Suncliff CBG Report

Page 1

Report: COA Evaluation Summary

OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com

Product Description Evaluation Summary

Client: GVB Oregon

Product Name:

CBG-Isolate B#7073

GVB - I - CBG

For OLCC/OHA Compliance Purposes.

Moisture Analysis

Cannabinoid Potency Analysis

THC

Abrv.

Process Date: 2021-08-09 THCA

Test Not Required < LOQ < LOQ

Retest Date: 2023-08-10 Δ-9-THC

Matrix: Hemp Concentrate Δ-8-THC

Metrc Source ID: n/a THCV

Dry Wt. %Dry Wt. mg/g

< LOQ < LOQ < LOQ < LOQ

< LOQ 0.69 % < LOQ < LOQ

Metrc Package ID: n/a . CBDA

< LOQ 6.9 mg/g

License Number: n/a CBD

Date Collected: 2021-08-10 CBGA

Date Received: 2021-08-10 CBG

Report Date: 2021-08-13 CBDVA

Report ID: A4340-04 CBDV CBN CBL CBC

Tests Requested: Cannabinoid Potency Analysis Pesticide Analysis Residual Solvent Analysis

Pesticide Analysis

Pesticide Status Pass

< LOQ

< LOQ < LOQ

99.03 %990.3 mg/g < LOQ < LOQ < LOQ < LOQ < LOQ

< LOQ < LOQ < LOQ

< LOQ 0.69 %6.9 mg/g < LOQ < LOQ

No Pesticides Were Detected above Oregon's action limit as stated in OAR 333-007-0400.

moisture compensated & adjusted for the loss of carboxylic acid group - OAR 333-064-0100

Report ID: A4340-04 |

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Page 1 of 11 | Rev 21.3 07/20/2021
*
IT2
Dup
Total
* Total CBD *

Report: Case Narrative

OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com

This certificate of analysis is prepared for… GVB Oregon

2490 Ewald Ave SE Salem, OR 97302

For OLCC/OHA Compliance Purposes.

This report presents the analytical findings for the sample collected on 2021-08-10 by Tony Melton using sampling plan A4340 and received by PREE Laboratory on 2021-08-10. The sample was assigned a laboratory ID of A4340-04. The results in this report only apply to sample A4340-04.

This report shall not be reproduced, except in full, without written consent of PREE Laboratory. Report alterations by any other entity beside PREE Laboratory are not allowed. If alterations are made to the original report after the initial release, they will be noted on the case narrative below.

The testing methods used are of sufficient sensitivity to meet the compliance criteria set in OAR 333-007. However, it is the responsibility of the client to utilize the data to comply with standards set in OAR 333-007.

All analyses were performed in accordance with PREE Laboratory’s NELAP/TNI approved quality control system and all quality control data was within the laboratory’s predefined acceptance criteria unless otherwise noted in the case narrative of this report. General comments are also recorded below.

Notes:

The Oregon Department of Agriculture requires hemp products to not contain more than 0.35% total THC, per OAR 603048. Residual solvent analysis was subcontracted. The report from the subcontracting laboratory is attached. No special conditions were noted during the processing and testing of the sample.

Sardar, Tamzid M. | Laboratory Director Corvallis, Oregon

If you have any questions regarding the information in this report, please feel free to call 541-257-5002 or email PREE at services@preelab.com.

A4340-04

Report ID:
| Page 2 of 11 | Rev 21.3 07/20/2021

Report: Evaluation Detail

OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com

Moisture Analysis

Cannabinoid Potency Analysis

Product Name:

IT2 CBG-Iso B#7073 Dup

Analysis Date: 2021-08-12

Testing Batch ID: V1641,1640,1639,1638,1637,1636,1635

Testing Method: LSOP #303 Cannabinoid Quantification

Evaluation Detail

Moisture Analysis

Note:

For OLCC/OHA Compliance Purposes.

Cannabinoid Potency Analysis |Compound Abrv.

Total THC * < LOQ < LOQ Total CBD * 0.69 % 6.9 mg/g

Evaluation Detail < LOQ

Test Not Requested/Required| 0.69 % < LOQ 99.03 % < LOQ < LOQ < LOQ < LOQ

Dry Wt. (%)

Tetrahydro-cannabinolic acidTHCA < LOQ 0.5 % Delta9 Tetrahydro-cannabinolΔ-9-THC < LOQ 0.5 % Delta8 Tetrahydro-cannabinolΔ-8-THC < LOQ 0.5 %

< LOQ < LOQ < LOQ

TetrahydrocannabivarinTHCV < LOQ 0.5 % Cannabidiolic acid CBDA < LOQ 0.5 % Cannabidiol CBD 6.90.5 % Cannabigerolic acidCBGA < LOQ 0.5 % Cannabigerol CBG 990.30.5 % Cannabidivarinic acidCBDVA < LOQ 0.5 % Cannabidivarin CBDV < LOQ 0.5 % Cannabinol CBN < LOQ 0.5 % Cannabicyclol CBL < LOQ 0.5 % Cannabichromene CBC < LOQ 0.5 %

Dry Wt. (mg/g) RL (%) < LOQ < LOQ

* moisture compensated & adjusted for the loss of carboxylic acid group - OAR 333-064-0100

Report ID: A4340-04 | Page 3 of 11 | Rev 21.3 07/20/2021

Accreditation for Δ-8-THC, THCV, CBGA,CBG, CBDVA, CBDV, CBL, CBC, CBN is not offered by ORELAP and therefore are not accredited tests.

Report: Evaluation Detail

OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com

Pesticide Analysis Evaluation Detail

Product Name:

Pesticide Name|

For OLCC/OHA Compliance Purposes.

Tested Value (ppm) Pass Criteria (ppm)

LOQ (ppm) Status Pass/Unsatisfactory

Abamectin < LOQ 0.50 Pass

Acephate < LOQ 0.40 Pass

Acequinocyl < LOQ 2.00 Pass

Acetamiprid < LOQ 0.20 Pass Aldicarb < LOQ 0.40 Pass

Azoxystrobin < LOQ 0.20 Pass Bifenazate < LOQ 0.20 Pass

Bifenthrin < LOQ 0.20 Pass

Boscalid < LOQ 0.40 Pass

Carbaryl < LOQ 0.20 Pass Carbofuran < LOQ 0.20 Pass

Chlorantraniliprole < LOQ 0.20 Pass

Chlorfenapyr < LOQ 1.00 Pass

Chlorpyrifos < LOQ 0.20 Pass Clofentezine < LOQ 0.20 Pass

Cyfluthrin < LOQ 1.00 Pass

Cypermethrin < LOQ 1.00 Pass

Daminozide < LOQ 1.00 Pass Diazinon < LOQ 0.20 Pass

Dichlorvos < LOQ 1.00 Pass

Dimethoate < LOQ 0.20 Pass

Ethoprophos < LOQ 0.20 Pass Etofenprox < LOQ 0.40 Pass

Etoxazole < LOQ 0.20 Pass Fenoxycarb < LOQ 0.20 Pass

Fenpyroximate < LOQ 0.40 Pass

Fipronil < LOQ 0.40 Pass

Flonicamid < LOQ 1.00 Pass Fludioxonil < LOQ 0.40 Pass

Hexythiazox < LOQ 1.00

Imazalil < LOQ 0.20

Analysis Date: 2021-08-11 0.20 0.04 0.20 0.04 0.04 0.04 0.04 0.20 0.04 0.04 0.04 0.04 1.00 0.04 0.20 1.00 1.00 0.20 0.04 0.20 0.04 0.04 0.20 0.04 0.04 0.20 0.04 0.04 0.20 0.04 0.04 0.04 0.20

Imidacloprid < LOQ 0.40 Kresoxim-methyl < LOQ 0.40

Pass

Pass Pass Pass

Continued on next page…

Report ID: A4340-04 | Page 4 of 11 | Rev 21.3 07/20/2021

IT2 CBG-Iso B#7073 Dup
LSOP #307 Pesticides by LCMS/MSTesting Method: Testing Batch ID: V1635,1634,1633,1630

Report:

OLCC License No.

545 SW 2nd Street.

Pesticide Analysis

Detail

|

| services@preelab.com | Preelab.com

Evaluation Detail

Pesticide Name|

Pass Criteria (ppm) LOQ (ppm) Status Pass/Unsatisfactory Malathion < LOQ 0.20 Pass

Tested Value (ppm)

Metalaxyl < LOQ 0.20 Pass Methiocarb < LOQ 0.20 Pass

Methomyl < LOQ 0.40 Pass

Methyl-Parathion < LOQ 0.20 Pass

MGK-264 < LOQ 0.20 Pass

Myclobutanil < LOQ 0.20 Pass

Naled < LOQ 0.50 Pass

Oxamyl < LOQ 1.00 Pass

Paclobutrazol < LOQ 0.40 Pass

Permethrins < LOQ 0.20 Pass

Phosmet < LOQ 0.20 Pass

Prallethrin < LOQ 0.20 Pass

0.20 Pass

Pyrethrins < LOQ 1.00 Pass

Piperonyl butoxide < LOQ 2.00 Pass < LOQ 0.20

Propoxur < LOQ 0.20 Spirotetramat

Pyridaben < LOQ 0.20 Spinosad < LOQ 0.20

< LOQ

< LOQ

Pass Pass

For OLCC/OHA Compliance Purposes. 0.04 0.04 0.04 0.04 0.20 0.20 0.20 0.04 0.04 0.04 0.20 0.04 0.04 0.20 0.20 0.04 1.00 0.04 bo 0.20 0.20 0.04 0.04 0.04 0.04 0.04 0.04

Pass Pass Spiroxamine

0.40 Pass

Tebuconazole < LOQ 0.40 Pass

Thiacloprid < LOQ Trifloxystrobin

Propiconazole < LOQ 0.40 Pass < LOQ 0.20

Spiromesifen 0.20 Pass Thiamethoxam < LOQ 0.20 Pass Pass

Report ID: A4340-04 |

Evaluation
10087092BDA | ORELAP ID. 4147
Corvallis OR. 97333
541.257.5002
Page 5 of 11 | Rev 21.3 07/20/2021

OLCC

Moisture Analysis

Cannabinoid Potency Analysis

Analysis Date:

Testing Batch ID:

Preelab.com

Quality Control Detail

For OLCC/OHA Compliance Purposes.

Quality Control Detail

Cannabinoid Potency Analysis |MBLCS

Tetrahydro-cannabinolic acid

Delta9 Tetrahydro-cannabinol Cannabidiolic acid

Cannabidiol

Tetrahydro-cannabinolic acid

Delta9 Tetrahydro-cannabinol

Cannabidiolic acid

Cannabidiol

Moisture Analysis| 100.0% 110.7%

Pass Criteria Tested Value (%) Expected Value (%) < 0.1% < 0.1% < 0.1% < 0.1%

115.2% 111.3% 111.7%

< 0.1% 80-120%

< 0.1% < 0.1% < 0.1% < 0.1% < 0.1% < 0.1% < 0.1% 100.0% 80-120%

100.0% 80-120% 100.0% 80-120%

Report ID: A4340-04 | Page 6 of 11 |

21.3 07/20/2021

Report: Quality Check
License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com |
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Rev
V1641,1640,1639,1638,1637,1636,1635
2021-08-12

Check

License No.

2nd

Pesticide Analysis

Analysis Date: 2021-08-11

For OLCC/OHA Compliance Purposes.

Quality Control Detail

Pesticide Name |

1 Abamectin

Acephate

Acequinocyl

Acetamiprid

Aldicarb

Azoxystrobin

Bifenazate

Bifenthrin

Boscalid

Carbaryl

Carbofuran

Chlorantraniliprole

1 Chlorfenapyr

0 Chlorpyrifos

0 Clofentezine

Cyfluthrin

Cypermethrin

Daminozide

Diazinon

Dichlorvos

Dimethoate

Ethoprophos

Etofenprox

Etoxazole

Fenoxycarb

Fenpyroximate

Fipronil

Flonicamid

Fludioxonil

Hexythiazox

Imazalil

Imidacloprid

Kresoxim-methyl

Expected Value (ppm) Tested Value (ppm) Pass Criteria (ppm) < 0.02< 0.02< 0.02

< 0.02< 0.02< 0.02

< 0.02< 0.02< 0.02

< 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02 < 0.5< 0.5 < 0.5

< 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1

< 0.02< 0.02< 0.02 < 0.02 < 0.1

< 0.5< 0.5 < 0.5 < 0.5< 0.5 < 0.5

< 0.02 < 0.1

< 0.02 < 0.02 < 0.1 < 0.02 < 0.02 < 0.1 < 0.02 < 0.1 < 0.02

< 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1 < 0.02 < 0.1 < 0.02 < 0.02 < 0.1 < 0.02 < 0.02 < 0.1 < 0.02< 0.02 < 0.02 < 0.1 < 0.02 < 0.02 < 0.02

< 0.02 < 0.02 < 0.1 < 0.02 < 0.02 < 0.1 < 0.02 < 0.02 < 0.1 < 0.02 < 0.02 < 0.02

< 0.02 < 0.02 < 0.1 < 0.1< 0.1

Continued on next page… Report ID: A4340-04 | Page 7 of 11 | Rev 21.3 07/20/2021

Report: Quality
OLCC
10087092BDA | ORELAP ID. 4147 545 SW
Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
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MB
Testing Batch ID: V1635,1634,1633,1630

For OLCC/OHA Compliance Purposes.

Pesticide Analysis

Quality Control Detail

Pesticide Name

Malathion

Metalaxyl

Methiocarb

Methomyl

Methyl-Parathion

MGK-264 I

MGK-264 II

Myclobutanil

Naled

Oxamyl

Paclobutrazol

Permethrin - trans

Permethrin - cis

Phosmet

Piperonyl butoxide

Prallethrin

Propiconazole

Propoxur

Pyrethrin - Cinerin

Pyrethrin - Jasmolin

Pyrethrin - Pyrethrins

Pyridaben

Spinosyn A

Spinosyn D

Spiromesifen

Spirotetramat

Spiroxamine

Tebuconazole

Thiacloprid

Thiamethoxam

Trifloxystrobin

Expected Value (ppm) < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02

Tested Value (ppm) Pass Criteria (ppm) < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1 < 0.1< 0.1 < 0.1

< 0.1< 0.1 < 0.1 < 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1

< 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1

< 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.5< 0.5 < 0.5 < 0.5< 0.5 < 0.5

< 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1 < 0.1< 0.1 < 0.1

< 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02

< 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02

< 0.5< 0.5 < 0.5 < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02

Continued on next page…

Report ID: A4340-04 | Page 8 of 11 | Rev 21.3 07/20/2021

Report: Quality Check OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
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|MB

For OLCC/OHA Compliance Purposes.

Pesticide Analysis

Quality Control Detail

Abamectin

Acephate

Acequinocyl

Acetamiprid

Aldicarb

Azoxystrobin

Bifenazate

Bifenthrin

Boscalid

Carbaryl

Carbofuran

Chlorantraniliprole

Chlorfenapyr

Chlorpyrifos

Clofentezine

Cyfluthrin

Cypermethrin

Daminozide

Diazinon

Dichlorvos

Dimethoate

Ethoprophos

Etofenprox

Etoxazole

Fenoxycarb

Fenpyroximate

Fipronil

Flonicamid

Fludioxonil

Hexythiazox

Imazalil

Imidacloprid

Kresoxim-methyl

100.0079.18 100.00135.19

Pesticide Name | 100.0099.57

60 - 140

100.00

138.59 100.00100.54

100.00110.23

60 - 140

100.00101.5860 - 140

Pass Criteria (%) 60 - 140

60 - 140 60 - 140 60 - 140

60 - 140

60 - 140 100.00115.1260 - 140

100.00101.9960 - 140

100.0090.3160 - 140

100.00125.63

100.0087.61 128.16 60 - 140 100.00123.3160 - 140

LCS Expected Recovery (%) Actual Recovery (%) 100.00 60 - 140 100.0094.8960 - 140

100.00113.55

100.0099.5660 - 140 100.00126.9460 - 140 60 - 140 100.00106.2960 - 140

100.00110.92

100.00104.67

100.0090.9360 - 140 100.00103.6160 - 140 60 - 140 100.0097.6960 - 140 60 - 140 100.0094.0260 - 140

100.00124.45

100.00106.9360 - 140 100.00100.7660 - 140

100.0091.9260 - 140 100.00110.8660 - 140 100.0094.1560 - 140 100.00105.6960 - 140 100.00127.2260 - 140

Continued on next page…

Report ID: A4340-04 | Page 9 of 11 | Rev 21.3 07/20/2021

Report: Quality Check OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
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For OLCC/OHA Compliance Purposes.

Pesticide Analysis

Quality Control Detail

Pesticide Name |

Malathion

Metalaxyl

Methiocarb

Methomyl

Methyl-Parathion

MGK-264 I

MGK-264 II

Myclobutanil

Naled

Oxamyl

Paclobutrazol

Permethrin - trans

Permethrin - cis

Phosmet

Piperonyl butoxide

Prallethrin

Propiconazole

Propoxur

Pyrethrin - Cinerin

Pyrethrin - Jasmolin

Pyrethrin - Pyrethrins

Pyridaben

Spinosyn A

Spinosyn D

Spiromesifen

Spirotetramat

Spiroxamine

Tebuconazole

Thiacloprid

Thiamethoxam

Trifloxystrobin

Actual Recovery (%) Pass Criteria (%) 100.00107.4860 - 140 100.00106.89

60 - 140 100.00119.1960 - 140

100.00129.0760 - 140 100.0089.3060 - 140 100.0080.6160 - 140 100.00113.7260 - 140

LCS Expected Recovery (%) 100.0096.8860 - 140

100.00100.9260 - 140 100.00124.5860 - 140 100.0090.8160 - 140

100.00132.9560 - 140 100.00117.1660 - 140 100.00115.0560 - 140

100.00122.8260 - 140

100.00110.3560 - 140 100.0088.2860 - 140 100.00113.4760 - 140

100.0097.1660 - 140 100.00121.8560 - 140 100.0077.5160 - 140

100.0097.9060 - 140 100.0088.3660 - 140 100.0094.8360 - 140 100.00102.0660 - 140 100.00104.2060 - 140

100.00108.5360 - 140 100.0095.2060 - 140 100.0087.4760 - 140

100.00109.6160 - 140

100.00105.7261 - 140

Report ID: A4340-04 | Page 10 of 11 | Rev 21.3 07/20/2021

Report: Quality Check OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
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OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com

Definitions

For OLCC/OHA Compliance Purposes.

Limit of Quantitation (LOQ) : The minimum level, concentration, or quantity of a target analyte that can be reported with a specific degree of confidence.

Method Blank (MB) : A quality control sample that is free of the analyte being measured.

Laboratory Control Sample (LCS) : A quality control sample with a known amount of the analyte used to demonstrate accuracy.

Field Duplicate : A second sample collected in the field using the same sampling method as the primary sample.

Action Limit : Analyte levels set by the state of Oregon (OAR 333-007) indicating that follow-up action is necessary.

ppm : parts per million, equivalent to 1 μg/g and 1 μg/L or 0.001 mg/g and 0.001 mg/L COA : Certificate of Analysis.

Report Flag (B) : Blank contamination - The analyte was detected above one-half the reporting limit in an associated blank.

Report Flag (E) : Compound tested above the upper limit of quantitation.

Report Flag (Q) : One or more quality control criteria (for example, LCS recovery, surrogate spike recovery) failed.

Calculations

Cannabinoid Potency : Wet WT% = (Exported concentration ppm) x (Dilution) x (Extraction Vol./Wet wt mg) x 100

Total THC% = (%THCA) x 0.877 + (%THC)

Total CBD% = (%CBDA) x 0.877 + (%CBD)

Total THC (Dry WT)% = % total THC(wet) / [1-(% moisture/100)]

Total CBD (Dry WT)% = % total CBD(wet) / [1-(% moisture/100)]

Percentage Recovery : % Rec. = [(Amount measured) / (Known amount)] * 100

Disclaimers

Disposal : All marijuana and hemp products received by PREE will be disposed of following the OLCC’s rules for Marijuana Waste Management, regardless of product type, unless PREE is given specific disposal instructions for a product based on test results from state regulatory agencies.

ID: A4340-04 |

Report: Definition
Report
Page 11 of 11 | Rev 21.3 07/20/2021

Residual Solvents

Analyte LOQAction LevelResult Units

Butanes 250 5000 ppm3 < LOQ

n-Butane 250 5000 ppm< LOQ

iso-Butane 250 5000 ppm< LOQ

Hexanes 174 290 ppm4 < LOQ

n-Hexane 174 290 ppm< LOQ

2-Methylpentane 174 290 ppm< LOQ

3-Methylpentane 174 290 ppm< LOQ

2,2-Dimethylbutane 174 290 ppm< LOQ 2,3-Dimethylbutane 174 290 ppm< LOQ

Pentanes 1400 5000 ppm5 < LOQ

n-Pentane 1400 5000 ppm< LOQ iso-Pentane 1400 5000 ppm< LOQ

Neopentane 250 5000 ppm< LOQ

Xylenes 1302 2170 ppm< LOQ

1,2-Dimethylbenzene 1302 2170 ppm< LOQ

1,3-Dimethylbenzene 1302 2170 ppm< LOQ

1,4-Dimethylbenzene 1302 2170 ppm< LOQ

Xylenes MP 1302 2170 ppm< LOQ

Ethyl benzene 1302 NA ppm< LOQ

2-Propanol (IPA) 1400 5000 ppm< LOQ

Acetone 1400 5000 ppm< LOQ

Acetonitrile 246 410 ppm< LOQ

Benzene 1.2 2 ppm< LOQ

Methanol 1000 3000 ppm< LOQ

Propane 250 5000 ppm< LOQ

Toluene 534 890 ppm< LOQ

Dichloromethane 360 600 ppm< LOQ

1,4-Dioxane 228 380 ppm< LOQ

2-Butanol 1400 5000 ppm< LOQ

2-Ethoxyethanol 96 160 ppm< LOQ

Cumene 42 70 ppm< LOQ

Cyclohexane 2278 3880 ppm< LOQ

Ethyl acetate 1400 5000 ppm< LOQ

Ethyl ether 1400 5000 ppm< LOQ

Ethylene glycol 558 620 ppm< LOQ

Ethylene oxide 30 50 ppm< LOQ

Heptane 1400 5000 ppm< LOQ

Isopropyl acetate 1400 5000 ppm< LOQ

Tetrahydrofuran 432 720 ppm< LOQ

Ethanol 1400 NA ppm7 < LOQ

5-hepten-2-one,6-methyl- NA NATIC 5-heptenal,2,6-dimethyl- NA NATIC Water NA NATIC

Certificate

Date Sampled: 08/12/21 09:00

Date Accepted: 08/12/21

Batch ID: Batch Size:

Sampling Method/SOP: SOP.T.20.010

Date/Time Extracted: 08/12/21 12:26

Date/Time Analyzed: 08/13/21 10:15 Analysis Method/SOP: SOP.T.40.031

3 - Total butanes are calculated as sum of n-butanes (CAS# 106-97-8) and iso-butane (CAS# 75-28-5)

4 - Total hexanes are calculated as sum of n-hexane (CAS# 110-54-3), 2-methylpentane (CAS# 107-83-5), 3-methylpentane (CAS# 96-14-0), 2,2-dimethylbutane (CAS# 75-83-2), 2,3-dimethylbutane (CAS# 79-29-8)

5 - Total pentanes are calculated as sum of n-pentane (CAS# 109-66-0), iso-pentane (CAS# 78-78-4), and neo-pentane (CAS# 463-82-1)

6 - Total xylenes are calculated as 1,2-dimethylbenzene (CAS# 95-47-6), 1,3-dimethylbenzene (CAS# 106-42-3), and 1-4-dimethylbenzene (CAS# 106-42-3)

7 - Ethanol is not regulated under OAR-333-007-0410.

TIC - Tentatively Identified Compound not regulated under OAR-333-007-0410

Results above the action level

will be highlighted RED LOQ=Limit of Quantitation; PPM=Parts per million;

PASS/FAIL status based on OAR 333-007.

Kawai Medeiros Manager
of Analysis EVIO Labs Portland 14775 SW 74th Ave, Tigard, OR 97224 503-954-2562 / OLCC 010-10046111391 / www.EVIOLabs.com A4340-04
Matrix: Extract/Concentrate
Sample ID: P210730-06 PREE Labs METRC Batch #:
010-10087092BDA
fail Oregon state testing requirements and
ND=Not detected; NT=Not tested; AC=Above calibration range.
This report shall not be reproduced, unless in its entirety, without written approval from EVIO Labs, Inc. Test results are confidential unless explicitly waived otherwise. All QC samples meet acceptance criteria of the method; data available upon request. The results relate only to the material or product analyzed for the sample included on this report. Page 1 of 3
Laboratory
- 8/13/2021

Quality Control

Analyte Recovery LimitsLOQResult

Butanes < LOQ250 (ppm) < LOQ n-Butane < LOQ250 (ppm) < LOQ iso-Butane < LOQ250 (ppm) < LOQ Hexanes < LOQ174 (ppm) < LOQ n-Hexane < LOQ174 (ppm) < LOQ 2-Methylpentane < LOQ174 (ppm) < LOQ 3-Methylpentane < LOQ174 (ppm) < LOQ 2,2-Dimethylbutane < LOQ174 (ppm) < LOQ 2,3-Dimethylbutane < LOQ174 (ppm) < LOQ Pentanes < LOQ1400 (ppm) < LOQ n-Pentane < LOQ1400 (ppm) < LOQ iso-Pentane < LOQ1400 (ppm) < LOQ Neopentane < LOQ250 (ppm) < LOQ Xylenes < LOQ1302 (ppm) < LOQ

1,2-Dimethylbenzene< LOQ1302 (ppm) < LOQ 1,3-Dimethylbenzene< LOQ1302 (ppm) < LOQ 1,4-Dimethylbenzene< LOQ1302 (ppm) < LOQ Xylenes MP < LOQ1302 (ppm) < LOQ

Ethyl benzene < LOQ1302 (ppm) < LOQ 2-Propanol (IPA) < LOQ1400 (ppm) < LOQ

Acetone < LOQ1400 (ppm) < LOQ Acetonitrile < LOQ246 (ppm) < LOQ

Benzene < LOQ1.2 (ppm) < LOQ Methanol < LOQ1000 (ppm) < LOQ

Propane < LOQ250 (ppm) < LOQ Toluene < LOQ534 (ppm) < LOQ

Dichloromethane < LOQ360 (ppm) < LOQ 1,4-Dioxane < LOQ228 (ppm) < LOQ

2-Butanol < LOQ1400 (ppm) < LOQ 2-Ethoxyethanol < LOQ96 (ppm) < LOQ

Cumene < LOQ42 (ppm) < LOQ Cyclohexane < LOQ2278 (ppm) < LOQ

Ethyl acetate < LOQ1400 (ppm) < LOQ Ethyl ether < LOQ1400 (ppm) < LOQ

Ethylene glycol < LOQ558 (ppm) < LOQ Ethylene oxide < LOQ30 (ppm) < LOQ

Heptane < LOQ1400 (ppm) < LOQ Isopropyl acetate < LOQ1400 (ppm) < LOQ

Tetrahydrofuran < LOQ432 (ppm) < LOQ Ethanol < LOQ1400 (ppm) < LOQ

Extracted: 08/12/21 12:26

LCS(P21H035-BS1)

% Recovery LOQAnalyte Recovery Limits

Analyzed: 08/13/21 10:15

Analyte Recovery LimitsLOQ% Recovery

Butanes 63.5 (ppm) 0-200 n-Butane 73.4 (ppm) 50-150 iso-Butane 53.5 (ppm) 50-150 Hexanes 83.1 (ppm) 0-200 n-Hexane 85.3 (ppm) 70-130 2-Methylpentane 83.2 (ppm) 70-130

3-Methylpentane 84.1 (ppm) 70-130 2,2-Dimethylbutane 89.2 (ppm) 70-130 2,3-Dimethylbutane 78.1 (ppm) 70-130 Pentanes 105 (ppm) 0-200 n-Pentane 87.3 (ppm) 70-130 iso-Pentane 78.5 (ppm) 70-130 Neopentane 96.1 (ppm) 50-150 Xylenes 85.4 (ppm) 0-200

1,2-Dimethylbenzene 84.0 (ppm) 70-130 1,3-Dimethylbenzene 87.0 (ppm) 70-130 1,4-Dimethylbenzene 87.2 (ppm) 70-130 Xylenes MP 85.0 (ppm) 0-200

Ethyl benzene 85.5 (ppm) 70-130 2-Propanol (IPA) 93.8 (ppm) 70-130

Acetone 86.3 (ppm) 70-130 Acetonitrile 84.3 (ppm) 70-130

Benzene 85.2 (ppm) 70-130 Methanol 100 (ppm) 70-130

Propane 42.5 (ppm) 50-150 Toluene 88.3 (ppm) 70-130

Dichloromethane 100 (ppm) 70-130 1,4-Dioxane 92.4 (ppm) 70-130

Kawai Medeiros Laboratory Manager - 8/13/2021
Certificate of Analysis EVIO Labs Portland 14775 SW 74th Ave, Tigard, OR 97224 503-954-2562 / OLCC 010-10046111391 / www.EVIOLabs.com
Batch: P21H035 - SOP.T.40.031 Solvents Blank(P21H035-BLK1) Result LOQAnalyte Recovery Limits Analyzed: 08/13/21 10:15Extracted: 08/12/21 12:26
This report shall not be reproduced, unless in its entirety, without written approval from EVIO Labs, Inc. Test results are confidential unless explicitly waived otherwise. All QC samples meet acceptance criteria of the method; data available upon request. The results relate only to the material or product analyzed for the sample included on this report. Page 2 of 3

Certificate of Analysis

Quality Control

Batch: P21H035 - SOP.T.40.031 Solvents (Continued)

Analyzed: 08/13/21 10:15Extracted: 08/12/21 12:26

Analyte Recovery Limits

% Recovery LOQ

Analyte Recovery LimitsLOQ% Recovery

2-Butanol 93.7 (ppm) 70-130 2-Ethoxyethanol 94.2 (ppm) 70-130

Cumene 97.6 (ppm) 50-150 Cyclohexane 88.3 (ppm) 70-130

Ethyl acetate 85.9 (ppm) 70-130 Ethyl ether 91.5 (ppm) 70-130

Ethylene glycol 83.6 (ppm) 70-130 Ethylene oxide 78.7 (ppm) 50-150

Heptane 86.0 (ppm) 70-130 Isopropyl acetate 90.1 (ppm) 70-130

Tetrahydrofuran 90.2 (ppm) 70-130

Kawai Medeiros

Manager -

EVIO Labs Portland 14775 SW 74th Ave, Tigard, OR 97224 503-954-2562 / OLCC 010-10046111391 / www.EVIOLabs.com
LCS(P21H035-BS1)
This report shall not be reproduced, unless in its entirety, without written approval from EVIO Labs, Inc. Test results are confidential unless explicitly waived otherwise. All QC samples meet acceptance criteria of the method; data available upon request. The results relate only to the material or product analyzed for the sample included on this report. Page 3 of 3
Laboratory
8/13/2021

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