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NA-LUBE速 EP 5000 Series


NA-LUBE速 EP 5000 Series

NA-LUBE EP 5000 Series consists of low odor, light colored sulfurized fatty acid esters, triglycerides and a-olefins. The 5000 Series is produced from hydrogen sulfide and elemental sulfur, offering improved oxidative stability and better solubility in paraffinic base oils. 5000 Series Product Key

5 5000 Series

0

0 0

Sulfurized Backbone Total Sulfur Content 1 - Olefin % Total Sulfur 2 - Fatty Acid Esters 3 - Fatty Acid Esters /Triglyceride 4 - Olefin / Triglyceride

Example: NA-LUBE EP-5210 5 - 5000 series 2 - Sulfurized Fatty Acid Ester

10 - 10% total sulfur NA-LUBE ADTC

NA-LUBE EP 5000 Series

EP 5100 Sulfurized Olefin

% Total Sulfur - 30 % Total Nitrogen - 6.5

EP 5400

EP 5200

EP 5300

Sulfurized Fatty Acid Esters

Sulfurized Fatty Acid Esters / Triglycerides

Sulfurized Olefin / Triglycerides / Fatty Acid Esters

EP-5131

EP-5210

EP-5310

EP-5415

% Total Sulfur - 30 % Active Sulfur - 19

% Total Sulfur - 10 % Active Sulfur - <1.5

% Total Sulfur - 10 % Active Sulfur - <1.0

% Total Sulfur - 15 % Active Sulfur - 4

EP-5216

EP-5316

% Total Sulfur - 16 % Active Sulfur - 5

% Total Sulfur - 16 % Active Sulfur - 5

EP-5218 % Total Sulfur - 18 % Active Sulfur - 6

EP-5420 % Total Sulfur - 20 % Active Sulfur - 10

EP-5425 % Total Sulfur - 26 % Active Sulfur - 19


Extreme Pressure / Antiwear Additives

Product

% Total Sulfur

% Active Sulfur

Viscosity @40ºC (cSt)

NA-LUBE EP-5131

30

17

20

Light colored, low odor sulfurized olefin with excellent extreme pressure properties.

Description

NA-LUBE EP-5210

10

<1.5

25

Unique low odor, very light colored inactive sulfur carrier based on fatty acid ester chemistry. Compatible with copper and its alloys. Enhances the oxidation stability of Group I & II oils when used with yellow metal deactivators and phenolic/aminic antioxidants.

NA-LUBE EP-5216

16

5

45

Light colored, low odor sulfurized fatty acid ester with excellent extreme pressure properties.

NA-LUBE EP-5218

18

6

50

Light colored, low odor sulfurized fatty acid ester with excellent extreme pressure properties.

NA-LUBE EP-5310

10

<1.0

240

Light colored, low odor inactive sulfurized fatty acid ester/fatty oil with excellent extreme pressure properties.

NA-LUBE EP-5316

16

5

265

Light colored, low odor sulfurized fatty acid ester/ fatty oil with excellent extreme pressure properties. Provides excellent boundary lubrication.

290

Light colored, low odor sulfurized olefin/fatty oil with excellent extreme pressure properties and outstanding thermal and hydrolytic stability. Compatible with copper and its alloys. Enhances the oxidation stability of Group I & II oils when used with yellow metal deactivators and phenolic/aminic antioxidants. Compatible with zinc dithiophosphates.

25

Light colored, low odor sulfurized olefin/fatty oil with excellent extreme pressure properties. Highly suitable for heavy duty drilling and cutting operations.

200

Light colored, low odor sulfurized olefin/fatty oil with excellent extreme pressure properties. Highly suitable for heavy duty drilling and cutting operations.

Powder

Bis-dimercaptothiadiazole derivative (yellow powder) with excellent extreme pressure/antiwear and antioxidant properties. Recommended for use in grease where heavy load carrying capability is required.

NA-LUBE EP-5415

NA-LUBE EP-5420

NA-LUBE EP-5425

NA-LUBE EP-5665

15

4

20

10

26

19

65

-

NA-LUBE® EP 5000 Series - Extreme Pressure Additives

King Industries offers a broad range of low color, low odor Extreme Pressure Additives used for metalworking fluids, greases, slideway oils and other industrial lubricants.

Product

% Total Sulfur

% Total Nitrogen

Viscosity @40ºC (cSt)

Description

NA-LUBE ADTC Ashless Dialkydithiocarbamate

30

6.5

370

A unique ashless dithiocarbamate offering extreme pressure, antiwear and antioxidant properties.

2


Applications for the NA-LUBE EP 5000 Series The NA-LUBE EP 5000 Series consists of a variety of novel sulfur-containing additives with total sulfur content ranging from approximately 10% to 65% and the active sulfur content ranging from <1.5% to 18%. Because these unique products provide both extreme pressure and antiwear properties and also perform as friction modifiers, they are used in a wide variety of lubricant applications, including: 

Industrial Gear Oils



Automotive Gear Oils



Automatic Transmission Fluids



Slideway Oils  NA-LUBE EP-5210 and EP-5415 are well suited for formulating slideway oils.



Hydraulic Fluids



Rust and Oxidation Oils



Greases  NA-LUBE EP-5210, NA-LUBE EP-5415 and NA-LUBE EP-5665 are highly recommended for grease applications including non-antimony/lead containing EP greases.



“Neat Oil” Metalworking Fluids  NA-LUBE EP-5131, EP-5210, EP-5216, EP-5218, EP-5310, EP-5316, EP-5415 and EP-5425 are outstanding alternatives to chlorinated paraffins in metalworking fluids, when used in combination with ash-producing or ashless phosphorus-type antiwear and boundary lubrication additives. 

NA-LUBE EP-5131, EP-5216, EP-5218, EP-5310, EP-5316, EP-5415 and EP-5425 are highly suitable for heavy-duty drilling and cutting operations.



Water Miscible Metalworking Fluid Concentrates



Environmentally Friendly Lubricants and Greases

The NA-LUBE EP 5000 sulfur carriers, when combined with NA-LUBE AW, NA-LUBE AO, NA-SUL and K-CORR products, are highly suitable for formulating high quality/high performance industrial and automotive lubricants and greases.

Solubility NA-LUBE EP-5121, EP-5131, EP-5210, EP-5216, and EP-5218 have excellent solubility in hydrotreated mineral oils, synthetic diesters, and fatty oils. NA-LUBE EP-5316 has solubility in napththenic and solvent refined Group I base oils. NA-LUBE EP-5415 extends solubility to Group II base oils as well. NA-LUBE EP-5310’s unique chemistry gives it outstanding solubility characteristics in naphthenic and solvent refined Group I base oils. Due to its novel chemistry, NA-LUBE EP-5310 provides improved lubricity over similar inactive sulfur fatty acid ester type extreme pressure additives.


 Series Performance in a ISO VG 32 Group I Base Oil The following table highlights the performance of the products in various bench tests for lubrication properties. Tests

NA-LUBE EP-5210

NA-LUBE EP-5216

NA-LUBE EP-5218

NA-LUBE EP-5316

NA-LUBE EP-5415

ISO VG 32 (Group I)

Base Oil

5.0

Treat Level, % Four Ball Weld (ASTM D 2783) 10 seconds, 25°C, 1800 rpm OK Load, kgf Weld Load, kgf

160 200

200 240

200 240

200 240

220 240

Four Ball Wear (ASTM D 4172) 1 hour, 75°C, 40 kgf, 1200 rpm Scar Diameter, mm

0.54

0.58

0.81

0.68

0.60

1a 2a

3a 4a

3a 4a

1b 3b

1b 3b

Copper Corrosion (ASTM D 130) 3 hours, 100ºC 24 hours, 100ºC

 NA-LUBE EP-5210 - Concentration Effect On Properties As shown below, with increasing concentrations of NA-LUBE EP-5210, the wear and extreme pressure properties improve with no negative effects on demulsibility or copper corrosion protection.

Tests

2.0% NA-LUBE EP-5210

7.5% NA-LUBE EP-5210

Base Oil

10.0% NA-LUBE EP-5210

10.0% NA-LUBE EP-5210 6.0% NA-LUBE AW-6010

ISO VG 32 (Group I)

Four Ball Weld (ASTM D 2783) 10 seconds, 25°C, 1800 rpm OK Load, kgf Weld Load, kgf

120 160

160 200

160 200

200 240

Four Ball Wear (ASTM D 4172) 1 hour, 75°C, 40 kgf, 1200 rpm Scar Diameter, mm

0.72

0.59

0.60

0.50

Falex PIN & VEE (ASTM D 3233) Lbs.

890

1050

1060

950

Copper Corrosion (ASTM D130) 3 hours, 100ºC 24 hours, 100ºC

1a 3a

1a 2a

1a 2a

1b 2a

39-39-2 10

41-39-0 10

41-39-0 10

40-40-0 10

Demulsibility (ASTM D 1401,DIN 51 599 Oil-Water-Emulsion, ml Time, Minutes

NA-LUBE® EP 5000 Series - Extreme Pressure Additives

Performance for the NA-LUBE EP 5000 Series


 NA-LUBE EP-5415 Metalworking Performance Data NA-LUBE EP-5415 imparts good extreme pressure performance for metalworking fluids and can be used to replace chlorinated paraffins as shown in the chart below. 10% Mid-chain Chlorinated Paraffin (C14-17 >50% Cl)

Tests

10% NA-LUBE EP-5415

ISO VG 32 (Group I)

Base Oil Four Ball Weld (ASTM D 2783) 10 seconds, 25°C, 1800 rpm OK Load, kgf Weld Load, kgf

160 180

320 340

Four Ball Wear (ASTM D 4172) 1 hour, 75°C, 40 kgf, 1200 rpm Scar Diameter (mm)

0.80 0.54

0.75 0.58

1a

1b

Copper Corrosion (ASTM D 130) 3 hours, 100ºC

As shown below, tapping torque tests were conducted to compare the performance of NA-LUBE EP-5415 versus the performance of a commonly used chlorinated paraffin. The tests were conducted using 4340-alloy steel under varying machining speeds.

4340 Alloy Steel Base Oil: Paraffinic ISO VG 32

10% Chlorinated Paraffin Average Peak Torque (inch - pounds)

10% NA-LUBE EP-5415 Average Peak Torque (inch - pounds)

% Efficiency

40 sfm* (407rpm)

68.8

70.79

97.2

48 sfm (488rpm)

69.2

71.32

97.0

58 sfm (586rpm)

71.0

69.88

101.6

69 sfm (703rpm)

71.7

72.05

99.5

83 sfm (844rpm)

69.1

70.95

97.4

*sfm = surface feet per minute

Additionally, NA-LUBE EP-5415 can be used to formulate premium quality machine tool slideway lubricants. Various treat levels of NA-LUBE EP-5415 in combination with 0.5% tackifier in an ISO VG 68 oil meet the requirements of the Cincinnati Lamb P-47 Heavy-Medium Way Oil specification. Tests

1.5% NA-LUBE EP-5415 0.5% Tackifier

5.0% NA-LUBE EP-5415 0.5% Tackifier

Cincinnati Lamb P-47 Specification

ISO VG 68

ISO VG 68

cSt @ 40ºC: 61.6-74.8 SUS @ 100ºF: 317-389

>380

>380

330 Minimum

>380

>380

360 Minimum

0.07

0.10

1.7 Maximum

0.0710 / 0.0982 = 0.72

0.0783 / 0.1009 = 0.78

0.80 Maximum

Steel 1 0.30 0.2

Steel 1 0.35 0.3

Base Oil

Flash Point (ASTM D 92) COC, ºF Fire Point (ASTM D 92) COC ºF Acid Number (ASTM D 974) mg KOH/g Cincinnati Lamb Stick-Slip (μs/μK)* Thermal Stability Test Procedure B: 24 hours, 101ºC CM Color Class Rod Weight of Deposit, mg Rod Metal Loss, mg Acid Number Change, mg KOH/g Precipitate * Ratio of static to kinetic friction

Copper 3 1.0 0.4 0.07 None

Copper 3 1.2 0.4 0.07 None

Maximum Limits Steel Copper 1 5 3.5 -1.0 5.0 5 --


NA-LUBE® ADTC Multifunctional Ashless Dialkyldithiocarbamate

Product

Composition

Sulfur Approx. (%)

Nitrogen Approx. (%)

Viscosity @ 100°C (ASTM D 445) Approx. mm2/s (cSt)

NA-LUBE ADTC

Methylene-bisdibutyldithiocarbamate

30

6.5

15

C 4H 9

S

S

C N

N C

C 4H 9

S

CH 2

S

C 4H 9 C 4H 9

NA-LUBE ADTC PROPERTIES & USES NA-LUBE ADTC exhibits the following properties:     

Excellent extreme pressure and antiwear Excellent oxidation inhibition Outstanding demulsification Good thermal stability Excellent solubility in highly paraffinic base stocks

Due to its multifunctionality, NA-LUBE ADTC is used in:       

Heavy Metal-free Greases Rust and Oxidation Oils Automotive and Industrial Gear Oils Extreme Pressure Turbine Oils Hydraulic Oils Engine Oils Metalworking Fluids

 Performance of NA-LUBE ADTC - Ashless Hydraulic Fluid Package The table below shows the performance capabilities of NA-LUBE ADTC in an ashless hydraulic fluid package containing K-CORR 1031, an amino acid derived rust inhibitor. Tests Treat Level of Additive Package, %

ASHLESS PACKAGE: NA-LUBE ADTC, NA-LUBE AO-130, NA-LUBE AW-6220, K-CORR 1031 0.5 ISO VG 32 (Group I)

Base Oil Demulsibility (ASTM D 1401, DIN 51 599) Oil-Water-Emulsion, ml Separation Time, Minutes

1.0

42-38-0 10

41-38-1 10

Steel Corrosion (ASTM D 665B, DIN 51 585)

Pass

Pass

Copper Corrosion (ASTM D 130, DIN 51 759) 3 hours, 135°C

1a

1a

RPVOT* (ASTM D 2272) Lifetime, Minutes

495

1260

Four Ball Wear (ASTM D 4172) 1 hour, 75°C, 40 kgf, 1200 rpm, Scar Diameter, mm

0.50

0.47

AFNOR Wet Filtration (E 68691) Filterability Index

1.25

1.10

Not Determined

>12

FZG A/8.3/90 (ASTM D 5182, DIN 51 354 Part 2) Damage Load Stage * Rotating Pressure Vessel Oxidation Test

NA-LUBE® EP 5000 Series & NA-LUBE ADTC

NA-LUBE ADTC is a unique, ashless dialkyldithiocarbamate additive that offers excellent extreme pressure, antiwear, and antioxidant properties. NA-LUBE ADTC has well-defined chemistry with sulfur and nitrogen present in the same molecule.


King Industries, Inc - USA Lubricant Additives Division Science Rd. Norwalk, CT 06852 Phone (203) 866-5551 Email: info@kingindustries.com

King Industries - Europe Mr. Marcel Groenewoud Noordake 64 2741 EZ Waddinxveen The Netherlands Phone: +31 182-631360 Email: mg@kingintl.nl

King Industries - Asia www.kingindustries.com Dr. Zhiqiang Alex He 42 Ju Lin Ya Yuan Rich Mond Hill (Juhaoyuan) Bo Ai 7th Road Zhongshan, Guangdong, China 528403 Phone: +86 760-88229866 Email: alex.he@kingindustries.com

The conditions of your use and application of our products, technical assistance and information (whether verbal, written or by way of product evaluations), including any suggested formulations and recommendations, are beyond our control. Therefore, it is imperative that you test our products, technical assistance and information to determine to your own satisfaction whether they are suitable for your intended uses and applications. Such testing has not necessarily been done by King Industries, Inc. ("King"). The facts, recommendations and suggestions herein stated are believed to be reliable; however, no guaranty or warranty of their accuracy is made. EXCEPT AS STATED, THERE ARE NO WARRANTIES, EXPRESS OR IMPLIED, OF MERCHANTABILITY, FITNESS OR OTHERWISE. KING SHALL NOT BE HELD LIABLE FOR SPECIAL, INCIDENTAL, CONSEQUENTIAL OR EXEMPLARY DAMAGES. Any statement inconsistent herewith is not authorized and shall not bind King. Nothing herein shall be construed as a recommendation to use any product(s) in conflict with patents covering any material or its use. No license is implied or granted under the claims of any patent. Sales or use of all products are pursuant to Standard Terms and Conditions stated in King sales documents.


NA-LUBE EP 5000 Series  

NA-LUBE EP 5000 Series Brochure

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