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São Carlos, 05 de Outubro de 2016. Quarta – feira Time Sweep (Oscilatório) Test type: Time sweep Test settings Duration: 0:30:00 Delay time: 0:00:10 Temperature (°C): 100 Equilibration time: -Controlled Variable % strain: 2,500 Frequency Single Angular frequency (rad/s): 0,05000

Strain Sweep (Pré – test) (Oscilatório) Test type: Strain sweep Test settings Sweep: % Strain From: 0,125 to 12,500 Mode: Log Points per decade: 8 Temperature (°C): 100 Equilibration time: 0:01:00 Angular frequency (rad/s): 6,283

Frequency Sweep (Test) (Oscilatório) Test type: Frequency sweep


Test settings Angular frequency (rad/s): 0,01000 to 100 Mode: Log Points per decade: 8 Temperature (°C): 100 Equilibration time: 0:01:00 Controlled Variable % strain: 1,0000

Steady state flow (Permanente) Test type: Steady state flow Test settings Ramp: Shear rate (1/s) From: 0,01000 to 500,0 Mode: Log Points per decade: 8 Temperature (°C): 100 Sample period: 0:00:10 Steady state Percentage tolerance: 5 Consecutive within tolerance: 3 Maximum point time: 0:01:00

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