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Solution Manual for A Small Scale Approach to Organic Laboratory Techniques, 3rd Edition

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TABLE OF CONTENTS Preface Equipping the Organic Chemistry Laboratory Waste Management Guidelines Laboratory Equipment and Supplies Organic Laboratory Techniques Practical Exams Organic lab practical exam advice for instructors Organic lab practical exam instructions for students Organic lab practical exam instructions and report sheet for crystallization Organic lab practical exam instructions and report sheet for extraction

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Chemicals and Supplies for Each Experiment Answers to Questions Experiment 1 Experiment 2 Experiment 3 Experiment 4 Experiment 5 Experiment 6 Experiment 7 Experiment 8 Experiment 9 Experiment 10 Experiment 11 Experiment 12 Experiment 13 Experiment 14 Experiment 15 Experiment 16 Experiment 17 Experiment 18 Experiment 19 Experiment 20 Experiment 21 Experiment 22 Experiment 23 Experiment 24 Experiment 25 Experiment 26 Experiment 27 Experiment 28 Experiment 29 Experiment 30 Experiment 31

Solubility Crystallization Extraction A Separation and Purification Scheme Chromatography Simple and Fractional Distillation Infrared Spectroscopy and Boiling-Point Determination Acetylsalicylic acid Acetaminophen TLC of Analgesic Drugs Isolation of Caffeine Isopentyl Acetate (Banana Oil) Isolation of Eugenol from Cloves Spearmint and Caraway Oil: (+)- and (-)-Carvones Isolation of Chlorophyll and Carotenoid Pigments from Spinach Ethanol from Sucrose An Introduction to Molecular Modeling Computation Chemistry Reactivity of Some Alkyl Halides Nucleophilic Substitution Reactions: Competing Nucleophiles Synthesis of n-Butyl Bromide and t-Pentyl Chloride 4-Methylcyclohexene Methyl Stearate from Methyl Oleate Gas Chromatographic Analysis of Gasolines Biodiesel Ethanol from Corn Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination Nitration of Aromatic Compounds Using a Recyclable Catalyst Reduction of Ketones Using Carrot Extract Resolution of α-Phenylethylamine and Determination of Optical Purity An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol © 2011 Brooks/Cole, Cengage Learning

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