Page 1

t cARul

Memorándum Ng 2645 Para: De: CC: Fecha: Asunto:

COMITÉ CIENTíFICO Secretaría Técnica (Ing. Alejandro Arcelus) Ing. Hernán Orduna; C/N (R) Gastón Silbermann 23/01/2013 Resultados Lab. Pacific Rim - Muestras tomadas en el ingreso del 20/11112 a UPM (Ex BOTNIA).

Señores integrantes del Comité Científico: Tengo el agrado de dirigirme a ese Órgano Subsidiario de C.A.R.U., a efectos de hacerles

llegar

los

resultados

recibidos

del

Laboratorio

Pacific

Rim,

correspondientes a las muestras tomadas el día 20 de noviembre de 2012, en el marco del Plan de Monitoreo de la Planta Orión (UPM-Ex Botnia). Como referencia, se adjuntan copias de las órdenes de compra remitidas por esta Secretaría Técnica.

Secretarlo Técnico

ComISIón Adm'''lstríNora del Río Uruguay

1/1


Work Order Cllent Paeifle Rim Laboratories Ine. #103, 19575-55A Ave Surrey, B.C. V3S8P8

eco no tec h

W.O.# E12275 log # 2065820 Date rec'd Results to email ce Phone Fax

Nov 26/12 Dave Hope dave@paeifierimlabs.eom parveen@paeifierimlabs.eom 604-532-8711 604-532-8712

.>t: description of samples Two effluent (2) samples Sample preservation confirmed by/date HB/Nov 26/12 Total Adsorbable Organic Halogen, AOX units

Sample ID I Descriptlon

'0

M.ethod Method blank

..

_ _ • ._ • . . • _

spike recovery, expected spike recovery, start, actual Recovery, start spike recovery , end, actual Reeovery, end Reeovery Iimits splke Batch dupllcate analysls RPD Rfº-!-Lmits .• _ _ _ loc criteria comments:

_

'

' _

.?9.: Q!:f:1.L -

.'

_ 0 -'

.

.._

I ... ..

.

o

.

• _ . .

ng .ng _ ng ng

* *

ng %

78-114

%

%

g..:l-.. ...__ 1. 91 1 1. 75 8.85

._ ...._ - + - .

119lk..

170 20()0. 10000 9340 93.4

.. ,

mg/ l %

01. _

.;_ _

Falled

AOX: analyzed in aceordance with USEPA method 1650 . 5amples were preserved with HN03 prio r to analysis. * Non-conformance: batch terminated before end spike analyzed . Other batch QC passed and duplicate satifactory ** Elevated detectlon Iimit due to insufficient sample volume


\J

lSox ,.. .' ( Page 1 of7

SAMPLE RECEIPT FORM I CHEMICAL ANALYSIS FORM FILE #: PR122428

CLIENT:

Comision Administradora Rio Uruguay Costsnera Norte S/N Paysandu,60000 Uruguay Phone - (5982) 47225000 ext 106 Email-Arcelus@caru.org.uy

RECEIVED BY: CONDITION:

J. Del Pozo good,4°C

Sample #of Containers '{me 1 Water 1 Water 1 Water Water 1 1 Water 1 Water 1 Water Water 1 1 Water 1 Water 1 Water 1 Water 1 Water STORAGE:

DATEITIME: November 23,2012 (1:00 p.m.)

Sample lClient Cedes) Lab Codes

---

1227876 1227649 »-: 1227647 ¿ / 1227648 ;-' 1227881 ___ 1227880 v ' 1227842 v1227820 »< 1227875 .;>/ 1227890 ¿p' 1227873 ,/ 1227874 ./' 1227872 ¡Y o

PR122428 PR122429 PR122430 PR122431 PR122432 PR122433 PR122434 PR122435 PR122436 PR122437 PR122438 PR122439 PR122440

Test Reguested Nitrate, Nitrite Arnmonia COD TKN

Phenols

pcnDIF OH & Grease Total Petroleum Hydrocarbons Organophosphate biocides Organochlorine biocides AOX Chlorates Sulphide Metals (except Mercury) Mercury Microtox ECSO

Stored at 4'C

. •. !

ANALYTES:

HRGCIHRMS analysis for polych1orinated dibenzo(p)dioxins and dibenzofurans (PCDDIF)

SPECIAL INSTRUCTIONS:

PRI22428-2429, 2431-2440 subcontracted out to Exova and Econotech . See separate reports .

Pacifie Rim Laboratories Ine. # \03, 19575-55A Avenue, Surrey, Be V3S 8P8 Canarla Te\: + 604.532.8111 Fax: + 604.532.8712 Email: info@pacifierimlabs.eom www.pacificrimlabs.eom


Page 20f7

METRODOLOGY Reference Method:

PCDD/F: SOP LABO 1; EPA Method 1613b, Environment Canada RM23

Data summarized in Data Report Attached Report sent to: Comments:

Alejandro Arcelus

Date: December 27,2012

Results relate onIy lo iterns tested.

David Hope, PChem, CEO

Pacilie Rim Laboratories Ine. #103, 19575-55AAvenue, Surrey, BC V3S 8P8 Canada Tel: + 604.532.8711 Fax: + 604.532.8712 Email: info@pacificrimlabs.com www.pacifierimlabs.com


Page 3 of7

DATAREPORT Cllent: Client lD: PRlID:

ComislonAdministradora del Rlo Uruguay

1227647 PR122430

DIOXINS

I

Conaeners

Cone. ! pa/l

2,3,7,8-TCOD Total TCOD

,

I

Dl pa/l

Contact: Date Extracted: Date Analysed:

AlejandroArcelus 4-0ec-12 14-0ec-12

WHO·TEQs

I·TEQs

Surrogate Reeoverles %

(ND=Ol pa/l

(ND=Dll pa/l

(ND=O) pa/L

(ND=Dll pg/l

NO NO

1 1

69

NO

1

NO

1

NO NO

2 2

51

NO

1

NO

2

NO NO NO NO

2 2

91 80

-

NO NO NO

0.2 0.2 0.2

NO NO NO

0.2 0.2 0.2

2

NO NO

3 3

B4

NO

0.03

NO

0.03

4

69

0.02

0.02

0.002

0.002

Total D/oxln TEQ

0.020

2.65

0.0020

3.63

!

1,2,3,7,8-PeCOD TotalPeCOO

, ! I

1,2,3.4,7,B-HxCDO 1,2,3,6,7.B-HxCDO 1,2,3,7,B.9-HxCOD Total HxCOD

i

1,2,3,4,6,7,B·HpCOO Total HpCOO

!

I

,

,

OCOO

2

20

FURANS Conaeners

I

Da/l

Dl Da/l

2,3,7,8-TCDF TotalTCOF

i

NO NO

1 1

¡

1,2,3,7,8-PeCDF 2,3.4,7,8-PeCOF Total PeCOF

I

1,2,3,4 ,7,B-HxCOF 1,2,3,6,7,B-HxCOF 1,2,3,7,B,9-HxCDF 2,3,4,6,7,8-HxCOF Total HxCOF

I '

:

NO NO NO NO

1--

2 1---. 2

+--N O--NO --- - - r - NO

2 2 2

2 2 2

I·TEQs

Surrogate Recoveries

.JND=OL Da/l

% -'-

WHO·TEQs

-iJcifl

61

NO

0.1

58

NO NO

0.1 __ 1

58

_ .

(ND=O) Da/l NO

(ND=Dl) pa/l 0.1

NO NO

0.1

0.2 0.2 0.2

--

1

- '

70 70 70 69

NO NO NO NO

0.2 0.2 0.2 0.2

NO -NO

76 72

NO NO

0.03 0.03

-NO

NO 0.00

0.004 2.0&

NO 0.00

4.71

0.0020

NO NO

I

1.2,3,4,6,7,8-HDCDF 1,2,3,4,7,B,9-HpCOF Total HpCDF

I

i

NO NO NO

OCOF

¡

NO

i

3 3 3 4

-

Total Furan TEQ

Total PCDDIPCDFToxle Equivalent

I

0.020

I

0.03 0.03

NO

0.0004

2.06

I

5.69

NO - none detected

Patriek Pond, ChiefTechnical Offieer Fonn Namo: DOC18 Dala Report DxW OI·Fob-07 DGH

Pacific Rim LaboratoriesInc.IiI03. I9575-55A Avenue, Surrey, Be V3S 8P8 Cenada Tel: + 604.532.87\ I Fax: + 604.532_8712 Email: info@pacificrimlabs_com www.paciñcrimlabs.com


Page4 oC7

QC REPORT • BLANK CI/ent: ClientlD: PRlID:

ComlsionAdministradora del Rlo Uruguay

Blank OF1210268

DIOX'NS

I

Conc. ! paIL ! NO ! NO

Conaeners 2,3,7,8-TCDO TotalTCDO

Dl pall 1 1

Surrogate Recovaríes

Alejandro Arcelus 4-Dec-12 14-0ec-12

Contact: Date Extractad: Date Analysed:

WHO-TEQs

'-TEQs

71

(ND=O) pg/l NO

(ND=Dl) PllIl 1

(ND=O) pgll NO

(ND=Dl) pgll 1

%

!

1,2,3,7,8-PeCDD TotalPeCOO

I

1,2,3,4,7,8-HxCOD 1,2,3,6,7,8-HxCOO 1,2,3,7,8,9-HxCOD Total HxCOO

1

i

NO NO

2 2

71

NO

1

NO

2

NO NO NO NO

2 2 2 2

100 92

-

NO NO NO

0.2 0.2 0.2

NO NO NO

0.2 0.2 0.2

NO NO

3 3

83

NO

0.03

NO

0.03

4 98 Total Dioxin TEQ

NO 0.00

0.004 2.63

NO 0.00

0.0004

I

1,2,3,4,6,7,8-HpCOO Total HpCOO

,

, ;

I

¡ I I

OCDO

i

FURANS

I,

Conaeners 2,3,7,8-TCOF Total TCOF

;

,

NO

Dall NO NO

Dl Dall 1 1

I-TEQs

Surrogate Recovaries

%

f-'

pa/L

52

NO

60

1-_ NO

64

NO

3.63

WHO-TEQs

(ND=Dll pall 0.1

(ND=O) Da/l NO

(ND=Dl) Dall 0.1

NO NO

0.1 1

I 1,2,3 7,8-PeCOF 2,3,4,7,8-PeCDF Total PeCOF 1,2,3,4,7,8-HxCOF 1,2,3,6,7,8-HxCOF 1,2,3,7,8,9-HxCOF 2,3,4,6,7,8-HxCOF Total HxCOF 1,2,3,4,6,7,8-HpCDF 1,2,3,4,7,8,9-HpCDF Total HpCOF OCOF

I

I

NO 2 2 NO NO __f - - _2 __

!

NO

I

0.1 1

--

-72 70 68 67

NO 0.21 NO NO

0.2 0.21 0.2 0.2

NO 0.21 NO

NO 2.8

2 2 2 2 2

0.2 0.21 0.2 f-- 0.2 ._

-ÑO NO NO

3 3 3

80 84

NO NO

0.03 0.03

NO NO

0.03 0.03

0.0043 0.21

0.0043 2.07

0.00043 0.21

0.00043 2.07

0.21

4.71

0.21

5.70

t- NO 2.1 ! -----j-

4.3

.

4 Total Furan TEQ

Total PCDD/PCDF Toxic Equlvalent

NO - none detectad

Patriek Pond, Chief Technical Officer FonnNamc: DOC 18 DalaReportDxW O\-FclHl7 DGH

Pacific RimLaboratories Inc, #103, 19575-55A Avenue,Surrey, Be V3S 8P8 Canalla Tel: + 604.532.8711 Fax: + 604.532.8712Email: inCo@pacificrimlabs.com era 0810 ReportOxW www.pacificrimlabs.corn

01·Feb-07 OGH


Page 50f7

DATAREPORT CARU Riverwater

Client: Project: Client ID: PRL ID: I

DL ng/L

a路HCH! p-HCHi Lindane(y路HCH)

0.05 0.05 0.05 0.05 0.2 0.2 0.2 0.2 0.1 0.1 0.1 0.1 0.5 0.2 0.2 0.2 0.2 0.2 0.2 0.2

Organochlorine Pestlcldes

-

Hentachlor HeptachlorEpoxide] Aldrinl Oxychlordanel y-Chlordane (trans) a-Chlordane (cis) trans-Nonachlor cis-Nonachlor] Chlordane o,p'-DDE pp-DDEI o,p'-DDD w-DDD o,p'-DDT' pp-DDTi Endosulfan Ji Endosulfun TI EndosulfanSulphate] Dieldrin Endrin Methoxychlor _ Mirex

Organophosphate Pestlcldes Parathion

0.2 0.2 0.5 0.5 0.2 1

1227842

Blank

PR122434

OC121010B

Conc nglL

Conc ng/L

NO NO NO NO NO NO NO NO NO NO NO NO . __ ._- -_._._-- -- - - -NO NO NO NO NO NO NO NO .- - - - - - ---- 1--,-__ NO _ r-.- - - - ---- - f-- .

NO

NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO

NO

NO

I

1.67

NO NO 0.68

Pacifie Rim Laboratories Ine. #103, 19575路55A Avenue , Surrey, Be V3S 8P8 Canada Tel: + 604.532.8711 Fax: + 604.532.8712 Email: info@paeificrimlabs.com www.pacificrimlabs.com

I


Page 6 of7

DATAREPORT CARU

Client: Project:

Riverwater Cllent ID: PRLID:

Standard Recoveries (%) 13C6-a-HCH 13 C6-P-HCH 13C6-Lindane (y-HCH) I 3 -o-HCH 4

1227842

Blank

PR122434

OC121010B

1

! •

¡3CIO-Heptachlor 13C6-Aldrin

i

13C¡o-y-Chlordane 13C¡O-cis-Nonachlor 13ClrEndosulpban 1

i I !

IJCl1-Endosulphan n 13 C12_P,p'·DDE BC¡rP,P' -DDD 13CI1_P,P'-DDT

I

13C¡rDieldrin

!

13ClrEndrin

I

IJClrEndosulphan Sulpbate 13 Cw Mirex

,I

i

I

.. .

_--- 1---

I

64 69 55 39 63 59 70 76 47 76 61 69 25 97 85 80 .60

66

"-- '- -

_._-

- - - _._--_ .

- -

ND • none detected

Patrick Pondo Chief Technical Officer

Pacifie Rim Laboratories Ine. #103. 19575·55A Avenue, Surrey, Be V3S 8P8 Canada Tel : + 604.532.8711 Fax: + 604.532.8712 Email : info@pacificrimlabs.com www.pacifierimlabs.com

70 62 37 66 51 70 81 48 30 50 52 46 90 24 72 60


Page 7 of7

Acronyms used in reporting dioxins and furans:

TCDD = Tetrachlorodibenzo-p-dioxin PeCDD = Pentachlorodibenzo-p-dioxin HxCOD = Hexachlorodibenzo-p-dioxin HpCDD = Heptachlorodibenzo-p-dioxin OCDD = Octachlorodibenzo-p-dioxin

Acceptable recoveries for surrogates

TCDF = Tetrachlorodibenzofuran PeCDF = Pentachlorodibenzofuran HxCDF = Hexachlorodibenzofuran HpCOF = Heptachlorodibenzofuran OCOF = Octachlorodibenzofuran

EPA 1613

Mio (%)

Max (%)

13C12 -2,3,7,8-TCOD 13C12 -1,2,3,7,8-PeCDO 13C12 路1,2,3,4,7,8-HxCDD I3C12 -1,2,3,6,7,8-HxCDO I3 C I2 -1,2,3,4,6,7,8-HpCDD 13C12 -OCDD

25 25 32 28 23 17

164 181 141 130 140 157

13C12 -2,3,7,8-TCDF 13C12 -1,2,3,7,8-PeCDF 13C12 -2,3,4,7,8-PeCDF 13C12 -1,2,3,4,7,8-HxCDF 13C12 -1,2,3,6,7,8-HxCDF 13C12 -1,2,3,7,8,9-HxCDF I3C12 -2,3,4,6,7,8-HxCDF 13C 12 -1,2,3,4,6,7,8-HpCDF 13C12 -1,2,3,4,7,8,9-HpCDF

24 24 21 26 26 29 28 28 26

169 185 178 152 123 147 136 143 138

PacifieRim Laboratories Inc, #103, 19575-55A Avenue,Surrey, BC V3S 8P8 Canad谩 Tel: + 604.532.8711 Fax: + 604.532.8712 Email: info@pacificrimlabs.eom www.paciflcrimlabs.com


Exova # 104, 19575-55 A Ave. Surrey, e: itish

T: +1 (804) 514-3322 F: +1 (604)514-3323 E: SurreY@8xova.Ulm

V3S 8P8, Canada

\o.: :

Exova

W\NW .c:.JtOJd.com

1111111

Report Transmission Cover Page BiI! To:

Paeifie Rim Laboratories Ine.

Project:

Report To:

Pacifie Rim Laboratories Ine.

ID:

#103, 19575 - 55A Avenue Surrey, BC, Canada

Name: Location:

V3S8P8

LSD:

Oave Hope

P.O.:

Atto:

UPM

Lot ID: Control Number:

907654

Date Raeeived: Nov 23,2012 Date Reported: Report Number:

Oee 3.2012 1788204

Acctcode:

Sampled By: Company:

Contact &Affiliation

Address

Delivery Commitments

Dava Hopa Paeific Rim Laboratories Inc.

#103. 19575-55AAvenue Surrey, British Columbia V3S 8P8

On [Lot Venfication] send

Phone: (604) 532-8711 Fax: (604) 532·8712 Email: dave@pacificrimlabs.com

(COA) by Email - Single Report On [Raport Approval] send (COC, Test Report) by Email • Merge Reports On [Lot Approval and Final Test Report Approval] send (COC, Test Report. Invoiee) by Hand Deliver

M

On [lot CreaUon] send (COR) by Email - Single Report Notes To Cllents:

• Sample 907654-1; 4253989 Sample 907654-1 was analyzed for Nitrite and Nitrate at 1:1Odilution due to high electrical conductivity. ' ''; 'Sample 90765'1-6; 4253994 Sample 907654-6 was analyzed for Chlorate at 1:5 dilution due to high electrical conductivity. Thls lead toour detectlon bXa factor of five.

uav .

r

e".

The information contained on this and all other pages transmitted, is íntended for the addressee only and is considered confidential. If the reader is not the intended recipient. you are hereby notified that any use, dissemination, distribution or copy of this transmission is strictly prohibited . If you receive this transmission by error, or ir this transmission is not satisfactory , please notify us by telephone . 'reems and Condilions: ww. ·.BXOV3.calterms&conditionr


·

ExO\... 19575-55':' A!e. f UTe: . S,mt h Cotumbi a CPC. Canada

T: +1 (604) 514-3322 F: +1 (604) 514-3323 E: Surre¡@ exovacom W: www.eXO·.8......cm

Exova

1I11111

Sample Custody BiII To: Paeifie Rím Laboralories Ine. Report To: Pacifie Rim Laboratories Ine.

Attn:

Project: ID: Name:

#103. 19575 - 55A Avenue Surrey, BC, Canada

Location:

V3S 8P8

LSD:

Dave Hope

P.O.:

Sampled By:

Lot ID: Control Number:

UPM

Dale Reeeived:

907654 Nov 23,2012

Date Reported: Dee 3, 2012 Report Number:

1788204

Acctcode:

Company:

Sample Disposal Date: January 02, 2013 AII samples will be stored until this date unless other instructions are received. Please indicate other requirements below and return this form to the address or fax number on the top of this page.

o

... Sample Storage Until

-----------

The following charges apply to extended sample storage: Storage for an additional 30 days Storage for an additional 60 days Storage for an additional 90 days

o

$ 2.50 per sample

$ 5.00 per sample $ 7.50 per sample

Return Sample, collect, to the address below via:

O Greyhound DDHL Dpurolator

D Name Company Address Phone Fax Signature

Terms and Con':'lions: www.eXOV.l.calterm:·1condilions

(MM/DDNY)

!


Exova 1,.104,19575055A AVJ.

Paga 1 of 10

T; +1 P 4) F; +1 (604) E:

SUfre¡ . Britísh Columbia

V3S apa, Canad a

W:

Exova

wyJw.eXOYa.r:)m

Analytical Report BiI! To:

Pacific Rim Laboratories Inc.

Report To: Paeifie Rim Laboratories Ine.

Projeet:

# 103, 19575 - 55A Avenue

Name:

Surrey, BC, Canada

Localion : LSO:

V3S 8P8 Attn: Oave Hope Sampled By:

Lot ID: Control Number:

UPM

10:

907654

Date Reeeived: Nov 23, 2012 Date Reportad: Oee 3,2012 Report Number:

1788204

P.O.: Acetcode:

Company:

Reference Number Sample Date SampleTime Sample Location 5ample Descrlption Matrix Analyte

Units

907654-1 Nov20 , 2012 NA PR122428 Wastewater

Results

Results

Results

Nominal Dateetlon limll

Routl ne Water Nitrate - N .

mg/L

<0.1

0.01

Nitrite - N Nitrate and Nitrite • N

mg/L

<0.05

mglL

<0.1

0.005 0.01

".. .....e

'-"W: ",:

Tarms and Conditions: WW\'.'.exo\ "a.cal ierms&condítiono


Exova

A Ay4. British Columrna

Page 2 of 10

T: +1 (604) 514-3322 F: +1 (604) 514-3323 E:

Exova

W:

V3S 8P8, Canada

Analytical Repart BiI! To: Paeine Rim Laboratories Ine. Report To:

Lot ID:

ID:

#103, 19575 - 55A Avenue

Name: Location:

Surrey, BC, Canada V3S8P8 Attn:

Projeet:

Paeifie Rim Laboratories Ine.

Oave Hope

UPM

Control Number: Date Received:

907654 Nov 23, 2012

Date Reported: Dee 3, 2012

LSO:

Report Number:

1788204

P.O.:

Sampled By:

Acetcode:

Company:

Reference Number Sample Date SampleTlme

Nov 20, 2012

907654-1

907654-2 Nov 20, 2012

907654路3 Nov20, 2012

NA

NA

NA

PR122428 Wastewater

PR122429

PR122431

Wastewater

Wastewater

Results

Results

Results

Sample Location Sample Description Matrlx Unlts

Analyte

Nominal Deta ction

Umi'

Aggregate Organlc Constituents mg 02/L

Chemical Oxygen Oemand

mg/L

Phenol Oif and Grease pH adjustment

",

.

.. ..

Terms and Condilion s:

Total required prior to O&G extraction

mg/L

160

5 0.002

<0.002 <1 No

1


E .ova

Page 3 of 10

T: +1 (604} 514-3322 F: +1 (60.:) 5 14.z323

#104, 19575-55 A Avp. British Columbia

ap8 . Can?da

Exova

E: ";urreY@exova.com W: WWW.eXDV8.c.:.m

Analytical Report BíII To :

Pacific Rim Laboratoríes Ine.

Project :

Report To:

Paclñc Rim Laboratories Inc.

ID:

# 103,19575 - 55A Avenue

Name :

Date Received:

Nov 23,2012

Surrey, BC, Canada

Location:

Date Reported :

Dec 3,2012

Attn :

V3S8PB

LSO:

Oave Hope

P.O.:

Lot ID: UPM

907654

Control Number:

Report Number:

1788204

Acctcode:

Sampled By: Company:

907654-1

907654-6

907654-7

Sample Date

Nov20.2012

Nov 20, 2012

Nov20.2012

SampleTime

NA

NA

NA

Reference Number

Sample Loeation PR122428

PR122436

PR122437

Wastewater

Wastewaler

Waslewaler

Unlts

Results

Resu tts

Results

mglL

<0.05

0.05

mglL

0.9

0.06

Sample Deserlptlon Matrlx Analyte

Nominal Dets<:tlon Limit

Inorgante Nonmetallie Parameters Ammonia -N Kjeldahl Nitrogen

Total

Sullide

Tolal

mg/L

Chlorate

Dissolved

mglL

Hydrogen Sullíde

Calculated

mglL

Terms end Condi tions: w ,yw.exova .caltermc&conditíons

0.020 <0.5

0.005 0.1

0.021


Exova # 104 . ':UI"rB; ",

A Avo. Columbia

Paga 4 of 10

T: +1 (604) 514-3322 F: +1 (604) 514-3323 E: Surrey(:j exov'1.com

Exova

W; www.exova.tJm

V3S 8P8.

Ahalytical Report BiII To:

Paeifie Rim Laboratories Inc.

Projeet:

Report To:

Paeifie Rim Laboratories Ine.

10:

Altn:

Lot ID:

UPM

907654

Control Number:

#103, 19575 • 55A Avenue

Name:

Date Received :

Nov 23,2012

Surrey , BC, Canada

Location:

Date Reportad :

Dee 3, 2012

V3S 8P8

LSO:

Oave Hope

P.O.:

Sampled By:

Raport Number.

1788204

Acctcode:

Company :

Reference Number Sample Date SampleTime Sample Location Sample Descrlplion Matrlx Analyte

Units

907654-4 Nov 20,2012 NA PR122432 Wastewate r

Results

Results

Results

Nominal Oetactian

ljrnn

Extractable Petroleum Hydrocarbons - Water EPHw 10-19

ug/L

129

100

EPHw 19·3 2

uglL

<100

100

Terms and Condiliona: www.exov:t.caI\erms&coodWoos


Page 5 of 10

T: .1 (804) 51·:-3322 F: ' 1 (801) 5 14-3323

E::o:a '1 04. 1&;;75-55 A A e. British Colur,lbia .y 3S. Canad3

E: W:

Exova

WWW .eXD V:' .C J m

Analytical Report BiII To:

Paeifie Rim Laboratories Ine.

Project:

Report To:

Paeifie Rim Laboralories Ine.

ID:

#103, 19575 - 55A Avenue

Name:

Surrey, BC, Canada V3S 8P8

Location: LSO:

Altn :

Oave Hope

Lot ID: Control Number:

UPM

Date Received :

907654 Nov 23,2012

Date Reported : Oee 3,2012 Report Number. 1788204

P.O.: Acctcode:

Sampled By: Company :

Reference Number Sample Date SampleTlme

907654-5 Nov20, 2012 NA

Sample Location Sample Descrlptlon Matrix Analyte

PR122433 Wastewater Nominal Deteclion

Units

Results

Aeephate

uglL

Aspan Azinphos-ethyl

ug/L uglL ug/L ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L ug/L ug/L uglL

<0.5 <0.5

0.5

<0.5 <0.5

0.5 0.5

Results

Results

Limi!

Organophosphate Pesticides In Water

Azinphos-methyl Bromophos Broníophos celhyl Carbophenolhion Chlorfenvinphos Chlormephos Chlorpyrifos Chlorpyrifos-melhyl Chlorthiophos Cyanophos Oemelon Oiazinon

ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L ug/l ug/l ug/l ug/L ugll ug/L uglL ug/L ug/L ug/L

Diehlofenthion Dichlorvos Oierolophos O!rnelhoale Ojsulfoton EPN Elhion f':lnqhlorphos Fenílrolhion Fenlhion Fonofos Isofenphos Malaoxon Malalh ion Melhidalhion Melhyl Parathion Mevinphos Omelhoate f'13l!'llhion Phorate Phosalone ; . .;

Terms ?_nd Condilicns:

WYfiN.eX!:)'.

0.5

<0.5

0.5

<0.5 <0.5

0.5

<0.5

0.5 0.5

<0.5 <0.5

0.5 0.5

<0.5 <0.5

0.5

<0.5 <0.5 <0.5

0.5 0.5 . 0.5' - ' .. 0.5

<0.5

0.5

<0.5 <0.5

0.5

<0.5 <0.5 <0.5

0.5 0.5 0.5 0.5

<0.5

0.5

<0.5 <0.5

0.5

<0.5

0.5 0.5

<0.5

0.5

<0.5 <0.5

0.5 0.5

<0.5

0.5

<0.5 <0.5 <0.5 <0.5

0.5 0.5 0.5

<0.5

0.5 0.5

<0.5

0.5

<0.5

0.5


E!tova

Page 6 of 10

T: +1 (604) (;14-:' 32 2 F; +1 (604) 5 14-3323

f,路104. 1J575-5 5 A Av a.

Exova 1I1111l

E:

British Columbi:

C. ,ad.

W; www .axova .com

Analytical Report BiII To:

Paeifie Rim Laboratories Ine.

Report To: Paeific Rim Laboralories Inc.

Attn:

Projeet: ID:

Lot ID:

UPM

907654

Controi Number:

#103, 19575 - 55A Avenue

Name:

Dale Received:

Surrey, BC, Canada

Location:

V3S 8P8

Date Reported: Dec 3,2012

LSD: P.O.:

Dave Hope

Sampled By:

Raport Number:

Nov 23, 2012 1788204

Acetcode:

Company:

Reference Number Sample Date

907654--5 Nov 20, 2012

SampleTime

NA

Sample Location Sample Descriptlon

PR122433

Matrix

Wastewaler

Analyte

Results

Results

Nomina' DetectJon lirnjt

Unlts

Results

ug/L ug/L ug/L ug/L ug/L ug/L ug/L uglL uglL ug/L

<0.5

0.5

<0.5 <0.5

0.5 0.5

<0.5

0.5

Organophosphate Pestlcldes in Water路 Contlnued Phosmel Phosphamldon Pirimiphos-ethyl Pirimiphos-methyl Profenofos

' Pyrazophos Quinalophos Sulfotep Terbufos Tetrachlorvinphos

<0.5

0.5

<0.5 <0.5

0 .5 0.5

<0.5

0.5

<0.5 <0.5

0.5 0.5

Organophosphate Pesticides -Water- Surrogate Rec. TPP

Terms a n-铆Condilion:.: v

Surrogate

%

99

50-140


Page 7 of 10

r.

Excva r-1D4, 1957S-55 A Av e. 3utre: . British Columbia

+1 (8D4) 514-:·322 F: ...1 ('-04) 514-3323

'13S ';PB, Canada

W: W'ñW.exov a.com

Exova

E:

Analytical Report BiII To:

Pacifie Rim Laboratories Ine.

Project :

Report To:

Paeifie Rim Laboratories Ine.

ID:

Altn:

Lot ID: UPM

907654

Control Numbe r:

#103 , 19575 - 55A Avenue

Name:

Date Reeeived:

surrey, BC, Canada

Location:

Date Reported : Dee 3,2012

V3S 8P8

LSD:

Dave Hope

P.O.: Acct cods :

Sampled By:

Report Number:

Nov 23,2012 1788204

Company :

907654-8

907654-9

Sample Date

Nov 20, 2012

Nov 20, 2012

SampleTime

NA

NA

Reference Number

Sample Locallon Sample Descrlption Matrlx Units

Analyte

PR122438

PR122439

Wastewate r

Wastewater

Results

Results

Results

Nominal OeteClion blrolt

Metals Total <0.00001

0.00001

Mereury

Total

mgfL

Aluminum

Total

mgfL

0.036

0.005

Antimony

Total

mg/L

0.0053

0.0001

Arsenic

Total

mgfL

0.00274

Barium

Total

mglL

0.188

Beryl/ium

Total

mgfL

<0.00005

Bismuth

Total

mglL

<0.0001

Boron

Total

mglL

0.047

Cadmium

Total

mglL

0.00005

Calcium

Total

mgfL

Chromium

Total

mglL

0.0281

152

0.00005 0.00005 . 0.00005 0.0001 .002 0.00001 0.05 0.0005

Cobalt

Total

mgfL

0.0001

0.0001

Copper

Total

mglL

0.0010

Iron

mgfl

0.033

Lead

Total Total

0.0001 0.002 .

mglL

0.0001

Lithium

Total

mgfl

0.0047

Total

mgfL

Manganese

Total

mglL

Molybdenum

Total Total

Potass íurn

Total

mgfL

Selenium

Total

mg/L

17.9

0.0005 0.04

0.0218

0.001 ·

mgfL

0.0349

0.00005

mglL

0.129

0.0002

Silicon

Total

mgfL

Silver

Total

mglL

Sodium

Total

mglL

Strontium

Total

mglL

59.7 0.0003 10.5 0.00008 911 0 .519

0.1-. 0.0001 0.02 0.0005 0.1 0.0001

Thallium

Total

mglL

0.000 18

0.00001

Thorium

Total

mglL

0.00001

0.00001

Tin

Total

mglL

<0.0001

0.0001

Titanium

Total

mg/L

0.0010

0.0005

Uranium Vanadíum

Total

mglL

0.00004

0.00001

Total

mglL

0.0543

0.0001

Zinc

Total

mglL

0.0192

0.0005

Zirconium

Total

mglL

<0.0005

0.0005

Terms

COflditions:


Exova

#104.

A k !e.

SurrJ¡ . British Columbia V3S BPB.

Page 8 of 10

T: ., (804) 514-3::22 F: ., (804) 514-3323 E: W: w.YW.exaJ::.com

Exova

Analytical Report BiII To :

Paeifie Rim Laboratories Inc.

Project :

Report To:

Pacifie Rim Laboratories Ine.

ID:

Attn:

Lot ID: UPM

#103, 19575 - 55A Avenue

Name:

Surrey, BC, Canada

Location :

V3S 8P8

LSO:

Oave Hope

P.O .:

Sampled By:

907654

Control Number: Date Received:

Nov 23, 2012

Date Reported:

Dee 3,2012

Report Number:

1788204

Acctcode:

Company:

Reference Number

907654-10

Sample Date

Nov 20,2012

SampleTime

NA

Sample Localion Sample Descrlptlon Matñx Analyte

Unlts

PR122440 Wastewater Results

Results

Results

Mlcrotox Interpretation (ERCB 0050)

Pass % Sample

>100

5 minutes

%Sample

>100

15 minutes

% Sample

>100

5 minutes

%Sample

>100

EC50

15 minutes

EC50 EC20 EC20 Lab Treatment

None

Microtox Model 500 unit #

330

SampleType

SumpUquid

pH

Clarified Sample- Initial

Turtlidity

As Reeeived

None

7.8

Colour

As Reeeived

Yellow

Colou r

As Tested

Yellow

Turbid ity

As Tested

pH

Clarified Sample- Final

95% Confidence Factor

(EC50 - 5 Minutes)

N/A

95% Confidence Factor

(EC20 - 5 Minutes)

N/A

95% Confidence Factor

(EC50 -15 Minutes)

N/A

95% Confidence Factor

(EC20 - 15 Minutes)

N/A

Colour Corrected Data

None Not Adjusted

No

Approved by: Antho ny Neumann, MSc Laboratory Operations Manager Tenns and Condilions:

W.Y 4·.eXOYJ..Wt1rms&ccnditions

Nominal Oeteclion Urol!


Exove :.:104, A Ave. Surre: , Brilish Columbia

T: +1 (604)514-3322 F: +1

V3S 8P8, Canadá

W; www.erc ve.ccm

Paga 9 of 10

Exova

E:

Methodology and Notes BiI! To:

Paeilie Rim Laboratories lne.

ProJect:

Report To:

Paeifie Rim Laboratories Ine.

ID:

#103, 19575 - 55A Avenue

Name :

Surrey, BC, Canada

Location :

V3S 8P8

LSO:

Oave Hope

P.O.:

Attn: Sampled By:

Lot ID: UPM

907654

Control Number: Date Received :

Nov 23, 2012

Date Reported:

Dee 3,2012

Report Number:

1788204

Acct code:

Company:

Method of Analysis Method Name

Reference

Ammonium-N in Water

APHA

Anions (Routine) by Ion Chromatography

APHA

BC ICP-MS Tolal Melals in Water

USEPA

BC Trace Total Melals in Water

APHA

·

Chemical Oxygen Demand in water

APHA

·

Chlomte and Chlorite by Ion Chromatography

APHA

·

EPH -Water

BCELM

Mercury Low Level (Total) in water (Surrey)

EPA

Microtox-15 Minute Multiple Concentration, EC50

Environment Canada

Oíl and Grease in water (Surrey)

BCELM

Organophosphate Pesticides - Water

USEPA

Phenol in water

Method

Date Analysis Slarted

Location

28-Nov-12

Exova Edmonton

Ion Chromatography with Chemical Suppression of Eluent Cond., 4110 B

28-Nov-12

Exova Edmonton

Determination of Trace Elements in Waters and Wastes by ICP-MS , 200 .8

28-Nov-12

Exova Edmonton

Inductively Coupled Plasma (ICP) Method , 3120 B

28-Nov-12

Exova Edmonton

Closed Reflux, Colorimetrie Method, 5220D

29-Nov-12

Exova Edmonton

Ion Chromatography with Chemical Suppression of E/uent Cond., 4110 B

28-Nov -12

Exova Edmonton

• Automated Phenate Method , 4500 NH3G

· ·

· ·

Extraclable Petroleum Hydrocarbons 28-Nov -12 (EPH) in Water by GC/FID , EPH Water

Exova Surrey

Mercury in Water by Cold Vapor Atomie Fluorescence Spectrometry, 245 .7

27-Nov-12

Exova Surrey

Biological Test Melhod: Toxieily Test Luminescent Bacteria , 1/RM/24

28-Nov-12

Exova Edmonton

Di! & Grease in Water - Oireet Hexane Extraction, Oil & Grease

29-Nov-12

Exova Surrey

OP Compounds by GC: Capillary Column Technique, 8141B

28-Nov-12

Exova Calgary

APHA

Direct Photometrie Melhod, 5530 D

29-Nov-12

Exova Edmonton

Sulfide in water

APHA

• Gas Dialysis, Automated Methylene Blue Method, 4500-52- E

29-Nov-12

Exova Edmonton

Tolal and Kjeldahl Nitrogen (Tolal) In Water

ISO

• Water auality - Determlnation of nitrogen,lSOITR 11905-2

27-Nov-12

Exova Edmonton

·

· ·

• Re_ce Method Modified

References APHA

Standard Melhods for Ihe Examination of Water and Wastewater

8.C.M.0.E

B.C. Minislry of Environment

BCELM

B.C. Environmental Laboratory Manual

Environment Canada

Toxieity Test Using Luminescent Bacteria

ISO

Inlemalional Organization for Slandardization

USEPA

US Environmental Proteetion Agency Test Melhods

Terms an j Conditions : WW\y.exova.caltermt.&cenditions


Exova

t' 104, 19575-55 A AVQ. Surrey. e ritish Columbia V3S Cenaoa

Page 10 of 10

T: +1 (fJ4) F: +1 (604)51 4-3323 E:

·wV:

Exova

\ JWY.· ,e XOVB! . -Jm

Methodology and Notes Bilf To: Pacific Rim Laboratories Inc. Repor! To: Pacific Rim Laborateries Inc.

Attn:

Proje ct: ID: Name:

#103, 19575 - 55A Avenue Surrey, BC, Canada V3S 8pa

Location: LSD:

Dave Hope

P.O.:

Lot ID: UPM

907654

Control Number: Date Received: Nov 23, 2012 Date Reported : Oec 3,2012 Repor! Number:

1788204

Acct code:

Sampled By: Company:

Comments: • Sample 907654- 1; 4253989 Sample 907654-1 was analyzed for Nitrite and Nitrate at 1:10 dilution due lo high electrical conductivity . • Sample 907654-6; 4253994 Sample 907654-6 was analyzed for Chlorate at 1:5 dilulion due te high electrical conductivity. This lead to our detection Iímil to increase by a factor of five .

Please direct any inquiries regarding this report to our Client Services group. Results relate only to samples as submitted. The test report shall not be reproduced except in full, without the written approval of the laboratory . Terrns and Condition ::,. : v. }."N.exova.calt erms &condífi ons


โ€ข

COMISION ADMINISTRADORA DEL RIO URUGUAY LABORATORVANALVSIS PURCHASE ORDER

.OT: 907654

COC

1111111111111

LABORATORV: PACIFIC RIM

n

ADDRESS: #103, 19575 - 55A Avenue - Surrey, B. C. Canada - V3S 8P8 TEL: 001-604-532-8711

FAX: 001-604-532-8712 QUOTATION: e-mail frorn Oave Hope DATE OF SAMPLES : 20/11/2012

23 UOV \ Z

LOCATION: UPM BOX: 2

, '-DO

SENO REPORT TO: Eng. Alejandro Areelus

JP c.ยกb

e-mail: arcelus@earu.org.uy Tel: (005982) 47225500 ext 106 Fax: (005982) 47226786

Analysis

Volume Bottle ( P: Plastic, (mi) AG: Amb Glass }

Preservation

Sealing # (CARU 10#)

Nitrate+Nltrite

\-').. tยก,42.g

Ammonia

-

1000

p

H2S04 ce. 2ml/l (pH<2)

1227876

Phenolie substanees

1000

AG

H2S04 ce. 1 ml/l (pH<4)

1227649

,\ 243 \

Oi! and Grease

1000

AG

H2S04 ce. (pH<2)

1227648

Z

'').431-

Total Petroleum Hydrocarbons

1000

AG

H2S04 ce. (pH<2)

1227881

{p

COO TKN (Total Kjeldhal Nitrogen)

.\

.

Z, \V


COMISION ADMINISTRADORA DEL RIO URUGUAY

\2.-2433

Organophosphate biocides

1000

AG

HCL O.1M to 3.5 <pH<4.5

-2

1227880

"" A't " JI"'''-

-.

-

1 /1 "

<2)

-"- -

250

P

NaOH O,2M, lml/100mL (pH>8)

1227875

<1

43-:r

Sulphide

250

P

Zinc Acetate 10%, 1 ml/l

1227890

6

438'

Metals (except Mercury)

125

P

HN03 cc. 2 ml/L, (pH <2)

1227873

a

P

K2Cr207 5% in HN03 (1+1) 1 ml/100ml (pH <2)

1227874

Refrigerate

1227872

"? ,

.:ita q ......

Mercury Microtox ECSO

.

. , .....

Ch/orates

'2 t\'3\P

"

rol"

125 125

P

Important Note: Identify the reported results of ea eh sample with the seeurity seal attaehed to eaeh bottle and the date of analysis .

. :.- '

Ing. ALEJANDRO ARCELUS SecretarIo Técnlco-CARU

".

-:

'2

...

... ..

......


vy r-'. Exo'll'c #104 . 19575-55 A AVD.

Surrey.Brilish Columbia V3S 8P8 . canada

T: +1 (604) F: +1 (604) 514-3323 E: Surrey@exov •. com W: W'MY.exova,com

Report Transmission Cover Page Bill To:

Paeifie Rim Laboratories Ine.

Project:

Report To:

Pacifie Rim Laboratories Ine.

ID:

Attn:

Lot ID: UPM

907660

Control Number:

#103, 19575 - 5SA Avenue

Name:

Date Receíved:

Nov 23, 2012

Surrey, BC. Canada

Location :

Date Reported:

Oee 12, 2012

V3S 8P8

LSO:

Oave Hope

P.O.:

Report Number:

1788212

Acctcode:

Sampled By: Company:

Contact & AffiUation

Address

Oelivery Commítments

OaveHope

#103, 19575 - 5SA Avenue

On(LotVerifieation]send

Paeifie Rim Laboratories Ine.

Surrey . British Columbia V3S 8P8 Phone: (604) 532·8711 Fax: (604) 532-8712 Email: dave@paeifierimlabs.com

(COA) by Email - Single Report On (Report Approval] send (COC, Test Report) by Email - Merge Reports On (Lot Approval and Final Test Report Approval] send (COC, Test Report, Invoice) by Hand Oeliver

M

On (Lot Craation] send (COR) by Email - Single Report Notes To Cllents:

=

• Mise 1 Daphnia Magna • Oaphnia Magna analysis was performed by a subcontract laboratory. See attaehed 1 page report 12-515249. • pH analysis was performed past the recommended holding time of 15 minutes from sample eolleelion .

The information contained on thls and all other pages transmitted, is intended for the addressee only and is considered confidential. If the reader is not the ¡ntended recipient, you are hereby nolified that any use , disseminalion, distribulion or copy of thís transmission is strietfy prohibited . If you necaive this transmission by error, or if this transmission is not satistaetory, please notify us by telephone. Tarrosand Conditicns:


Exova

T: +1 (604) 5 14-3322 (604) 514-3323 F: E: Surrey@excva.com

+,

#104, 19575-55 A Ave . Surrey . British Colu mbia V3S 8P6. Canada

Exova

W: WY/N.9xova.com

Sample Custody BiII To:

Pacific Rim Laboralories Ine.

Project:

Report To:

Pacilic Rim Laboratories Ine.

ID:

#103, 19575 - 55A Avenue

Name:

Date Received:

Nov 23, 2012

Surrey, BC. Canada

Locatlon:

Date Reporled :

Dee 12, 2012

Attn:

V3S 8P8

LSO:

Dave Hope

P.O.:

Sampled By:

Lot ID:

UPM

907660

Control Number:

Report Number:

1788212

Acetcode:

Company:

Sample Disposal Date: January 11, 2013 AII samples will be stored until this date unless other instructions are received. Please indicate other requirements below and return this form to the address or fax number on the top of this page.

D

Extend Sample Storage Until

-----------

The following charges apply to extended sample storage: Storage for an additional 30 days Storage for an additional 60 days Storage for an additional 90 days

o

$ 2.50 per sample $ 5.00 per sample $ 7.50 par sample

Return Sample, collect, to the address below via:

O Greyhound ODHL

D Purolator D Other (specify) Name Company Address Phone Fax Signatura

Terms Jnd Cond 铆ttons: w\w'路.BXOV8.ca/terms&condiUons

(MM/DDNY)


Exova # 104. 19575-55 A Ave.

T: +1 (604) 514-3322 F; +1 (W4 ) 514-3323

Su,rey. British Columbia V3S eP B. Canada

W; WWYI.Bxova.com

Paga 1 of3

Exova

E:

Analytical Report BiI! To: Paeifie Rim Laboratories Ine. Report To: Paeifie Rim Laboratories lne. #103,19575路55AAvenue Surrey, Be , Canada V3S 8P8

Projeet: ID:

Lot ID: UPM

907660

Control Number: Date Received: Nov 23, 2012

Name: Location:

Date Reported: Dee 12. 2012 Report Number: 1788212

LSD:

P .O.:

Attn: Dave Hope

Aeetcode :

Sampled By: Company:

Reference Number Sample Date SampleTime

NA

Sample Locatlon Sample Descrlption

PR122452

Matrlx

Wastewater

Units

Analyte

907660-1 Nov20.2012

Results

Results

Re8ulta

Nominal Del8c1ion Umjt

Physlcal and Aggregate Propertles Solids Solids

Total Total Suspended

Routine Water Eleetriea! Conduetivity

TBrms and Conditions: '.路tWW.Bxova.callerms&C"ln ditions

mg/L mg/L

3370

IJSlcm al 25 e

4240

<2

5 2


Exova

#104, 19575-55 A Ave. Su,rey, British Columbia V3S

epe, Canada

Page 2 of 3

T: ' 1 (604) 514-3322 F: +1 (604) 514-3323 E: Surrey@e;;.,va.com W; W\'oIW.exo"-s.com

Exova

Analytical Report Bil! To:

Paeilie Rim Laboratories Ine.

Repar! To:

Paeifie Rim Laboratories Inc.

Project: ID:

#103,19575 - 55A Avenue

Name:

Surrey. BC. Canada V3S 8P8

Location: LSO:

Attn: Sampled By:

Dave Hope

LotlO: Control Number:

UPM

P.O.:

907660

Date Received:

Nov 23.2012

Date Reporled: Report Number:

Oee 12, 2012 1788212

Acetcode:

Company:

Reference Number Sample Date SampleTlme Sample Locatlon

907660-3 Nov20.2012 NA

Sample Description

PR122454

Matrlx

Wastewater

Analyte

Unlts

Inorganlc Nonmetalllc Parameters Phosphorus Total

mg/ L

Results

Results

1.03

NominalDetecl!on

Umi! 0.003

Approved by: Mathieu Simoneau Operations Manager Tenn s and Conditions; lMNW.exova.cd\erms&conditions

Results


Exova #104 . 19575·55 A Ave. Surrey. BriUsh Columbia V3S 8pe. Candda

Page 3

T: +1 (604) 514-:.322 F; +1 (604) 514-3323 E: Surrey@eltOva.com

ot 3

Exova

W: www.exova.com

Methodology and Notes BiII To:

Pacilie Rim Laboratories Inc.

Project:

Report To:

Pacilie Rim Laboratories Inc.

ID:

#103, 19575 - 55A Avenu e

Name:

Date Received :

Nov 23,2012

Surrey, BC, Canada

Location:

Date Reported:

Dee 12, 2012

Attn:

V3S8P8

LSD:

Dave Hope

P.O.:

Lot ID: UPM

907660

Control Number:

Report Number:

1788212

Acctcode:

Sampled By: Company:

Method of Analysis Date Analysis Started

Location

• ConduclMty, 2510 B

26-Nov-12

Exova Surrey

APHA

• Preliminary Aeid Hydrolysis, Ascorbic Aeid Reduclion Melhod, 4500-P B,E

27-Nov-12

Exova Surrey

Solids (Total, Fixed and Volatile)

APHA

• Total Solids Oried at 103·105'C, 2540 B

28-Nov-12

Exova Surrey

Solids Suspended (Total, Fixed and Volatile)

APHA

• Total Suspended Solids Drled at 103105'C, 2540 D

28-Nov-12

Exova Surrey

Method Name

Reference

AJk,pH, EC, Turb in water (Surrey)

APHA

Pnosphcrus - total (Iow level) • Surrey

Method

• Rof&rsncsMethodModlfied

References APHA

Standard Methods for the Examination of Water and Wastewater

Comments: • Mise 1= Daphnia Magna • Daphnia Magna analysis was performed by a subcontract laboratory. Ses attaehed 1 page report 12-515249. • pH analysis was perfonned past lhe recommended holding time of 15 minutes from sample eolleclion .

Please direct any inquiries regarding this report to our Client Services group. Results relate only to samples as submitted. The test report shall not be reproduced except in tull, without the written approvaJ of the laboratory. Terms and Conditions: WVM'.exova.calterms&condilions


Appendix CI/ent:

j'

2260312 PR122453- 2012-11·26

lIb. No: Your referenee: MatrIx: Sempled by: Slte .ampled

Date and hourstartana/ysls (Ohra):

2012·11·28

ECSO-48h ('lovlv): lower CJ. at 95%: Upper C.I. al 95%: Calculatlon melhod:

>100

NA NA Aucune méthode ulilisée

Ana/YSed by:

JeJB

15:00

l%vM

01'1

O

O

6.25

10 10

12.5

2012·11·26 2012-11-28 10:30:00

ConfOll11

2012-11-30

15:00

20

Average number of neonates perbrood: Age attlrat brood (days): Number of Daphnlalcontalner: loadlngdenslly (mUDaphnla): Volume oflest soIut/ons (ml): Pholoperfod: Dllutlon water: Culture Ind dllUlJon water hardnen (mg/L CaC03): Pr.aeratlonof SImple: Pre-aerallon rate (mUmlnIL t1): SImple hardneas (mg/L CaC03): SImple hardness adjusted (mg/L CaC03): Pre-trealment of limpie: Protocoll Reference method: ImmobllJty Immoblllty 48hra 48hrs (number) ('.)

Date andhourend ana/YSls (48hra):

NA

Dlphnt. m.gn. «24 heures) <1% ofmortafltY ofbrood stock 7 days before test

Organltms:

number of

.

Sampllng method: Date sampled (date endhour): Date recalved (date andhour): . StIte of aampled recelved:

Water NA NA

sampJe concentraUon

12-515249

Request number:

EXOVA (NORWESn

8

10 30

300 16hrs lighl/8hrs darlmess Dechlorinated municipal water, hardness adiusted

168 Ominute NA 460 NA NA

5PE11RM'14, 2000 temperatura ("C)

conducllYlty (pS/cm)

mortallty 48hrs (number)

mortallty 48hra

Ohrs

48hrs

ohrs

48111'11

ohrs

O

O

O

18.3

18.6

7.4

7.6

8.7

8.2

517

O

O

O

O

18.5

18.4

7.4

7.6

8.9

8.4

863

10

O

O

18.5

18.4

7.6

8.3

O

O

O

18.6

18.5

8.6

8.4

1127 1751

50 100

10

O

O

O

O

18.8

18.4

7.7 7.7

7.7 7.8

8.9

10

O O

O

25

8.0

9.0

8.6

2888

10

O

O

O

O

19.0

18.5

7.8

8.3

9.0

8.2

5120

SImple characterfstlcs befare analysls Reference as.ay(Potasslum dlehromate): Reference auay date: lCo50-48h (mg/l of Cr): Lower C.I. at 95%: lower CJ. at95%:

ADD8arance YelIow.clear

2012·11-30 0.306 0.292 0.321

(%)

18.8 Geometrle average: lower control "mil: Upper controlllmlt:

C1I1SOlVIlI

pt1

7.7

oxygen Cm ILI

8.4

48hrs

ohrs

5OBO

0.309 0.211 0.408

lhis certificate muBt notbereproduced. exceplln irl entir&ly, wi1IJoot wrillen cansent from !he laboratary. lhe offlc:lal VlIr&ion ollhlsC8f1fficBle I1pratec!&d andcannol be modified. lhe ebove-mentionne<! samp!es Wllberellllne<! lo!a period of 30daysfDUowlng !he Í$&ue of lhiscartlficBle with lhe8Xcepllon 01 m!crobic!ogy lample.s cras1ns1rUcllld bytlieclienL Resulls pertain only IDlhesarnpfe$ submilllld lar analysis.


โ€ข

COMISION ADMINISTRADORA DEL RIO URUGUAY LABORATORY ANALYSIS PURCHASE ORDER LABORATORY: PACIFIC RIM

-,01: 907660

I""

COC

ยกWI

ADDRESS: #103, 19575- 55A Avenue- Surrey, B. C. Canada - V3S 8P8 TEL: 001-604-532-8711

FAX: 001-604-532-8712 QUOTATION: e-mail from Dave Hope DATE OF SAMPlES : 20/11/2012 LOCATION: UPM BOX:3 SENO REPORT TO: Eng. Alejandro Arcelus e-mail: arcelus@caru.org.uy Tel: (005982) 47225500ext 106 Fax: (005982) 47226786

Analysis

1-

(\ 245 3

i\

Total Suspended . Solids TotalSolids Conductivity Oaphnia magna Total Phosphorous

Volume (mI)

80ttle (P: Plastic,AG: AmbGlass)

Preservation

Sealing# (CARU ID #)

2xlOOO

P

Refrigerate

1227650

2xl000

P

Refrigerate

1227877

1000

AG

H2S04 ce. 2ml/l (pH<2)

1727863

P

7


Profile for Fundavida Gualeguaychu

Anexo 38  

Anexo 38  

Profile for fundavida
Advertisement