c LC-MS/MS. 224:T507,RESULTS Table 1 shows the mycotoxins analysed along with their corresponding Limits of Quantification (LOQ). Mycotoxin family Aflatoxins Zearalenone + Metabolite A-Trichothecenes B-Trichothecenes Fumonisins + Metabolite Ochratoxin Emerging mycotoxins Penicillium toxins Ergot alkaloids Alternaria toxin Mycotoxin Abbreviation LOQ (μg/kg) Aflatoxin B1 AFB1 < 0,4 Aflatoxin B2 AFB2 < 0,4 Aflatoxin G1 AFG1 < 0,4 Aflatoxin G2 AFG2 < 0,4 α – Zearalenol α -ZEL < 10 β – Zearalenol β -ZEL < 10 Zearalanone ZAN < 10 Zearalenone ZEN <5 Diacetoxyscirpenol DAS <3 HT-2 toxin HT-2 < 9,6 < 9,6 T-2 toxin T-2 Neosolaniol NEO < 10 3-Acetyl Deoxynivalenol 3-ADON < 20 15-Acetyl Deoxynivalenol 15-ADON < 20 Deoxynivalenol DON < 20 Nivalenol NIV < 20 Deoxynivalenol-3-Glucoside D3G < 30 Fumonisin B1 FB1 < 25 Fumonisin B2 FB2 < 25 Fumonisin B3 FB3 < 25 Fusaric Acid FA <3 Moniliformin MON <3 Fusarenon X FX < 40 Ochratoxin A OTA < 1,6 Beauvericin BEA <1 Enniatin A ENN A <1 Enniatin A1 ENN A1 <1 Enniatin B ENNI B <1 Enniatin B1 ENN B1 <1 Citrinin CIT < 50 Patulin PAT < 100 Ergosine ES <1 Ergocryptinine ECR <1 Alternariol AOH < 20 Table 1. Mycotoxins analysed and their LOQs. 525:T50b,Table 2 shows the recovery (%) of mycotoxins screened in corn, wheat, and barley. RECOVERY (%) Analyte CORN WHEAT BARLEY 90 1. Moniliformin 82 91 2. Nivalenol 85 89 88 3. Deoxynivalenol 103 108 105 4. Fusaric Acid 102 96 109 5. 3-Acetil Deoxynivalenol 80 88 90 6. 15-Acetil Deoxynivalenol 83 92 91 99 7. Aflatoxin G2 99 99 8. Aflatoxin G1 98 98 92 9. Aflatoxin B2 93 96 96 10. Aflatoxin B1 96 93 104 11. Diacetoxyscirpenol 96 101 103 12. HT-2 toxin 92 93 99 13. Fumonisin B1 103 96 94 14. β – Zearalenol 101 96 89 15. α – Zearalenol 87 104 99 16. T-2 toxin 98 103 90 17. Zearalanone 103 103 95 18. Ochratoxin A 94 97 98 19. Zearalen