result 1
Endosulfan II
mg/L
< 0.0001
Endosulfan sulphate Endrin Endrin aldehyde
mg/L mg/L mg/L
< 0.0001 < 0.0001 < 0.0001
0.0001 0.0001 0.0001
Pass Pass Pass
Endrin ketone
mg/L
< 0.0001
0.0001
Pass
g-BHC (Lindane) Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor
mg/L mg/L mg/L mg/L mg/L
< 0.0001 < 0.0001 < 0.0001 < 0.0001 < 0.0001
0.0001 0.0001 0.0001 0.0001 0.0001
Pass Pass Pass Pass Pass
Toxaphene
mg/L
< 0.01
0.01
Pass
Bolstar Chlorpyrifos Demeton-O
mg/L mg/L mg/L
< 0.002 < 0.002 < 0.002
0.002 0.002 0.002
Pass Pass Pass
Diazinon
mg/L
< 0.002
0.002
Pass
Dichlorvos
mg/L
< 0.002
0.002
Pass
Disulfoton Ethion
mg/L mg/L
< 0.002 < 0.002
0.002 0.002
Pass Pass
Ethoprop Fenitrothion Fensulfothion
mg/L mg/L mg/L
< 0.002 < 0.002 < 0.002
0.002 0.002 0.002
Pass Pass Pass
Fenthion
mg/L
< 0.002
0.002
Pass
Merphos Methyl azinphos
mg/L mg/L
< 0.002 < 0.002
0.002 0.002
Pass Pass
Methyl parathion
mg/L
< 0.002
0.002
Pass
Mevinphos Naled
mg/L mg/L
< 0.002 < 0.002
0.002 0.002
Pass Pass
Phorate
mg/L
< 0.002
0.002
Pass
Ronnel Tokuthion
mg/L mg/L
< 0.002 < 0.002
0.002 0.002
Pass Pass
Trichloronate
mg/L
< 0.002
0.002
Pass
Method Blank Organophosphorous Pesticides
Method Blank Polychlorinated Biphenyls Aroclor-1016
mg/L
< 0.001
0.001
Pass
Aroclor-1221
mg/L
< 0.001
0.001
Pass
Aroclor-1232 Aroclor-1242
mg/L mg/L
< 0.001 < 0.001
0.001 0.001
Pass Pass
Aroclor-1248 Aroclor-1254
mg/L mg/L
< 0.001 < 0.001
0.001 0.001
Pass Pass
Aroclor-1260 Total PCB*
mg/L mg/L
< 0.001 < 0.001
0.001 0.001
Pass Pass
Method Blank Heavy Metals Arsenic (filtered)
mg/L
< 0.001
0.001
Pass
Cadmium (filtered) Chromium (filtered)
mg/L mg/L
< 0.0002 < 0.001
0.0002 0.001
Pass Pass
Copper (filtered) Lead (filtered) Mercury (filtered)
mg/L mg/L mg/L
< 0.001 < 0.001 < 0.0001
0.001 0.001 0.0001
Pass Pass Pass
Nickel (filtered)
mg/L
< 0.001
0.001
Pass
mg/L
< 0.001
0.001
Pass
Zinc (filtered) LCS - % Recovery
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 9 of 14 Report Number: 454407-W
Test
Acceptance Pass Qualifying Limits Limits Code
Units
Result 1
% %
114 101
70-130 70-130
Pass Pass
% % % % %
107 108 108 106 107
70-130 70-130 70-130 70-130 70-130
Pass Pass Pass Pass Pass
%
109
70-130
Pass
%
100
70-130
Pass
Acenaphthene
%
89
70-130
Pass
Acenaphthylene
%
92
70-130
Pass
Anthracene Benz(a)anthracene
% %
85 112
70-130 70-130
Pass Pass
Benzo(a)pyrene Benzo(b&j)fluoranthene Benzo(g.h.i)perylene
% % %
110 106 110
70-130 70-130 70-130
Pass Pass Pass
Benzo(k)fluoranthene
%
119
70-130
Pass
Chrysene Dibenz(a.h)anthracene
% %
115 117
70-130 70-130
Pass Pass
Fluoranthene
%
107
70-130
Pass
Fluorene Indeno(1.2.3-cd)pyrene
% %
94 118
70-130 70-130
Pass Pass
Naphthalene
%
88
70-130
Pass
Phenanthrene Pyrene
% %
93 115
70-130 70-130
Pass Pass
4.4'-DDD 4.4'-DDE
% %
113 111
70-130 70-130
Pass Pass
4.4'-DDT
%
81
70-130
Pass
a-BHC Aldrin
% %
79 88
70-130 70-130
Pass Pass
b-BHC d-BHC
% %
102 84
70-130 70-130
Pass Pass
Dieldrin Endosulfan I
% %
124 110
70-130 70-130
Pass Pass
Endosulfan II Endosulfan sulphate
% %
118 113
70-130 70-130
Pass Pass
Endrin
%
112
70-130
Pass
Endrin aldehyde Endrin ketone
% %
108 93
70-130 70-130
Pass Pass
g-BHC (Lindane) Heptachlor Heptachlor epoxide Hexachlorobenzene
% % % %
92 73 95 90
70-130 70-130 70-130 70-130
Pass Pass Pass Pass
%
72
70-130
Pass
Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 TRH C10-C14 LCS - % Recovery BTEX Benzene Toluene Ethylbenzene m&p-Xylenes Xylenes - Total LCS - % Recovery Total Recoverable Hydrocarbons - 2013 NEPM Fractions TRH C6-C10 TRH >C10-C16 LCS - % Recovery Polycyclic Aromatic Hydrocarbons
LCS - % Recovery Organochlorine Pesticides
Methoxychlor LCS - % Recovery
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 10 of 14 Report Number: 454407-W
Test
Acceptance Pass Qualifying Limits Limits Code
Units
Result 1
Diazinon Ethion Fenitrothion
% % %
74 90 80
Methyl parathion
%
70
70-130
Pass
Mevinphos LCS - % Recovery Heavy Metals Arsenic (filtered) Cadmium (filtered)
%
118
70-130
Pass
% %
98 98
80-120 80-120
Pass Pass
Chromium (filtered)
%
97
80-120
Pass
Copper (filtered) Lead (filtered)
% %
97 98
80-120 80-120
Pass Pass
Mercury (filtered) Nickel (filtered) Zinc (filtered)
% % %
110 98 99
Units
Result 1
%
Result 1 106
Organophosphorous Pesticides
Test
Lab Sample ID
QA Source
70-130 70-130 70-130
Pass Pass Pass
70-130 Pass 80-120 Pass 80-120 Pass Acceptance Pass Qualifying Limits Limits Code
Spike - % Recovery Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C10-C14 M15-Ap13637 NCP
70-130
Pass
70-130
Pass
Spike - % Recovery Total Recoverable Hydrocarbons - 2013 NEPM Fractions TRH >C10-C16 Spike - % Recovery
Result 1
M15-Ap13637
NCP
%
4.4'-DDD
M15-Ap01669
NCP
%
102
70-130
Pass
4.4'-DDE
M15-Ap01669
NCP
%
119
70-130
Pass
4.4'-DDT
M15-Ap01669
NCP
%
89
70-130
Pass
a-BHC
M15-Ap01669
NCP
%
97
70-130
Pass
Aldrin b-BHC
M15-Ap01669 M15-Ap01669
NCP NCP
% %
120 113
70-130 70-130
Pass Pass
d-BHC Dieldrin
M15-Ap01669 M15-Ap01669
NCP NCP
% %
82 120
70-130 70-130
Pass Pass
Endosulfan I
M15-Ap01669
NCP
%
125
70-130
Pass
Endosulfan II
M15-Ap01669
NCP
%
111
70-130
Pass
Endosulfan sulphate
M15-Ap01669
NCP
%
98
70-130
Pass
Endrin Endrin aldehyde Endrin ketone
M15-Ap01669 M15-Ap01669 M15-Ap01669
NCP NCP NCP
% % %
117 124 89
70-130 70-130 70-130
Pass Pass Pass
g-BHC (Lindane)
M15-Ap01669
NCP
%
96
70-130
Pass
Heptachlor
M15-Ap01669
NCP
%
85
70-130
Pass
Heptachlor epoxide
M15-Ap01669
NCP
%
105
70-130
Pass
Hexachlorobenzene
M15-Ap01669
NCP
%
106
70-130
Pass
Methoxychlor Spike - % Recovery
M15-Ap01669
NCP
%
101
70-130
Pass
Arsenic (filtered)
B15-Ap13034
CP
%
98
70-130
Pass
Cadmium (filtered)
B15-Ap13034
CP
%
96
70-130
Pass
Chromium (filtered)
B15-Ap13034
CP
%
95
70-130
Pass
Copper (filtered)
B15-Ap13034
CP
%
94
70-130
Pass
Lead (filtered) Mercury (filtered)
B15-Ap13034 M15-Ap16288
CP NCP
% %
94 77
70-130 70-130
Pass Pass
Nickel (filtered)
B15-Ap13034
CP
%
96
70-130
Pass
Zinc (filtered)
B15-Ap13034
CP
%
88
70-130
Pass
Organochlorine Pesticides
104 Result 1
Heavy Metals
Result 1
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 11 of 14 Report Number: 454407-W
Test
Lab Sample ID
QA Source
Acceptance Pass Qualifying Limits Limits Code
Units
Result 1
mg/L
Result 1 < 0.05
Result 2 < 0.05
RPD <1
Duplicate Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C10-C14 M15-Ap13636 NCP
30%
Pass
TRH C15-C28
M15-Ap13636
NCP
mg/L
< 0.1
< 0.1
<1
30%
Pass
TRH C29-C36
M15-Ap13636
NCP
mg/L
< 0.1
< 0.1
<1
30%
Pass
mg/L mg/L mg/L
Result 1 < 0.05 < 0.1 < 0.1
Result 2 < 0.05 < 0.1 < 0.1
RPD <1 <1 <1
30% 30% 30%
Pass Pass Pass
Duplicate Total Recoverable Hydrocarbons - 2013 NEPM Fractions TRH >C10-C16 M15-Ap13636 NCP TRH >C16-C34 M15-Ap13636 NCP TRH >C34-C40 M15-Ap13636 NCP Duplicate Organochlorine Pesticides Chlordanes - Total
M15-Ap10962
NCP
mg/L
Result 1 < 0.001
Result 2 < 0.001
RPD <1
30%
Pass
4.4'-DDD 4.4'-DDE 4.4'-DDT
M15-Ap10962 M15-Ap10962 M15-Ap10962
NCP NCP NCP
mg/L mg/L mg/L
< 0.0001 < 0.0001 < 0.0001
< 0.0001 < 0.0001 < 0.0001
<1 <1 <1
30% 30% 30%
Pass Pass Pass
a-BHC
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
Aldrin
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
b-BHC
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
d-BHC
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
Dieldrin Endosulfan I
M15-Ap10962 M15-Ap10962
NCP NCP
mg/L mg/L
< 0.0001 < 0.0001
< 0.0001 < 0.0001
<1 <1
30% 30%
Pass Pass
Endosulfan II
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
Endosulfan sulphate
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
Endrin
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
Endrin aldehyde
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
Endrin ketone
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
g-BHC (Lindane) Heptachlor
M15-Ap10962 M15-Ap10962
NCP NCP
mg/L mg/L
< 0.0001 < 0.0001
< 0.0001 < 0.0001
<1 <1
30% 30%
Pass Pass Pass
Heptachlor epoxide
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Hexachlorobenzene
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
Methoxychlor
M15-Ap10962
NCP
mg/L
< 0.0001
< 0.0001
<1
30%
Pass
M15-Ap10962
NCP
mg/L
< 0.01
< 0.01
<1
30%
Pass
M15-Ap10962 M15-Ap10962 M15-Ap10962 M15-Ap10962 M15-Ap10962 M15-Ap10962
NCP NCP NCP NCP NCP NCP
mg/L mg/L mg/L mg/L mg/L mg/L
Result 1 < 0.001 < 0.001 < 0.001 < 0.001 < 0.001 < 0.001
Result 2 < 0.001 < 0.001 < 0.001 < 0.001 < 0.001 < 0.001
RPD <1 <1 <1 <1 <1 <1
30% 30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass Pass
M15-Ap10962 M15-Ap10962
NCP NCP
mg/L mg/L
< 0.001 < 0.001
< 0.001 < 0.001
<1 <1
30% 30%
Pass Pass
Result 1
Result 2
RPD
Arsenic (filtered) Cadmium (filtered)
B15-Ap13034 B15-Ap13034
CP CP
mg/L mg/L
< 0.001 < 0.0002
< 0.001 < 0.0002
<1 <1
30% 30%
Pass Pass
Chromium (filtered) Copper (filtered) Lead (filtered) Mercury (filtered)
B15-Ap13034 B15-Ap13034 B15-Ap13034 B15-Ap13034
CP CP CP CP
mg/L mg/L mg/L mg/L
< 0.001 0.007 < 0.001 < 0.0001
< 0.001 0.006 < 0.001 < 0.0001
<1 2.0 <1 <1
30% 30% 30% 30%
Pass Pass Pass Pass
Nickel (filtered) Zinc (filtered)
B15-Ap13034 B15-Ap13034
CP CP
mg/L mg/L
0.006 0.080
0.006 0.080
4.0 1.0
30% 30%
Pass Pass
Toxaphene Duplicate Polychlorinated Biphenyls Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260 Total PCB* Duplicate Heavy Metals
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 12 of 14 Report Number: 454407-W
Duplicate Total Recoverable Hydrocarbons - 1999 NEPM Fractions TRH C6-C9 B15-Ap13035 CP
mg/L
Result 1 < 0.02
Result 2 < 0.02
RPD <1
30%
Pass
Duplicate BTEX
Result 1
Result 2
RPD
CP CP CP CP CP CP
mg/L mg/L mg/L mg/L mg/L mg/L
< 0.001 < 0.001 < 0.001 < 0.002 < 0.001 < 0.003
< 0.001 < 0.001 < 0.001 < 0.002 < 0.001 < 0.003
<1 <1 <1 <1 <1 <1
30% 30% 30% 30% 30% 30%
Pass Pass Pass Pass Pass Pass
Duplicate Total Recoverable Hydrocarbons - 2013 NEPM Fractions Naphthalene B15-Ap13035 CP TRH C6-C10 B15-Ap13035 CP TRH C6-C10 less BTEX (F1) B15-Ap13035 CP
mg/L mg/L mg/L
Result 1 < 0.02 < 0.02 < 0.02
Result 2 < 0.02 < 0.02 < 0.02
RPD <1 <1 <1
30% 30% 30%
Pass Pass Pass
Benzene Toluene Ethylbenzene m&p-Xylenes o-Xylene Xylenes - Total
B15-Ap13035 B15-Ap13035 B15-Ap13035 B15-Ap13035 B15-Ap13035 B15-Ap13035
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 13 of 14 Report Number: 454407-W
Comments Sample Integrity Custody Seals Intact (if used)
N/A
Attempt to Chill was evident
Yes
Sample correctly preserved
Yes
Appropriate sample containers have been used
Yes
Sample containers for volatile analysis received with minimal headspace
Yes
Samples received within HoldingTime
Yes
Some samples have been subcontracted
No
Qualifier Codes/Comments Code Description N01
F2 is determined by arithmetically subtracting the "naphthalene" value from the ">C10-C16" value. The naphthalene value used in this calculation is obtained from volatiles (Purge & Trap analysis).
N02
Where we have reported both volatile (P&T GCMS) and semivolatile (GCMS) naphthalene data, results may not be identical. Provided correct sample handling protocols have been followed, any observed differences in results are likely to be due to procedural differences within each methodology. Results determined by both techniques have passed all QAQC acceptance criteria, and are entirely technically valid.
N04
F1 is determined by arithmetically subtracting the "Total BTEX" value from the "C6-C10" value. The "Total BTEX" value is obtained by summing the concentrations of BTEX analytes. The "C6-C10" value is obtained by quantitating against a standard of mixed aromatic/aliphatic analytes.
N07
Please note:- These two PAH isomers closely co-elute using the most contemporary analytical methods and both the reported concentration (and the TEQ) apply specifically to the total of the two co-eluting PAHs
Authorised By Sarah Gould
Analytical Services Manager
Carroll Lee
Senior Analyst-Organic (VIC)
Emily Rosenberg
Senior Analyst-Metal (VIC)
Richard Corner
Senior Analyst-Volatile (QLD)
Glenn Jackson National Laboratory Manager - Indicates Not Requested * Indicates NATA accreditation does not cover the performance of this service Uncertainty data is available on request Eurofins | mgt shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretation given in this report. In no case shall Eurofins | mgt be liable for consequential damages including, but not limited to, lost profits, damages for failure to meet deadlines and lost production arising from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.
Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172 Date Reported: Apr 27, 2015
ABN : 50 005 085 521 Telephone: +61 7 3902 4600 Facsimile: +61 7 3902 4646
Page 14 of 14 Report Number: 454407-W
True
QA/QC Compliance Assessment for DQO Reporting Work Order
: EB1517053
Page
: 1 of 4
Client Contact
: PRENSA
Laboratory
: Environmental Division Brisbane
: JOHN SCOTT
Telephone
: +61-7-3243 7222
Project
: 53217 G0038
Date Samples Received
: 20-Apr-2015
Site
: ----
Issue Date
: 27-Apr-2015
Sampler
: JOHN SCOTT
No. of samples received
:1
Order number
: ----
No. of samples analysed
:1
This report is automatically generated by the ALS LIMS through interpretation of the ALS Quality Control Report and several Quality Assurance parameters measured by ALS. This automated reporting highlights any non-conformances, facilitates faster and more accurate data validation and is designed to assist internal expert and external Auditor review. Many components of this report contribute to the overall DQO assessment and reporting for guideline compliance.
Brief method summaries and references are also provided to assist in traceability.
Summary of Outliers Outliers : Quality Control Samples This report highlights outliers flagged in the Quality Control (QC) Report.
l
NO Method Blank value outliers occur.
l
NO Duplicate outliers occur.
l
NO Laboratory Control outliers occur.
l
NO Matrix Spike outliers occur.
l
For all regular sample matrices, NO surrogate recovery outliers occur.
Outliers : Analysis Holding Time Compliance l
NO Analysis Holding Time Outliers exist.
Outliers : Frequency of Quality Control Samples l
Quality Control Sample Frequency Outliers exist - please see following pages for full details.
RIGHT SOLUTIONS | RIGHT PARTNER
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: : : :
2 of 4 EB1517053 PRENSA 53217 G0038
Outliers : Frequency of Quality Control Samples Matrix: WATER Quality Control Sample Type Method
Count QC
Quality Control Specification
Rate (%) Regular
Actual
Expected
Matrix Spikes (MS) PAH/Phenols (GC/MS - SIM)
0
3
0.00
5.00
NEPM 2013 Schedule B(3) and ALS QCS3 requirement
TRH - Semivolatile Fraction
0
16
0.00
5.00
NEPM 2013 Schedule B(3) and ALS QCS3 requirement
Analysis Holding Time Compliance This report summarizes extraction / preparation and analysis times and compares each with ALS recommended holding times (referencing USEPA SW 846, APHA, AS and NEPM) based on the sample container provided. Dates reported represent first date of extraction or analysis and preclude subsequent dilutions and reruns. A listing of breaches (if any) is provided herein. Holding time for leachate methods (e.g. TCLP) vary according to the analytes reported. Assessment compares the leach date with the shortest analyte holding time for the equivalent soil method. These are: 14 days, mercury 28 days & other metals 180 days. A recorded breach does not guarantee a breach for all non-volatile parameters. Holding times for VOC in soils vary according to analytes of interest. Vinyl Chloride and Styrene holding time is 7 days; others 14 days. should be verified in case the reported breach is a false positive or Vinyl Chloride and Styrene are not key analytes of interest/concern.
A recorded breach does not guarantee a breach for all VOC analytes and Evaluation: û = Holding time breach ; ü = Within holding time.
Matrix: WATER Method
organics
Extraction / Preparation
Sample Date
Container / Client Sample ID(s)
Analysis
Date extracted
Due for extraction
Evaluation
Date analysed
Due for analysis
Evaluation
EG020F: Dissolved Metals by ICP-MS Miscellanous Nitric Preserved - field filtered (EG020A-F) 53217_QC10_160415
16-Apr-2015
----
----
----
22-Apr-2015
13-Oct-2015
ü
EG035F: Dissolved Mercury by FIMS Miscellanous Nitric Preserved - field filtered (EG035F) 53217_QC10_160415
16-Apr-2015
----
----
----
22-Apr-2015
14-May-2015
ü
EP080/071: Total Petroleum Hydrocarbons Miscellaneous Glass Bottle - unpreserved (EP071) 53217_QC10_160415
16-Apr-2015
22-Apr-2015
23-Apr-2015
ü
24-Apr-2015
01-Jun-2015
ü
EP075(SIM)T: PAH Surrogates Miscellaneous Glass Bottle - unpreserved (EP075(SIM)) 53217_QC10_160415
16-Apr-2015
22-Apr-2015
23-Apr-2015
ü
24-Apr-2015
01-Jun-2015
ü
EP080S: TPH(V)/BTEX Surrogates Amber VOC Vial - Sulfuric Acid (EP080) 53217_QC10_160415
16-Apr-2015
23-Apr-2015
30-Apr-2015
ü
23-Apr-2015
30-Apr-2015
ü
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: : : :
3 of 4 EB1517053 PRENSA 53217 G0038
Quality Control Parameter Frequency Compliance The following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which the submitted sample(s) was(were) processed. Actual rate should be greater than or equal to the expected rate. A listing of breaches is provided in the Summary of Outliers. Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.
Matrix: WATER Quality Control Sample Type
Analytical Methods Laboratory Duplicates (DUP) Dissolved Mercury by FIMS
Count Method
QC
Regular
Actual
Rate (%) Expected
EG035F
2
12
16.67
10.00
EG020A-F
2
20
10.00
10.00
EP075(SIM)
1
3
33.33
10.00
TRH - Semivolatile Fraction
EP071
2
16
12.50
10.00
TRH Volatiles/BTEX
EP080
2
20
10.00
10.00
Dissolved Metals by ICP-MS - Suite A PAH/Phenols (GC/MS - SIM)
Laboratory Control Samples (LCS) Dissolved Mercury by FIMS Dissolved Metals by ICP-MS - Suite A PAH/Phenols (GC/MS - SIM)
EG035F
1
12
8.33
5.00
EG020A-F
1
20
5.00
5.00
3
33.33
5.00
EP075(SIM)
1
TRH - Semivolatile Fraction
EP071
1
16
6.25
5.00
TRH Volatiles/BTEX
EP080
1
20
5.00
5.00
Method Blanks (MB) Dissolved Mercury by FIMS
EG035F
1
12
8.33
5.00
EG020A-F
1
20
5.00
5.00
EP075(SIM)
1
3
33.33
5.00
TRH - Semivolatile Fraction
EP071
1
16
6.25
5.00
TRH Volatiles/BTEX
EP080
1
20
5.00
5.00
Dissolved Metals by ICP-MS - Suite A PAH/Phenols (GC/MS - SIM)
Matrix Spikes (MS) Dissolved Mercury by FIMS
EG035F
1
12
8.33
5.00
EG020A-F
1
20
5.00
5.00
EP075(SIM)
0
3
0.00
5.00
TRH - Semivolatile Fraction
EP071
0
16
0.00
5.00
TRH Volatiles/BTEX
EP080
1
20
5.00
5.00
Dissolved Metals by ICP-MS - Suite A PAH/Phenols (GC/MS - SIM)
Quality Control Specification Evaluation
ü ü ü ü ü
NEPM 2013 Schedule B(3) and ALS QCS3 requirement
ü ü ü ü ü
NEPM 2013 Schedule B(3) and ALS QCS3 requirement
ü ü ü ü ü
NEPM 2013 Schedule B(3) and ALS QCS3 requirement
ü ü û û ü
NEPM 2013 Schedule B(3) and ALS QCS3 requirement
NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement
NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement
NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement
NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement NEPM 2013 Schedule B(3) and ALS QCS3 requirement
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: : : :
4 of 4 EB1517053 PRENSA 53217 G0038
Brief Method Summaries The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.
Analytical Methods
Method
Matrix
EG020A-F
WATER
Dissolved Mercury by FIMS
EG035F
WATER
TRH - Semivolatile Fraction
EP071
WATER
EP075(SIM)
WATER
EP080
WATER
Dissolved Metals by ICP-MS - Suite A
PAH/Phenols (GC/MS - SIM)
TRH Volatiles/BTEX
Method Descriptions
In house: Referenced to APHA 21st ed., 3125; USEPA SW846 - 6020, ALS QWI-EN/EG020. Samples are 0.45 um filtered prior to analysis. The ICPMS technique utilizes a highly efficient argon plasma to ionize selected elements. Ions are then passed into a high vacuum mass spectrometer, which separates the analytes based on their distinct mass to charge ratios prior to their measurement by a discrete dynode ion detector. In house: Referenced to AS 3550, APHA 21st ed. 3112 Hg - B (Flow-injection (SnCl2)(Cold Vapour generation) AAS) Samples are 0.45 um filtered prior to analysis. FIM-AAS is an automated flameless atomic absorption technique. A bromate/bromide reagent is used to oxidise any organic mercury compounds in the filtered sample. The ionic mercury is reduced online to atomic mercury vapour by SnCl2 which is then purged into a heated quartz cell. Quantification is by comparing absorbance against a calibration curve. This method is compliant with NEPM (2013) Schedule B(3) USEPA SW 846 - 8015A The sample extract is analysed by Capillary GC/FID and quantification is by comparison against an established 5 point calibration curve of n-Alkane standards. This method is compliant with the QC requirements of NEPM (2013) Schedule B(3) USEPA SW 846 - 8270D Sample extracts are analysed by Capillary GC/MS in SIM Mode and quantification is by comparison against an established 5 point calibration curve. This method is compliant with NEPM (2013) Schedule B(3) USEPA SW 846 - 8260B Water samples are directly purged prior to analysis by Capillary GC/MS and quantification is by comparison against an established 5 point calibration curve. Alternatively, a sample is equilibrated in a headspace vial and a portion of the headspace determined by GCMS analysis. This method is compliant with the QC requirements of NEPM (2013) Schedule B(3)
3.00 3 True False
QUALITY CONTROL REPORT EB1517053
Page
: 1 of 7
: PRENSA
Laboratory
: Environmental Division Brisbane
Contact
: JOHN SCOTT
Contact
: Customer Services EB
Address
: LEVEL 2 16 DOUGLAS STREET
Address
: 2 Byth Street Stafford QLD Australia 4053
: ALSEnviro.Brisbane@alsglobal.com
Telephone
: +61-7-3243 7222
Facsimile
: +61-7-3243 7218
QC Level
: NEPM 2013 Schedule B(3) and ALS QCS3 requirement
Date Samples Received
: 20-Apr-2015
: ----
Date Analysis Commenced
: 21-Apr-2015
Sampler
: JOHN SCOTT
Issue Date
: 27-Apr-2015
Site
: ----
No. of samples received
:1
Quote number
: ----
No. of samples analysed
:1
Work Order
:
Client
:
Telephone
:
Facsimile
:
Project
:
Order number
:
C-O-C number
MILTON QLD, AUSTRALIA 4064 john.scott@prensa.com.au +61 03 9508 0100 +61 03 9509 6125 53217 G0038 ----
This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This Quality Control Report contains the following information: l Laboratory Duplicate (DUP) Report ; Relative Percentage Difference (RPD) and Acceptance Limits l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits l Matrix Spike (MS) Report ; Recovery and Acceptance Limits NATA Accredited Laboratory 825 Accredited for compliance with ISO/IEC 17025.
Signatories This document has been electronically signed by compliance with procedures specified in 21 CFR Part 11.
the
authorized
signatories
indicated
below.
Electronic
Signatories
Position
Accreditation Category
Edwandy Fadjar
Organic Coordinator
Sydney Organics
Kim McCabe
Senior Inorganic Chemist
Brisbane Inorganics
Matt Frost
Senior Organic Chemist
Brisbane Organics
RIGHT SOLUTIONS | RIGHT PARTNER
signing
has
been
carried
out
in
Page Work Order Client Project
: : : :
2 of 7 EB1517053 PRENSA 53217 G0038
General Comments The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house developed procedures are employed in the absence of documented standards or by client request. Where moisture determination has been performed, results are reported on a dry weight basis. Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high mois Key :
Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society. LOR = Limit of reporting RPD = Relative Percentage Difference # = Indicates failed QC
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: : : :
3 of 7 EB1517053 PRENSA 53217 G0038
Laboratory Duplicate (DUP) Report The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR: No Limit; Result between 10 and 20 times LOR:- 0% - 50%; Result > 20 times LOR:0% - 20%. Laboratory Duplicate (DUP) Report
Sub-Matrix: WATER Laboratory sample ID
Client sample ID
Method: Compound
CAS Number
LOR
Unit
Original Result
Duplicate Result
RPD (%)
Recovery Limits (%)
EG020F: Dissolved Metals by ICP-MS (QC Lot: 84972) EB1517043-002
EB1516810-009
Anonymous
Anonymous
EG020A-F: Cadmium
7440-43-9
0.0001
mg/L
<0.0001
<0.0001
0.00
No Limit
EG020A-F: Arsenic
7440-38-2
0.001
mg/L
0.006
0.006
0.00
No Limit
EG020A-F: Chromium
7440-47-3
0.001
mg/L
<0.001
<0.001
0.00
No Limit
EG020A-F: Copper
7440-50-8
0.001
mg/L
0.042
0.042
0.00
0% - 20%
EG020A-F: Lead
7439-92-1
0.001
mg/L
0.004
0.004
0.00
No Limit
EG020A-F: Nickel
7440-02-0
0.001
mg/L
0.004
0.004
0.00
No Limit
EG020A-F: Zinc
7440-66-6
0.005
mg/L
0.063
0.062
0.00
0% - 50%
EG020A-F: Cadmium
7440-43-9
0.0001
mg/L
<0.0001
<0.0001
0.00
No Limit
EG020A-F: Arsenic
7440-38-2
0.001
mg/L
0.002
0.002
0.00
No Limit
EG020A-F: Chromium
7440-47-3
0.001
mg/L
<0.001
<0.001
0.00
No Limit
EG020A-F: Copper
7440-50-8
0.001
mg/L
0.004
0.004
0.00
No Limit
EG020A-F: Lead
7439-92-1
0.001
mg/L
<0.001
<0.001
0.00
No Limit
EG020A-F: Nickel
7440-02-0
0.001
mg/L
<0.001
<0.001
0.00
No Limit
EG020A-F: Zinc
7440-66-6
0.005
mg/L
0.018
0.015
21.4
No Limit
EG035F: Dissolved Mercury by FIMS (QC Lot: 84973) EB1517067-006
Anonymous
EG035F: Mercury
7439-97-6
0.0001
mg/L
<0.0001
<0.0001
0.00
No Limit
EB1516810-009
Anonymous
EG035F: Mercury
7439-97-6
0.0001
mg/L
<0.0001
<0.0001
0.00
No Limit
EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QC Lot: 85195) EB1517053-001
53217_QC10_160415
EP075(SIM): Benzo(a)pyrene EP075(SIM): Benzo(a)pyrene TEQ (zero)
50-32-8
0.5
µg/L
<0.5
<0.5
0.00
No Limit
----
0.5
µg/L
<0.5
<0.5
0.00
No Limit
83-32-9
1
µg/L
<1.0
<1.0
0.00
No Limit
EP075(SIM): Acenaphthylene
208-96-8
1
µg/L
<1.0
<1.0
0.00
No Limit
EP075(SIM): Anthracene
120-12-7
1
µg/L
<1.0
<1.0
0.00
No Limit
56-55-3
1
µg/L
<1.0
<1.0
0.00
No Limit
1
µg/L
<1.0
<1.0
0.00
No Limit
EP075(SIM): Benzo(g.h.i)perylene
205-99-2 205-82-3 191-24-2
1
µg/L
<1.0
<1.0
0.00
No Limit
EP075(SIM): Benzo(k)fluoranthene
207-08-9
1
µg/L
<1.0
<1.0
0.00
No Limit
EP075(SIM): Chrysene
218-01-9
1
µg/L
<1.0
<1.0
0.00
No Limit
53-70-3
1
µg/L
<1.0
<1.0
0.00
No Limit
EP075(SIM): Acenaphthene
EP075(SIM): Benz(a)anthracene EP075(SIM): Benzo(b+j)fluoranthene
EP075(SIM): Dibenz(a.h)anthracene EP075(SIM): Fluoranthene EP075(SIM): Fluorene EP075(SIM): Indeno(1.2.3.cd)pyrene EP075(SIM): Naphthalene EP075(SIM): Phenanthrene EP075(SIM): Pyrene
206-44-0
1
µg/L
<1.0
<1.0
0.00
No Limit
86-73-7
1
µg/L
<1.0
<1.0
0.00
No Limit
193-39-5
1
µg/L
<1.0
<1.0
0.00
No Limit
91-20-3
1
µg/L
<1.0
<1.0
0.00
No Limit
85-01-8
1
µg/L
<1.0
<1.0
0.00
No Limit
129-00-0
1
µg/L
<1.0
<1.0
0.00
No Limit
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4 of 7 EB1517053 PRENSA 53217 G0038 Laboratory Duplicate (DUP) Report
Sub-Matrix: WATER Laboratory sample ID
Client sample ID
CAS Number
LOR
EP071: C15 - C28 Fraction
----
EP071: C10 - C14 Fraction
----
EP071: C29 - C36 Fraction
----
50
µg/L
<50
<50
0.00
No Limit
EP071: C15 - C28 Fraction
----
100
µg/L
<100
<100
0.00
No Limit
EP071: C10 - C14 Fraction
----
50
µg/L
<50
<50
0.00
No Limit
EP071: C29 - C36 Fraction
----
50
µg/L
<50
<50
0.00
No Limit
Method: Compound
Unit
Original Result
Duplicate Result
RPD (%)
100
µg/L
<100
<100
0.00
No Limit
50
µg/L
<50
<50
0.00
No Limit
Recovery Limits (%)
EP080/071: Total Petroleum Hydrocarbons (QC Lot: 85196) EB1517091-001
EB1517053-001
Anonymous
53217_QC10_160415
EP080/071: Total Petroleum Hydrocarbons (QC Lot: 86227) EB1517042-001
Anonymous
EB1517067-004
Anonymous
EP080: C6 - C9 Fraction
----
20
µg/L
<20
<20
0.00
No Limit
EP080: C6 - C9 Fraction
----
20
µg/L
<20
<20
0.00
No Limit
EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 85196) EB1517091-001
EB1517053-001
Anonymous
53217_QC10_160415
EP071: >C10 - C16 Fraction
>C10_C16
100
µg/L
<100
<100
0.00
No Limit
EP071: >C16 - C34 Fraction
----
100
µg/L
<100
<100
0.00
No Limit No Limit
EP071: >C34 - C40 Fraction
----
100
µg/L
<100
<100
0.00
EP071: >C10 - C16 Fraction
>C10_C16
100
µg/L
<100
<100
0.00
No Limit
EP071: >C16 - C34 Fraction
----
100
µg/L
<100
<100
0.00
No Limit
EP071: >C34 - C40 Fraction
----
100
µg/L
<100
<100
0.00
No Limit
EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 86227) EB1517042-001
Anonymous
EP080: C6 - C10 Fraction
C6_C10
20
µg/L
<20
<20
0.00
No Limit
EB1517067-004
Anonymous
EP080: C6 - C10 Fraction
C6_C10
20
µg/L
<20
<20
0.00
No Limit
No Limit
EP080: BTEXN (QC Lot: 86227) EB1517042-001
Anonymous
71-43-2
1
µg/L
<1
<1
0.00
EP080: Ethylbenzene
100-41-4
2
µg/L
<2
<2
0.00
No Limit
EP080: meta- & para-Xylene
2
µg/L
<2
<2
0.00
No Limit
EP080: ortho-Xylene
108-38-3 106-42-3 95-47-6
2
µg/L
<2
<2
0.00
No Limit
EP080: Toluene
108-88-3
2
µg/L
<2
<2
0.00
No Limit
91-20-3
5
µg/L
<5
<5
0.00
No Limit No Limit
EP080: Benzene
EP080: Naphthalene EB1517067-004
Anonymous
71-43-2
1
µg/L
<1
<1
0.00
EP080: Ethylbenzene
100-41-4
2
µg/L
<2
<2
0.00
No Limit
EP080: meta- & para-Xylene
2
µg/L
<2
<2
0.00
No Limit
EP080: ortho-Xylene
108-38-3 106-42-3 95-47-6
2
µg/L
<2
<2
0.00
No Limit
EP080: Toluene
108-88-3
2
µg/L
<2
<2
0.00
No Limit
91-20-3
5
µg/L
<5
<5
0.00
No Limit
EP080: Benzene
EP080: Naphthalene
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5 of 7 EB1517053 PRENSA 53217 G0038
Method Blank (MB) and Laboratory Control Spike (LCS) Report The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Sample (LCS) refers to a certified reference material, or a known interference free matrix spiked with target analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS. Method Blank (MB) Report
Sub-Matrix: WATER Method: Compound
CAS Number
LOR
Unit
Result
Laboratory Control Spike (LCS) Report Spike
Spike Recovery (%)
Concentration
LCS
Recovery Limits (%) Low
High
EG020F: Dissolved Metals by ICP-MS (QCLot: 84972) EG020A-F: Arsenic
7440-38-2
0.001
mg/L
<0.001
0.1 mg/L
100
88
116
EG020A-F: Cadmium
7440-43-9
0.0001
mg/L
<0.0001
0.1 mg/L
102
88
108
EG020A-F: Chromium
7440-47-3
0.001
mg/L
<0.001
0.1 mg/L
101
87
113
EG020A-F: Copper
7440-50-8
0.001
mg/L
<0.001
0.2 mg/L
101
88
114 110
EG020A-F: Lead
7439-92-1
0.001
mg/L
<0.001
0.1 mg/L
102
89
EG020A-F: Nickel
7440-02-0
0.001
mg/L
<0.001
0.1 mg/L
103
89
113
EG020A-F: Zinc
7440-66-6
0.005
mg/L
<0.005
0.2 mg/L
104
87
113
7439-97-6
0.0001
mg/L
<0.0001
0.01 mg/L
95.8
84
118
EG035F: Dissolved Mercury by FIMS (QCLot: 84973) EG035F: Mercury
EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 85195) 83-32-9
1
µg/L
<1.0
10 µg/L
100
50
104
EP075(SIM): Acenaphthylene
208-96-8
1
µg/L
<1.0
10 µg/L
108
46
109
EP075(SIM): Anthracene
120-12-7
1
µg/L
<1.0
10 µg/L
101
48
113
EP075(SIM): Benz(a)anthracene
56-55-3
1
µg/L
<1.0
10 µg/L
79.4
48
125
EP075(SIM): Benzo(a)pyrene
50-32-8
0.5
µg/L
<0.5
10 µg/L
97.2
49
125
1
µg/L
<1.0
10 µg/L
75.0
43
130
EP075(SIM): Benzo(g.h.i)perylene
205-99-2 205-82-3 191-24-2
1
µg/L
<1.0
10 µg/L
80.4
39
136
EP075(SIM): Benzo(k)fluoranthene
207-08-9
1
µg/L
<1.0
10 µg/L
93.5
46
130
EP075(SIM): Chrysene
218-01-9
1
µg/L
<1.0
10 µg/L
112
45
119
53-70-3
1
µg/L
<1.0
10 µg/L
70.7
42
140
206-44-0
1
µg/L
<1.0
10 µg/L
116
48
120
86-73-7
1
µg/L
<1.0
10 µg/L
89.1
50
114
193-39-5
1
µg/L
<1.0
10 µg/L
75.5
40
132
91-20-3
1
µg/L
<1.0
10 µg/L
97.0
47
101
EP075(SIM): Acenaphthene
EP075(SIM): Benzo(b+j)fluoranthene
EP075(SIM): Dibenz(a.h)anthracene EP075(SIM): Fluoranthene EP075(SIM): Fluorene EP075(SIM): Indeno(1.2.3.cd)pyrene EP075(SIM): Naphthalene EP075(SIM): Phenanthrene EP075(SIM): Pyrene
85-01-8
1
µg/L
<1.0
10 µg/L
101
49
114
129-00-0
1
µg/L
<1.0
10 µg/L
110
48
119
EP080/071: Total Petroleum Hydrocarbons (QCLot: 85196) EP071: C10 - C14 Fraction
----
50
µg/L
<50
1211 µg/L
98.1
38
114
EP071: C15 - C28 Fraction
----
100
µg/L
<100
2103 µg/L
95.8
50
132
EP071: C29 - C36 Fraction
----
50
µg/L
<50
----
----
----
----
----
20
µg/L
<20
260 µg/L
107
75
127
EP080/071: Total Petroleum Hydrocarbons (QCLot: 86227) EP080: C6 - C9 Fraction
EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 85196)
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6 of 7 EB1517053 PRENSA 53217 G0038 Laboratory Control Spike (LCS) Report
Method Blank (MB) Report
Sub-Matrix: WATER CAS Number
Method: Compound
LOR
Unit
Result
Spike
Spike Recovery (%)
Concentration
LCS
Low
Recovery Limits (%) High
EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 85196) - continued EP071: >C10 - C16 Fraction
>C10_C16
100
µg/L
<100
1696 µg/L
98.4
43
119
EP071: >C16 - C34 Fraction
----
100
µg/L
<100
1496 µg/L
96.1
49
134
EP071: >C34 - C40 Fraction
----
100
µg/L
<100
----
----
----
----
EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 86227) EP080: C6 - C10 Fraction
C6_C10
20
µg/L
<20
310 µg/L
109
75
127
EP080: BTEXN (QCLot: 86227) 71-43-2
1
µg/L
<1
10 µg/L
84.1
70
124
EP080: Ethylbenzene
100-41-4
2
µg/L
<2
10 µg/L
84.4
70
120
EP080: meta- & para-Xylene
2
µg/L
<2
10 µg/L
82.2
69
121
EP080: Naphthalene
108-38-3 106-42-3 91-20-3
5
µg/L
<5
10 µg/L
96.3
70
124
EP080: ortho-Xylene
95-47-6
2
µg/L
<2
10 µg/L
81.2
72
122
108-88-3
2
µg/L
<2
10 µg/L
88.7
65
129
EP080: Benzene
EP080: Toluene
Matrix Spike (MS) Report The quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference. Matrix Spike (MS) Report
Sub-Matrix: WATER Laboratory sample ID
Client sample ID
Method: Compound
CAS Number
Spike
SpikeRecovery(%)
Concentration
MS
Low
Recovery Limits (%) High
EG020F: Dissolved Metals by ICP-MS (QCLot: 84972) EB1516919-001
Anonymous
EG020A-F: Arsenic
7440-38-2
0.1 mg/L
97.9
70
130
EG020A-F: Cadmium
7440-43-9
0.1 mg/L
103
70
130
EG020A-F: Chromium
7440-47-3
0.1 mg/L
90.8
70
130
EG020A-F: Copper
7440-50-8
0.2 mg/L
96.8
70
130
EG020A-F: Lead
7439-92-1
0.1 mg/L
93.9
70
130
EG020A-F: Nickel
7440-02-0
0.1 mg/L
99.2
70
130
EG020A-F: Zinc
7440-66-6
0.2 mg/L
106
70
130
EG035F: Mercury
7439-97-6
0.01 mg/L
88.1
70
130
EP080: C6 - C9 Fraction
----
325 µg/L
125
70
130
EP080: C6 - C10 Fraction
C6_C10
375 µg/L
121
70
130
EP080: Benzene
71-43-2
25 µg/L
77.6
70
130
EG035F: Dissolved Mercury by FIMS (QCLot: 84973) EB1517043-001
Anonymous
EP080/071: Total Petroleum Hydrocarbons (QCLot: 86227) EB1517042-001
Anonymous
EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 86227) EB1517042-001
Anonymous
EP080: BTEXN (QCLot: 86227) EB1517042-001
Anonymous
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7 of 7 EB1517053 PRENSA 53217 G0038 Matrix Spike (MS) Report
Sub-Matrix: WATER Laboratory sample ID
Client sample ID
Spike
SpikeRecovery(%)
Concentration
MS
100-41-4
25 µg/L 25 µg/L
EP080: Naphthalene
108-38-3 106-42-3 91-20-3
EP080: ortho-Xylene
95-47-6
EP080: Toluene
108-88-3
25 µg/L
Method: Compound
CAS Number
EP080: Ethylbenzene EP080: meta- & para-Xylene
Recovery Limits (%) Low
High
91.0
70
130
89.2
70
130
25 µg/L
98.4
70
130
25 µg/L
90.0
70
130
90.5
70
130
EP080: BTEXN (QCLot: 86227) - continued EB1517042-001
Anonymous
CERTIFICATE OF ANALYSIS Page
: 1 of 4
: PRENSA
Laboratory
: Environmental Division Brisbane
Contact
: JOHN SCOTT
Contact
: Customer Services EB
Address
: LEVEL 2 16 DOUGLAS STREET
Address
: 2 Byth Street Stafford QLD Australia 4053
: ALSEnviro.Brisbane@alsglobal.com
Telephone
: +61-7-3243 7222
Facsimile
: +61-7-3243 7218
QC Level
: NEPM 2013 Schedule B(3) and ALS QCS3 requirement
Date Samples Received
: 20-Apr-2015 14:40
Work Order
:
Client
EB1517053
MILTON QLD, AUSTRALIA 4064 john.scott@prensa.com.au +61 03 9508 0100 +61 03 9509 6125 53217 G0038 ----
:
Telephone
:
Facsimile
:
Project
:
Order number
:
C-O-C number
: ----
Date Analysis Commenced
: 21-Apr-2015
Sampler
: JOHN SCOTT
Issue Date
: 27-Apr-2015 17:36
Site
: ----
Quote number
: ----
No. of samples received
:1
No. of samples analysed
:1
This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This Certificate of Analysis contains the following information: l General Comments l Analytical Results NATA Accredited Laboratory 825 Accredited for compliance with ISO/IEC 17025.
Signatories This document has been electronically signed by the authorized signatories indicated below. Electronic signing has been carried out in compliance with procedures specified in 21 CFR Part 11. Signatories
Position
Accreditation Category
Edwandy Fadjar Kim McCabe Matt Frost
Organic Coordinator Senior Inorganic Chemist Senior Organic Chemist
Sydney Organics Brisbane Inorganics Brisbane Organics
RIGHT SOLUTIONS | RIGHT PARTNER
Page Work Order Client Project
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2 of 4 EB1517053
PRENSA 53217 G0038
General Comments The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house developed procedures are employed in the absence of documented standards or by client request. Where moisture determination has been performed, results are reported on a dry weight basis. Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference. When sampling time information is not provided by the client, sampling dates are shown without a time component. In these instances, the time component has been assumed by the laboratory for processing purposes. Key :
l
CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society. LOR = Limit of reporting ^ = This result is computed from individual analyte detections at or above the level of reporting ø = ALS is not NATA accredited for these tests.
Benzo(a)pyrene Toxicity Equivalent Quotient (TEQ) is the sum total of the concentration of the eight carcinogenic PAHs multiplied by their Toxicity Equivalence Factor (TEF) relative to Benzo(a)pyrene. TEF values are provided in brackets as follows: Benz(a)anthracene (0.1), Chrysene (0.01), Benzo(b+j) & Benzo(k)fluoranthene (0.1), Benzo(a)pyrene (1.0), Indeno(1.2.3.cd)pyrene (0.1), Dibenz(a.h)anthracene (1.0), Benzo(g.h.i)perylene (0.01). Less than LOR results for 'TEQ Zero' are treated as zero.
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3 of 4 EB1517053
PRENSA 53217 G0038
Analytical Results Client sample ID
Sub-Matrix: WATER (Matrix: WATER)
Client sampling date / time Compound
CAS Number
LOR
Unit
53217_QC10_160415
----
----
----
----
16-Apr-2015 16:00
----
----
----
----
EB1517053-001
--------
--------
--------
--------
Result
Result
Result
Result
Result
EG020F: Dissolved Metals by ICP-MS Arsenic
7440-38-2
0.001
mg/L
<0.001
----
----
----
----
Cadmium
7440-43-9
0.0001
mg/L
<0.0001
----
----
----
----
Chromium
7440-47-3
0.001
mg/L
<0.001
----
----
----
----
Copper
7440-50-8
0.001
mg/L
0.007
----
----
----
-------
Lead
7439-92-1
0.001
mg/L
<0.001
----
----
----
Nickel
7440-02-0
0.001
mg/L
0.005
----
----
----
----
Zinc
7440-66-6
0.005
mg/L
0.066
----
----
----
----
7439-97-6
0.0001
mg/L
<0.0001
----
----
----
----
EG035F: Dissolved Mercury by FIMS Mercury
EP075(SIM)B: Polynuclear Aromatic Hydrocarbons 91-20-3
1
µg/L
<1.0
----
----
----
----
208-96-8
1
µg/L
<1.0
----
----
----
----
Acenaphthene
83-32-9
1
µg/L
<1.0
----
----
----
----
Fluorene
86-73-7
1
µg/L
<1.0
----
----
----
----
Phenanthrene
85-01-8
1
µg/L
<1.0
----
----
----
----
120-12-7
1
µg/L
<1.0
----
----
----
----
Fluoranthene
206-44-0
1
µg/L
<1.0
----
----
----
----
Pyrene
129-00-0
1
µg/L
<1.0
----
----
----
----
56-55-3
1
µg/L
<1.0
----
----
----
-------
Naphthalene Acenaphthylene
Anthracene
Benz(a)anthracene
218-01-9
1
µg/L
<1.0
----
----
----
205-99-2 205-82-3
1
µg/L
<1.0
----
----
----
----
207-08-9
1
µg/L
<1.0
----
----
----
-------
Chrysene Benzo(b+j)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Indeno(1.2.3.cd)pyrene Dibenz(a.h)anthracene
50-32-8
0.5
µg/L
<0.5
----
----
----
193-39-5
1
µg/L
<1.0
----
----
----
----
53-70-3
1
µg/L
<1.0
----
----
----
----
1
µg/L
<1.0
----
----
----
----
^ Sum of polycyclic aromatic hydrocarbons
----
0.5
µg/L
<0.5
----
----
----
----
^ Benzo(a)pyrene TEQ (zero)
----
0.5
µg/L
<0.5
----
----
----
----
C6 - C9 Fraction
----
20
µg/L
<20
----
----
----
----
C10 - C14 Fraction
----
50
µg/L
<50
----
----
----
----
C15 - C28 Fraction
----
100
µg/L
<100
----
----
----
----
C29 - C36 Fraction
----
50
µg/L
<50
----
----
----
----
----
50
µg/L
<50
----
----
----
----
Benzo(g.h.i)perylene
191-24-2
EP080/071: Total Petroleum Hydrocarbons
^ C10 - C36 Fraction (sum)
EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions
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4 of 4 EB1517053
PRENSA 53217 G0038
Analytical Results Client sample ID
Sub-Matrix: WATER (Matrix: WATER)
Client sampling date / time Compound
CAS Number
LOR
Unit
53217_QC10_160415
----
----
----
----
16-Apr-2015 16:00
----
----
----
----
EB1517053-001
--------
--------
--------
--------
Result
Result
Result
Result
Result
EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions - Continued C6_C10
20
µg/L
<20
----
----
----
----
C6_C10-BTEX
20
µg/L
<20
----
----
----
-------
C6 - C10 Fraction
^ C6 - C10 Fraction minus BTEX (F1) >C10 - C16 Fraction
>C10_C16
100
µg/L
<100
----
----
----
>C16 - C34 Fraction
----
100
µg/L
<100
----
----
----
----
>C34 - C40 Fraction
----
100
µg/L
<100
----
----
----
----
^ >C10 - C40 Fraction (sum)
----
100
µg/L
<100
----
----
----
----
^ >C10 - C16 Fraction minus Naphthalene (F2)
----
100
µg/L
<100
----
----
----
----
EP080: BTEXN Benzene
71-43-2
1
µg/L
<1
----
----
----
----
Toluene
108-88-3
2
µg/L
<2
----
----
----
----
Ethylbenzene
100-41-4
2
µg/L
<2
----
----
----
----
108-38-3 106-42-3
2
µg/L
<2
----
----
----
----
95-47-6
2
µg/L
<2
----
----
----
----
^ Total Xylenes
1330-20-7
2
µg/L
<2
----
----
----
----
^ Sum of BTEX
----
1
µg/L
<1
----
----
----
----
91-20-3
5
µg/L
<5
----
----
----
----
13127-88-3
1
%
15.6
----
----
----
----
93951-73-6
1
%
51.6
----
----
----
----
118-79-6
1
%
65.6
----
----
----
----
2-Fluorobiphenyl
321-60-8
1
%
112
----
----
----
----
Anthracene-d10
1719-06-8
1
%
75.8
----
----
----
----
4-Terphenyl-d14
1718-51-0
1
%
116
----
----
----
----
17060-07-0
2
%
96.5
----
----
----
----
2037-26-5
2
%
106
----
----
----
----
460-00-4
2
%
90.2
----
----
----
----
meta- & para-Xylene ortho-Xylene
Naphthalene
EP075(SIM)S: Phenolic Compound Surrogates Phenol-d6 2-Chlorophenol-D4 2.4.6-Tribromophenol
EP075(SIM)T: PAH Surrogates
EP080S: TPH(V)/BTEX Surrogates 1.2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
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>ĂƵƌĂ KΖ,ĞĂ 'ŽǀĞƌŶŵĞŶƚ WƌŽƉĞƌƚLJ E^t >ĞǀĞů ϭ͕ ϰͲϲ ůŝŐŚ ^ƚƌĞĞƚ ^LJĚŶĞLJ E^t ϮϬϬϬ
ĞĂƌ >ĂƵƌĂ͕
ƐďĞƐƚŽƐ ƵůŬ ^ĂŵƉůĞ ŶĂůLJƐŝƐ ZĞƉŽƌƚ ϯϭ sŝĐƚŽƌŝĂ ^ƚƌĞĞƚ͕ 'ƌĂĨƚŽŶ E^t WůĞĂƐĞ ĨŝŶĚ ĂƚƚĂĐŚĞĚ ƚŚĞ ĂƐďĞƐƚŽƐ ďƵůŬ ƐĂŵƉůĞ ĂŶĂůLJƐŝƐ ƌĞƐƵůƚƐ ŽĨ ƚŚĞ ϮϮ ƐĂŵƉůĞƐ ĐŽůůĞĐƚĞĚ ďLJ :ŽŚŶ ^ĐŽƚƚ ŽĨ WƌĞŶƐĂ WƚLJ >ƚĚ ĨŽƌ ϯϭ sŝĐƚŽƌŝĂ ^ƚƌĞĞƚ͕ 'ƌĂĨƚŽŶ E^t ŽŶ ϵ Ɖƌŝů ϮϬϭϱ ĂŶĚ ƌĞĐĞŝǀĞĚ Ăƚ ƚŚĞ WƌĞŶƐĂ WƚLJ >ƚĚ ůĂďŽƌĂƚŽƌLJ ;'&͕ ϮϲϭͲϮϳϭ tĂƚƚůĞƚƌĞĞ ZŽĂĚ͕ DĂůǀĞƌŶ͕ s/ ͕ ϯϭϰϰͿ ŽŶ ϭϯ Ɖƌŝů ϮϬϭϱ͘ dŚĞ ƐĂŵƉůĞƐ ǁĞƌĞ ĂŶĂůLJƐĞĚ ŽŶ Ϯϵ Ɖƌŝů ϮϬϭϱ ĂŶĚ ƚŚĞ ƌĞƐƵůƚƐ ĂƌĞ ƉƌĞƐĞŶƚĞĚ ŽŶ ƚŚĞ ĨŽůůŽǁŝŶŐ ƉĂŐĞ;ƐͿ͘ WƌĞŶƐĂ ƋƵĂůŝƚĂƚŝǀĞůLJ ĂŶĂůLJƐĞƐ ďƵůŬ ƐĂŵƉůĞƐ ĨŽƌ ĂƐďĞƐƚŽƐ ƵƐŝŶŐ ƉŽůĂƌŝƐŝŶŐ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ĂŶĚ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ ƚĞĐŚŶŝƋƵĞƐ ŝŶ ĂĐĐŽƌĚĂŶĐĞ ǁŝƚŚ WƌĞŶƐĂ͛Ɛ EĂƚŝŽŶĂů ƐƐŽĐŝĂƚŝŽŶ ŽĨ dĞƐƚŝŶŐ ƵƚŚŽƌŝƚŝĞƐ ;E d Ϳ͕ ƵƐƚƌĂůŝĂ ĂƉƉƌŽǀĞĚ WZ> ϮϬϬϮ ƐďĞƐƚŽƐ /ĚĞŶƚŝĨŝĐĂƚŝŽŶ dĞƐƚ DĞƚŚŽĚ͕ ĂŶĚ ŝŶ ĂĐĐŽƌĚĂŶĐĞ ǁŝƚŚ ƵƐƚƌĂůŝĂŶ ^ƚĂŶĚĂƌĚ ; ^Ϳ ϰϵϲϰ ʹ ϮϬϬϰ͕ DĞƚŚŽĚ ĨŽƌ ƚŚĞ ƋƵĂůŝƚĂƚŝǀĞ ŝĚĞŶƚŝĨŝĐĂƚŝŽŶ ŽĨ ĂƐďĞƐƚŽƐ ŝŶ ďƵůŬ ƐĂŵƉůĞƐ ĂŶĚ ^ /^Kͬ/ ϭϳϬϮϱ ʹ ϮϬϬϱ͕ 'ĞŶĞƌĂů ƌĞƋƵŝƌĞŵĞŶƚƐ ĨŽƌ ƚŚĞ ĐŽŵƉĞƚĞŶĐĞ ŽĨ ƚĞƐƚŝŶŐ ĂŶĚ ĐĂůŝďƌĂƚŝŽŶ ůĂďŽƌĂƚŽƌŝĞƐ ͘
/Ĩ LJŽƵ ƌĞƋƵŝƌĞ ĨƵƌƚŚĞƌ ŝŶĨŽƌŵĂƚŝŽŶ ƉůĞĂƐĞ ĐŽŶƚĂĐƚ ƚŚĞ WƌĞŶƐĂ ŽĨĨŝĐĞ ŽŶ ;ϬϯͿ ϵϱϬϴ ϬϭϬϬ͘ ZĞŐĂƌĚƐ͕
ZĂǀŝ ,ĞŶĚĞƌƐŽŶ WƌĞŶƐĂ ^ŝŐŶĂƚŽƌLJ
ĐĐƌĞĚŝƚĞĚ ĨŽƌ ĐŽŵƉůŝĂŶĐĞ ǁŝƚŚ /^Kͬ/ ϭϳϬϮϱ͘ ŽƌƉŽƌĂƚĞ ^ŝƚĞ EƵŵďĞƌ ϭϵϭϮϭ͘ dŚŝƐ ĚŽĐƵŵĞŶƚ ƐŚĂůů ŶŽƚ ďĞ ƌĞƉƌŽĚƵĐĞĚ ĞdžĐĞƉƚ ŝŶ ĨƵůů͘ ^ĂŵƉůŝŶŐ ŝƐ ŶŽƚ ĐŽǀĞƌĞĚ ďLJ ƚŚĞ ƐĐŽƉĞ ŽĨ ƚŚĞ E d ĂĐĐƌĞĚŝƚĂƚŝŽŶ͘
ƐďĞƐƚŽƐ ƵůŬ ^ĂŵƉůĞ ŶĂůLJƐŝƐ ZĞƉŽƌƚ ϯϭ sŝĐƚŽƌŝĂ ^ƚƌĞĞƚ͕ 'ƌĂĨƚŽŶ E^t ^ĂŵƉůĞ >ŽĐĂƚŝŽŶ ͬ ĞƐĐƌŝƉƚŝŽŶ ͬ ^ŝnjĞ
^ĂŵƉůĞ EŽ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϭͺϬ͘ϭϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϬϭ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϴϮ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϴϮ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϯ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϭͺϭ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϬϮ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϰϳ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϰϳ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϮ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϮͺϬ͘ϭͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϬϯ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϯϭϱ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϯϵ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϳϲ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϮ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϮͺϬ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϬϰ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϮϬϮ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϭϭ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϵϭ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϰϵ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϯͺϬ͘ϭͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϬϱ
ƌŽǁŶ ŐƌĂǀĞůůLJ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϬϳ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϱϳ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϱϬ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϯͺϬ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϬϲ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϰϱ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϴ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϮϳ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϰϱ ŐƌĂŵƐ
WĂŐĞ Ϯ ŽĨ ϱ
ZĞƐƵůƚ EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
'ϬϬϯϴ͗ Ɖƌŝů ϮϬϭϱ
ƐďĞƐƚŽƐ ƵůŬ ^ĂŵƉůĞ ŶĂůLJƐŝƐ ZĞƉŽƌƚ ϯϭ sŝĐƚŽƌŝĂ ^ƚƌĞĞƚ͕ 'ƌĂĨƚŽŶ E^t ^ĂŵƉůĞ >ŽĐĂƚŝŽŶ ͬ ĞƐĐƌŝƉƚŝŽŶ ͬ ^ŝnjĞ
^ĂŵƉůĞ EŽ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϰͺϬ͘ϭͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϬϳ
ƌŽǁŶ ŐƌĂǀĞůůLJ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϳϲ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϳ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϱϵ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϬ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϰͺϭ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϬϴ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϳϭ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϳϭ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϭ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϱͺϬ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϬϵ
KƌĂŶŐĞͲďƌŽǁŶ ŐƌĂǀĞůůLJ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů
ZĞƐƵůƚ EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
dŽƚĂů ƐĂŵƉůĞ Ε ϭϴϵ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϬϴ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϴϭ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϰϳ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϱͺϭ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϭϬ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϬϭ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϬϭ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϰϵ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϲͺϬ͘ϭͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
Ϭϭϭ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϲϬ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϴϲ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϳϰ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϰϵ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϲͺϬ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϭϮ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϱϭ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϱϭ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϬ ŐƌĂŵƐ
WĂŐĞ ϯ ŽĨ ϱ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
'ϬϬϯϴ͗ Ɖƌŝů ϮϬϭϱ
ƐďĞƐƚŽƐ ƵůŬ ^ĂŵƉůĞ ŶĂůLJƐŝƐ ZĞƉŽƌƚ ϯϭ sŝĐƚŽƌŝĂ ^ƚƌĞĞƚ͕ 'ƌĂĨƚŽŶ E^t ^ĂŵƉůĞ >ŽĐĂƚŝŽŶ ͬ ĞƐĐƌŝƉƚŝŽŶ ͬ ^ŝnjĞ
^ĂŵƉůĞ EŽ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϳͺϬ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
Ϭϭϯ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϴϬ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϭ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϲϵ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϰϴ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϳͺϭ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
Ϭϭϰ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϲϱ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϲϱ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϮ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϴͺϬ͘ϭͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
Ϭϭϱ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϰϳ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϰϳ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϭ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϴͺϬ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
Ϭϭϲ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϴϴ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϴϴ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϬ ŐƌĂŵƐ 'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϵͺϬ͘ϱͿ
ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
Ϭϭϳ
ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
Ϭϭϴ
ZĞƐƵůƚ EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
ŚƌLJƐŽƚŝůĞ ;ǁŚŝƚĞ ĂƐďĞƐƚŽƐͿ ĚĞƚĞĐƚĞĚ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů ǁŝƚŚ Ϯ ĨƌĂŐŵĞŶƚƐ ŽĨ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ ǁŚŝƚĞ ĨŝďƌŽƵƐ ďŽĂƌĚ ŵĂƚĞƌŝĂů ĨŽƵŶĚ ŝŶ ŐƌĞĂƚĞƌ ƚŚĂŶ Ϯŵŵ ĨƌĂĐƚŝŽŶ ;ϭϱ dž ϭϬ dž Ϯ ŵŵͿ ; ŚƌLJƐŽƚŝůĞ ĂƐďĞƐƚŽƐͿ dŽƚĂů ƐĂŵƉůĞ Ε ϭϳϴ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϱϰ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϮϰ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϭ ŐƌĂŵƐ EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ 'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϵͺϭ͘ϬͿ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ dŽƚĂů ƐĂŵƉůĞ Ε ϭϳϲ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϳϲ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϬ ŐƌĂŵƐ
WĂŐĞ ϰ ŽĨ ϱ
'ϬϬϯϴ͗ Ɖƌŝů ϮϬϭϱ
ƐďĞƐƚŽƐ ƵůŬ ^ĂŵƉůĞ ŶĂůLJƐŝƐ ZĞƉŽƌƚ ϯϭ sŝĐƚŽƌŝĂ ^ƚƌĞĞƚ͕ 'ƌĂĨƚŽŶ E^t ^ĂŵƉůĞ >ŽĐĂƚŝŽŶ ͬ ĞƐĐƌŝƉƚŝŽŶ ͬ ^ŝnjĞ
^ĂŵƉůĞ EŽ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϭϬͺϭ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
Ϭϭϵ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϳϱ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϰϭ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϯϰ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϭϬͺϯ͘ϬͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϮϬ
ƌŽǁŶ ŐƌĂǀĞůůLJ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϭϵ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϴϮ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϯϳ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϭϭͺϬ͘ϱͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϮϭ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϱϮ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϯϱ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϳ ŐƌĂŵƐ
'ƌŝĚĚĞĚ >ŽĐĂƚŝŽŶ ;ϱϯϮϭϳͺ ,ϭϭͺϭ͘ϬͿ ϱϯϮϭϳ
Ͳ ϬϬϰ Ͳ
ϬϮϮ
ƌŽǁŶ ŶŽŶͲŚŽŵŽŐĞŶŽƵƐ ƐŽŝů dŽƚĂů ƐĂŵƉůĞ Ε ϭϵϭ ŐƌĂŵƐ хϮŵŵ ĨƌĂĐƚŝŽŶ Ε Ϯϯ ŐƌĂŵƐ фϮŵŵ ĨƌĂĐƚŝŽŶ Ε ϭϲϴ ŐƌĂŵƐ фϮŵŵ ƐƵďͲƐĂŵƉůĞ Ε ϱϮ ŐƌĂŵƐ
ZĞƐƵůƚ EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
EŽ ĂƐďĞƐƚŽƐ ĨŽƵŶĚ͕ Ăƚ ƚŚĞ ƌĞƉŽƌƚŝŶŐ ůŝŵŝƚ ŽĨ Ϭ͘ϭ ŐͬŬŐ͕ ďLJ ƉŽůĂƌŝnjĞĚ ůŝŐŚƚ ŵŝĐƌŽƐĐŽƉLJ ŝŶĐůƵĚŝŶŐ ĚŝƐƉĞƌƐŝŽŶ ƐƚĂŝŶŝŶŐ KƌŐĂŶŝĐ ĨŝďƌĞƐ ĚĞƚĞĐƚĞĚ
KŶůLJ ƚŚĞ ƐĂŵƉůĞƐ ƐƵďŵŝƚƚĞĚ ĨŽƌ ĂŶĂůLJƐŝƐ ŚĂǀĞ ďĞĞŶ ĐŽŶƐŝĚĞƌĞĚ ŝŶ ƉƌĞƐĞŶƚŝŶŐ ƚŚĞƐĞ ƌĞƐƵůƚƐ͘
WĂŐĞ ϱ ŽĨ ϱ
'ϬϬϯϴ͗ Ɖƌŝů ϮϬϭϱ